Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti34Nb via laser powder bed fusion
Source abstract
Abstract
Abstract A parametric experimental study on the role played by the power (P), velocity (VL) and profile (top-hat or Gaussian) of the laser on the porosity, inclusion content and microstructural evolution of in-situ alloyed laser powder bed fusion (LPBF) manufactured Ti34Nb was conducted. For this, alloys were printed with three sets of processing parameters, in which the above-mentioned parameters were varied but the energy density was held constant. A detailed tomographic and microstructural investigation of these alloys was followed by tensile tests. Observations of melt pools in the single tracks and single stripes were complemented by thermal finite element method (FEM) simulations that studied their evolution. Results show that a top-hat laser profile combined with high P (> 650 W), high VL (> 650 mm/s) and short stripe width scanning strategy forms a large single stripe melt pool that moves slowly and has a low aspect ratio. The large and slow melt pool allows Nb to melt efficiently and minimizes its unmelted content while the low melt pool aspect ratio prevents keyholing that can otherwise result in porosity. These melt pool attributes also favor the formation of a columnar β-Ti microstructure with a strong {100} texture, which has the ideal combination of strength and elastic modulus. The mechanisms of microstructural evolution were explained and the scope of this parameter optimization principle was discussed in the context of further improving the properties of this alloy.
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Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · High Entropy Alloys Studies · Titanium Alloys Microstructure and Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (54)
Show source-provided references
1. Problem of stress shielding and improvement to the hip implant designs: a review10.3923/jms.2007.460.467 ↗
2. Das gesetz der transformation der knochen
3. Recent metallic materials for biomedical applications10.1007/s11661-002-0109-2 ↗
4. Implications of metallic corrosion in total knee arthroplasty
5. Effect of stress-induced α″ martensite on Young's modulus of β Ti–33.6Nb–4Sn alloy10.1016/j.msea.2013.09.053 ↗
6. Design and fabrication of a metastable β-type titanium alloy with ultralow elastic modulus and high strength10.1038/srep14688 ↗
7. New developments of Ti-based alloys for biomedical applications10.3390/ma7031709 ↗
8. Micro-and meso-structures and their influence on mechanical properties of selectively laser melted Ti-6Al-4V10.1016/j.actamat.2018.05.044 ↗
9. Microstructural optimization through heat treatment for enhancing the fracture toughness and fatigue crack growth resistance of selective laser melted Ti6Al4V alloy10.1016/j.actamat.2019.03.003 ↗
10. High cycle fatigue in selective laser melted Ti-6Al-4V10.1016/j.actamat.2020.05.041 ↗
11. Recent advances on high‐entropy alloys for 3D printing10.1002/adma.201903855 ↗
12. Simultaneous enhancements of strength and toughness in an Al-12Si alloy synthesized using selective laser melting10.1016/j.actamat.2016.06.009 ↗
13. Effect of defocusing distance on laser powder bed fusion of high strength Al–Cu–Mg–Mn alloy
14. Laser additive manufacturing of Mg-based composite with improved degradation behaviour
15. Selective laser melting of Ti42Nb composite powder and the effect of laser re-melting10.4028/www.scientific.net/KEM.801.270 ↗
16. Selective laser melting of titanium alloy with 50 wt% tantalum: effect of laser process parameters on part quality10.1016/j.ijrmhm.2018.08.006 ↗
17. Selective laser melting of lattice structures: a statistical approach to manufacturability and mechanical behavior10.1016/j.rcim.2017.06.006 ↗
18. Selective laser melting of titanium alloy with 50 wt% tantalum: microstructure and mechanical properties10.1016/j.jallcom.2015.11.141 ↗
19. In situ alloying of elemental Al-Cu12 feedstock using selective laser melting10.1080/17452759.2019.1584402 ↗
20. Controlling the microstructure and mechanical properties of a metastable β titanium alloy by selective laser melting10.1016/j.msea.2018.04.087 ↗
21. In situ elaboration of a binary Ti–26Nb alloy by selective laser melting of elemental titanium and niobium mixed powders10.1016/j.msec.2016.02.033 ↗
22. Remelt processing and microstructure of selective laser melted Ti25Ta10.1016/j.jallcom.2019.153082 ↗
23. Observation of keyhole-mode laser melting in laser powder-bed fusion additive manufacturing10.1016/j.jmatprotec.2014.06.005 ↗
24. New aspects about the search for the most relevant parameters optimizing SLM materials10.1016/j.addma.2018.11.023 ↗
25. - Thermal Stresses in Materials Due to Laser Heating,
26. Identification of a suitable volumetric heat source for modelling of selective laser melting of Ti6Al4V powder using numerical and experimental validation approach10.1007/s00170-018-2631-4 ↗
27. Simulation of temperature distribution in single metallic powder layer for laser micro-sintering10.1016/j.commatsci.2011.09.012 ↗
28. Numerical investigation and an effective modelling on the selective laser melting (SLM) process with aluminium alloy 606110.1016/j.ijheatmasstransfer.2014.09.014 ↗
29. In situ synthesis of a binary Ti–10at% Nb alloy by electron beam melting using a mixture of elemental niobium and titanium powders10.1016/j.jmatprotec.2020.116646 ↗
30. Classification of defect types in SLM Ti-6Al-V4 by X-ray refraction topography10.1520/MPC20190080 ↗
31. Microstructure and mechanical properties of a novel β titanium metallic composite by selective laser melting10.1016/j.actamat.2014.01.018 ↗
32. The effect of grain size and stability on ambient temperature tensile and creep deformation in metastable beta titanium alloys10.1016/S1359-6454(02)00561-X ↗
33. Selective laser melting of Ti–35Nb composite from elemental powder mixture: Microstructure, mechanical behavior and corrosion behavior10.1016/j.msea.2019.06.001 ↗
34. Dynamics of pore formation during laser powder bed fusion additive manufacturing10.1038/s41467-019-10009-2 ↗
35. In situ fabrication of a titanium-niobium alloy with tailored microstructures, enhanced mechanical properties and biocompatibility by using selective laser melting
36. The formation of humps and ripples during selective laser melting of 316l stainless steel10.1007/s11837-019-03987-7 ↗
37. Physics of humping formation in laser powder bed fusion10.1016/j.ijheatmasstransfer.2019.119172 ↗
38. Simultaneously enhanced strength and ductility for 3D-printed stainless steel 316L by selective laser melting10.1038/s41427-018-0018-5 ↗
39. Elastic constants of single crystalline β-Ti70Nb3010.1016/j.scriptamat.2011.10.039 ↗
40. Martensitic transformation, shape memory effect and superelasticity of Ti–Nb binary alloys10.1016/j.actamat.2006.01.019 ↗
41. Tensile anisotropy associated microstructural and microtextural evolution in a metastable beta titanium alloy10.1016/j.msea.2019.01.053 ↗
42. Deformation behavior of age-hardened Ti-Mo alloys10.1016/0001-6160(74)90057-1 ↗
43. Selective laser melting of titanium alloy with 50 wt% tantalum: microstructure and mechanical properties10.1016/j.jallcom.2015.11.141 ↗
44. Laser powder bed fusion of titanium-tantalum alloys: compositions and designs for biomedical applications10.1016/j.jmbbm.2020.103775 ↗
45. Theory of microstructural development during rapid solidification10.1016/0001-6160(86)90056-8 ↗
46. Steady state columnar and equiaxed growth of dendrites and eutectic10.1016/0025-5416(84)90201-5 ↗
47. V. Fallah, Solidification in laser powder deposition of Ti-Nb alloys, ( 2011 ).10.1016/j.actamat.2011.12.009 ↗
48. On the origin of sliver defects in single crystal investment castings10.1016/j.actamat.2013.04.071 ↗
49. Origins of misorientation defects in single crystal castings: a time resolved in situ synchrotron X-ray radiography study, MATEC web of conferences
50. On the deformation of dendrites during directional solidification of a nickel-based superalloy10.1007/s11661-019-05429-0 ↗
51. Origin of small-angle grain boundaries during directional solidification in multicrystalline silicon10.1016/j.mtla.2018.08.034 ↗
52. Microstructure and mechanical properties of the near-beta titanium alloy Ti-5553 processed by selective laser melting10.1016/j.matdes.2016.04.103 ↗
53. Method and apparatus for producing a single-crystalline workpiece
54. Multi-scale microstructural investigation of a laser 3D printed Ni-based superalloy