Investigation of strengthening mechanisms in an additively manufactured Haynes 230 alloy
Source abstract
Abstract
Abstract There are abundant studies on additive manufacturing of Ni alloys, such as Inconel 718. However, the studies on the microstructure and the deformation behavior of solid solution strengthened Ni alloys, such as Haynes 230, are limited. Here we compare the microstructure and the mechanical behavior of as-printed and stress-relieved Haynes 230 Ni alloys prepared by laser powder bed fusion. Transmission electron microscopy analysis revealed M23C6 carbides decorated at the dislocation cell walls in the as-printed material transformed to well-aligned arrays of M6C nanoprecipitates separated by an array spacing of 500 nm after stress-relief (heat treatment). The nanoprecipitates in stress-relieved alloy have formed numerous aligned orientation relationships with the matrix despite their large lattice mismatch. Post-tension microscopy analyses demonstrated high-density dislocation networks in the as-printed samples, whereas high-density stacking faults and nanoscale deformation twins were observed in the stress-relieved counterparts. This study provides insights for understanding the influence of nanoprecipitates on the deformation mechanisms of additively manufactured Ni alloys.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Additive Manufacturing and 3D Printing Technologies
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (81)
Show source-provided references
1. Weldability Studies of Haynes(R)-230 Alloy
2. Veverkova · HIGH TEMPERATURE MICROSTRUCTURAL DEGRADATION OF HAYNES ALLOY · 2008 · 230
3. The machinability of nickel-based alloys: A review10.1016/S0924-0136(98)00314-8 ↗
4. A review on sintered nickel based alloys
5. T.G. Gallmeyer, S. Moorthy, B.B. Kappes, M.J. Mills, B. Amin-Ahmadi, A.P. Stebner, Knowledge of process-structure-property relationships to engineer better heat treatments for laser powder bed fusion additive manufactured Inconel 718, Additive Manufacturing. 31 (2020). https://doi.org/10.1016/j.addma.2019.100977.10.1016/j.addma.2019.100977 ↗
6. Formation of the Ni3Nb δ-Phase in Stress-Relieved Inconel 625 Produced via Laser Powder-Bed Fusion Additive Manufacturing10.1007/s11661-017-4304-6 ↗
7. The role of side-branching in microstructure development in laser powder-bed fusion10.1038/s41467-020-14453-3 ↗
8. New insights on cellular structures strengthening mechanisms and thermal stability of an austenitic stainless steel fabricated by laser powder-bed-fusion
9. S.A. Khairallah, A.T. Anderson, A.M. Rubenchik, W.E. King, Laser powder-bed fusion additive manufacturing: Physics of complex melt flow and formation mechanisms of pores, spatter, and denudation zones, Additive Manufacturing Handbook: Product Development for the Defense Industry. 108 (2017) 613–628. https://doi.org/10.1201/9781315119106.10.1201/9781315119106-33 ↗
10. Laser powder-bed fusion additive manufacturing: Physics of complex melt flow and formation mechanisms of pores, spatter, and denudation zones10.1016/j.actamat.2016.02.014 ↗
11. Determination of True Temperature in Selective Laser Melting of Metal Powder Using Infrared Camera10.4028/www.scientific.net/MSF.834.93 ↗
12. Homogenization kinetics of a nickel-based superalloy produced by powder bed fusion laser sintering10.1016/j.scriptamat.2016.12.037 ↗
13. High Strength and Ductility of Additively Manufactured 316L Stainless Steel Explained
14. Y. Wang, C. Zhang, C. Yu, L. Xing, K. Li, J. Chen, J. Ma, W. Liu, Z. Shen, Construction of Cellular Substructure in Selective Laser Melting, (2019). https://doi.org/10.20944/preprints201910.0065.v1.10.20944/preprints201910.0065.v1 ↗
15. Study of the Microstructure and Cracking Mechanisms of Hastelloy X Produced by Laser Powder Bed Fusion10.3390/ma11010106 ↗
16. Microstructure and mechanical characterisation of SLM processed Haynes® 230®
17. Effect of post heat-treatment on the microstructure and mechanical properties of Hastelloy-X structures manufactured by laser based Directed Energy Deposition10.1016/j.jallcom.2019.05.050 ↗
18. Anomalous deformation behavior and twin formation of Ni-base superalloys at the intermediate temperatures10.1016/j.msea.2011.05.083 ↗
19. Y.M. Wang, T. Voisin, J.T. Mckeown, J. Ye, N.P. Calta, Z. Li, Z. Zeng, Y. Zhang, W. Chen, T.T. Roehling, R.T. Ott, M.K. Santala, P.J. Depond, M.J. Matthews, A. V Hamza, T. Zhu, Additively manufactured hierarchical stainless steels with high strength and ductility, (2017). https://doi.org/10.1038/NMAT5021.10.1038/nmat5021 ↗
20. Hierarchical structures of stainless steel 316L manufactured by Electron Beam Melting10.1016/j.addma.2017.07.003 ↗
21. Unexpected δ-Phase Formation in Additive-Manufactured Ni-Based Superalloy10.1007/s11837-015-1772-2 ↗
22. E.A. Ja¨gle, J. Ja¨gle, Z. Sheng, L. Wu, L. Lu, J. Risse, A. Weisheit, D. Raabe, Precipitation Reactions in Age-Hardenable Alloys During Laser Additive Manufacturing, (n.d.). 2021 https://doi.org/10.1007/s11837-015-1764-2.10.1007/s11837-015-1764-2 ↗
23. D. Deng, Additively Manufactured INCONEL 718: Microstructures and Mechanical Properties, 2018. https://doi.org/10.3384/lic.diva-144491.10.3384/lic.diva-144491 ↗
24. Powder bed binder jet 3D printing of Inconel 718: Densification, microstructural evolution and challenges☆10.1016/j.cossms.2016.12.002 ↗
25. Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting10.1016/j.actamat.2011.12.032 ↗
26. Microstructure and mechanical behavior of direct metal laser sintered Inconel alloy 71810.1016/j.matchar.2016.01.003 ↗
27. Microstructure of Selective Laser Melted Alloy 718 in As-Manufactured and Post Heat Treated Condition
28. Texture and microstructural features at different length scales in Inconel 718 produced by selective laser melting
29. Microstructure and mechanical properties of Inconel 625 superalloy10.1016/S0022-3115(00)00723-6 ↗
30. Predicting Precipitation Kinetics During the Annealing of Additive Manufactured Inconel 625 Components10.1007/s40192-019-00134-7 ↗
31. Characterization and Comparison of Inconel 625 Processed by Selective Laser Melting and Laser Metal Deposition10.1002/adem.201600635 ↗
32. Additive manufacturing of high-strength crack-free Ni-based Hastelloy X superalloy10.1016/j.addma.2019.100919 ↗
33. Microscopic investigation of as built and hot isostatic pressed Hastelloy X processed by Selective Laser Melting10.1016/j.matchar.2019.05.024 ↗
34. Boundary liquation and interface cracking characterization in laser deposition of Inconel 738 on directionally solidified Ni-based superalloy10.1016/j.scriptamat.2005.03.047 ↗
35. Study of the fusion zone and heat-affected zone microstructures in tungsten inert gas-welded INCONEL 738LC superalloy10.1007/s11661-006-0013-2 ↗
36. Atomic imaging of the interface between M 23 C 6 -type carbide and matrix in a long-term ageing polycrystalline Ni-based superalloy10.1080/09500839.2015.1039621 ↗
37. Microstructure and yield strength of SLM-fabricated CM247LC Ni-Superalloy10.1016/j.actamat.2017.02.007 ↗
38. Microstructure of selective laser melted CM247LC nickel-based superalloy and its evolution through heat treatment10.1016/j.matchar.2016.02.004 ↗
39. Formation of topologically closed packed phases within CMSX-4 single crystals produced by additive manufacturing
40. Microstructures of Rene 142 nickel-based superalloy fabricated by electron beam melting10.1016/j.actamat.2013.04.002 ↗
41. Cracking behavior and control of Rene 104 superalloy produced by direct laser fabrication10.1016/j.jmatprotec.2015.06.002 ↗
42. T.G. Gallmeyer, S. Moorthy, B.B. Kappes, M.J. Mills, B. Amin-Ahmadi, A.P. Stebner, Knowledge of Process-Structure-Property Relationships to Engineer Better Heat Treatments for Laser Powder Bed Fusion Additive Manufactured Inconel 718, 2021 n.d.10.1016/j.addma.2019.100977 ↗
43. The effect of interdendritic δ phase on the mechanical properties of Alloy 718 built up by additive manufacturing10.1016/j.matdes.2016.12.026 ↗
44. Veverkova · HIGH TEMPERATURE MICROSTRUCTURAL DEGRADATION OF HAYNES ALLOY · 2008 · 230
45. Creep deformation and mechanisms in Haynes 230 at 800°C and 900°C10.1016/j.jnucmat.2013.08.009 ↗
46. Carbide reactions (M 3 C→M 7 C 3 →M 23 C 6 →M 6 C) during tempering of rapidly solidified high carbon Cr-W and Cr-Mo steels10.1007/BF02661203 ↗
47. The shape and mechanism of formation of M23C6 carbide in austenite10.1016/0001-6160(67)90159-9 ↗
48. Precipitation of M23C6 in austenitic steels10.1016/0001-6160(65)90053-2 ↗
49. Formation of M23C6-type precipitates and chromium-depleted zones in austenite stainless steel10.1016/j.scriptamat.2011.06.010 ↗
50. M23C6 precipitation behavior and grain boundary serration in Ni-based Alloy 69010.1016/j.matchar.2014.07.008 ↗
51. Characterization of M23C6 carbide precipitated at grain boundaries in a superalloy10.1016/0026-0800(89)90021-9 ↗
52. Mechanism of primary MC carbide decomposition in Ni-base superalloys
53. Effects of Solution Heat Treatment on Carbide of Ni-Cr-W Superalloy10.1016/S1875-5372(10)60112-9 ↗
54. Singh Handa · Precipitation of Carbides in a Ni-based Superalloy · 2014
55. Dissociation of Cr-rich M23C6 carbide in Alloy 617 by severe plastic deformation10.1016/j.jnucmat.2010.09.027 ↗
56. The metallurgy and processing science of metal additive manufacturing10.1080/09506608.2015.1116649 ↗
57. Formation of metastable cellular microstructures in selective laser melted alloys10.1016/j.jallcom.2016.12.209 ↗
58. Intrinsic strain aging, Σ3 boundaries, and origins of cellular substructure in additively manufactured 316L10.1016/j.addma.2019.100784 ↗
59. Tensile deformation behavior of a nickel based superalloy at different temperatures10.1016/j.msea.2014.01.056 ↗
60. Solute partitioning on solidification of nickel-base ternary alloys10.1007/BF00580130 ↗
61. Carbide precipitation characteristics in additive manufacturing of Co-Cr-Mo alloy via selective election beam melting10.1016/j.scriptamat.2017.09.022 ↗
62. X-Ray Diffraction Characterization of Residual Stresses Produced By Shot Peening
63. S. Chatterjee, Mechanical behavior of alloy 230 at temperatures relevant to NGNP program, 2010.
64. The thermal fatigue behavior of the combustor alloys in 617 and HAYNES 230 before and after welding10.1007/s11661-999-0151-4 ↗
65. Tailoring the strength and ductility of T91 steel by partial tempering treatment10.1016/j.actamat.2019.02.043 ↗
66. Elastic constants of monocrystal iron from
67. Hall-Petch relationship in a nanotwinned nickel alloy10.1016/j.scriptamat.2008.01.025 ↗
68. Modeling solid solution strengthening in nickel alloys10.1007/s11661-997-0268-2 ↗
69. A. Thesis, O. Anderoglu, Residual Stress Measurement Using X-Ray Diffraction Residual Stress Measurement Using X-Ray Diffraction, (2004).
70. Lattice strains and diffraction elastic constants of cubic polycrystals10.1016/j.jmps.2020.103899 ↗
71. Contrasting mechanical behavior in precipitation hardenable AlXCoCrFeNi high entropy alloy microstructures: Single phase FCC vs. dual phase FCC-BCC10.1016/j.msea.2018.10.021 ↗
72. Strengthening via deformation twinning in a nickel alloy10.1016/j.msea.2007.06.072 ↗
73. Strengthening mechanisms and deformability of nanotwinned AlMg alloys10.1557/jmr.2018.372 ↗
74. High strength, epitaxial nanotwinned Ag films10.1016/j.actamat.2010.09.011 ↗
75. Revealing the maximum strength in nanotwinned copper10.1126/science.1167641 ↗
76. In-situ studies on the mechanical properties of He ion irradiated nanotwinned Ag10.1016/j.jnucmat.2020.152392 ↗
77. Microstructural evolution of nanotwinned Al-Zr alloy with significant 9R phase10.1080/21663831.2020.1840451 ↗
78. Deformation behavior and phase transformation of nanotwinned Al/Ti multilayers10.1016/j.apsusc.2020.146776 ↗
79. High strength, deformable nanotwinned Al–Co alloys10.1080/21663831.2018.1552211 ↗
80. Scripta Materialia Work hardening discrepancy designing to strengthening gradient nanotwinned Cu10.1016/j.scriptamat.2021.113975 ↗
81. High temperature thermal and mechanical stability of high-strength nanotwinned Al alloys10.1016/j.actamat.2018.11.011 ↗