journal article·2017-01Open access

Influence of Mg and Li content on the microstructure evolution of Al Cu Li alloys during long-term ageing

A. Deschamps, M. Garcia, J. Chevy, B. Davo, F. De Geuser

Acta Materialia· Volume 122

Abstract

The evolution of microstructure during long-term ageing (LTA) up to 3000 h at 85 °C following a T8 heat treatment has been characterised in three AlCuLiMg alloys of variable Mg and Li content. A combination of transmission electron microscopy, differential scanning calorimetry and small-angle X-ray scattering has been used to evaluate the evolution of the different phases. In the T8 condition all three alloys contain a high density of T1 precipitates together with S precipitates along the dislocations introduced by pre-stretching. In addition, the alloy with highest Li contains δ′ precipitates. During LTA this last alloy experiences a significant complementary precipitation of δ′. The two other alloys experience a much more limited microstructure evolution, which appears to be linked to the formation and subsequent evolution of metastable phases (GP and GPB zones) in the regions between T1 platelets. The evolution of the alloys' strength is shown to be well correlated to their microstructure.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Aluminum Alloy Microstructure Properties · Aluminum Alloys Composites Properties · Microstructure and mechanical properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (65)

Show source-provided references
1. Progress in structural materials for aerospace systems10.1016/j.actamat.2003.08.023 ↗
2. Recently-developed aluminium solutions for aerospace applications10.4028/www.scientific.net/MSF.519-521.1271 ↗
3. The evolution of Al-Li base products for aerospace and space applications10.1007/s11661-012-1155-z ↗
4. Recent developments in advanced aircraft aluminium alloys10.1016/j.matdes.2013.12.002 ↗
5. Application of modern aluminium alloys to aircraft10.1016/0376-0421(95)00004-6 ↗
6. The influence of Cu/Li ratio on precipitation in Al-Cu-Li-x alloys10.1016/j.actamat.2012.12.041 ↗
7. Microstructure distribution in an AA2050 T34 friction stir weld and its evolution during post-welding heat treatment10.1016/j.actamat.2015.08.068 ↗
8. Aluminum-copper-lithium alloy 2050 developed for medium to thick plate10.1007/s11665-009-9554-z ↗
9. Relations between microstructure, precipitation, age-formability and damage tolerance of Al-Cu-Mg-Li (Mn, Zr, Sc) alloys for age forming10.1016/j.msea.2005.11.023 ↗
10. Effect of ageing time on strength and microstructures of an Al-Cu-Li-Zn-Mg-Mn-Zr alloy10.1016/j.msea.2008.08.001 ↗
11. Microstructures and properties of 2099 Al-Li alloy10.1016/j.matchar.2013.07.015 ↗
12. Microscopy and microanalysis of complex nanosized strengthening precipitates in new generation commercial Al-Cu-Li alloys10.1111/jmi.12143 ↗
13. Ageing response of a Al-Cu-Li 2198 alloy10.1016/j.matdes.2014.04.063 ↗
14. Formation mechanism of precipitate T1 in AlCuLi alloys10.1016/j.jallcom.2014.10.208 ↗
15. Atomic structure and growth mechanism of T1 precipitate in Al-Cu-Li-Mg-Ag alloy10.1016/j.scriptamat.2015.07.020 ↗
16. Effect of age-forming on microstructure, mechanical and corrosion properties of a novel Al-Li alloy10.1016/j.jallcom.2015.03.212 ↗
17. Microstructure and mechanical properties of Mg, Ag and Zn multi-microalloyed Al-(3.2-3.8)Cu-(1.0-1.4)Li alloys10.1016/S1003-6326(15)63821-3 ↗
18. Microstructure, texture and hardness of Al-Cu-Li alloy sheet during hot gas forming with integrated heat treatment10.1016/j.matdes.2016.01.001 ↗
19. Quantification of the influence of increased pre-stretching on microstructure-strength relationships in the Al-Cu-Li alloy AA219510.1016/j.actamat.2016.02.017 ↗
20. Transmission electron microscopy in the early stages of precipitates in aged Al-Li-Cu alloys10.1016/S1359-6454(03)00104-6 ↗
21. Effect of silver on precipitation response of Al-Li-Cu-Mg alloys RID D-1730-200910.1179/174328408X262391 ↗
22. Refinement of the crystal structure of hexagonal Al2CuLi10.1016/S0022-4596(05)80086-6 ↗
23. Atomic structure of T-1 precipitates in Al-Li-Cu alloys revisited with HAADF-STEM imaging and small-angle X-ray scattering10.1016/j.actamat.2010.09.044 ↗
24. Combined electron beam imaging and ab initio modeling of T(1) precipitates in Al-Li-Cu alloys10.1063/1.3590171 ↗
25. The effect of plastic deformation on Al2CuLi (T1) precipitation10.1007/BF02656799 ↗
26. Microstructural evolution during aging of an Al_Cu_Li_Ag_Mg_Zr alloy10.1016/1359-6454(95)00319-3 ↗
27. The role of plastic deformation on the competitive microstructural evolution and mechanical properties of a novel Al-Cu-Li-X alloy10.1016/S1471-5317(00)00002-X ↗
28. Effect of cold compression on precipitation and conductivity of an Al-Li-Cu alloy10.1111/j.1365-2818.2008.02116.x ↗
29. Influence of natural ageing and deformation on precipitation in an Al–Cu–Li alloy10.1002/adem.201300098 ↗
30. Quantification and modelling of the microstructure/strength relationship by tailoring the morphological parameters of the T1 phase in an Al–Cu–Li alloy10.1016/j.actamat.2014.04.046 ↗
31. Effects of cold work on precipitation in Al-Cu-Mg-(Ag) and Al-Cu-Li-(Mg-Ag) alloys10.1007/BF02670753 ↗
32. Effects of a small addition of magnesium and silver on the precipitation of T1 phase in an Al—4%Cu—1.1%Li—0.2%Zr alloy10.1016/0921-5093(95)10157-8 ↗
33. Trace elements effects on precipitation processes and mechanical properties in an Al-Cu-Li alloy10.1007/s11661-997-0203-6 ↗
34. Independent and combined roles of trace Mg and Ag additions in properties precipitation process and precipitation kinetics of Al–Cu–Li–(Mg)–(Ag)–Zr–Ti alloys10.1016/S1359-6454(98)00079-2 ↗
35. Role of Ag and Mg on precipitation of T1 phase in an Al-Cu-Li-Mg-Ag alloy10.1016/S1359-6462(00)00651-5 ↗
36. The role of trace additions on the T1 coarsening behaviour in Al-Li-Cu-X alloys10.4028/www.scientific.net/MSF.396-402.699 ↗
37. Transmission electron microscopy study of the evolution of precipitates in aged Al–Li–Cu alloys: the θ′ and T1 phases10.1016/S1359-6454(03)00253-2 ↗
38. Precipitates and intermetallics phases in precipitation hardening Al-Cu-Mg-(Li) based alloys10.1179/174328005X14357 ↗
39. TEM diffraction study of Al2CuMg (S ′/S) precipitation in an Al-Li-Cu-Mg(Zr) alloy10.1080/14786435.2012.659288 ↗
40. Atom probe tomography and transmission electron microscopy characterisation of precipitation in an Al–Cu–Li–Mg–Ag alloy10.1016/j.ultramic.2010.12.004 ↗
41. Microstructural evolution during ageing of Al–Cu–Li–x alloys10.1016/j.actamat.2013.12.001 ↗
42. The influence of precipitation on plastic deformation of Al-Cu-Li alloys10.1016/j.actamat.2013.03.015 ↗
43. The effects of prolonged thermal exposure on the mechanical properties and fracture toughness of C458 aluminum-lithium alloy10.1016/j.engfailanal.2004.10.008 ↗
44. Low temperature thermal stability of quaternary Al-Li-Cu-Mg-alloys
45. Microstructural stability during low temperature exposure of alloys within the Al-Li-Cu-Mg system10.1016/j.msea.2007.10.020 ↗
46. A new method for evaluating the size of plate-like precipitates by small-angle scattering10.1107/S0021889812039891 ↗
47. Quantitative characterization of precipitate microstructures in metallic alloys using small-angle scattering10.1007/s11661-012-1435-7 ↗
48. Interactions between zirconium and manganese dispersoid-forming elements on their combined addition in Al–Cu–Li alloys10.1016/j.actamat.2012.06.012 ↗
49. Kinetics of solid-state reactions in Al-Li-Cu-Mg-Zr alloys from calorimetric studies10.1007/s11661-007-9250-2 ↗
50. Calorimetric studies of 8090 and 1441 Al–Li–Cu–Mg–Zr alloys of conventional and retrogressed and reaged tempers10.1007/s10853-006-0619-1 ↗
51. Quantitative description of the T1 formation kinetics in an Al–Cu–Li alloy using differential scanning calorimetry, small-angle X-ray scattering and transmission electron microscopy10.1080/14786435.2013.878047 ↗
52. Relations between microstructure, precipitation, age-formability and damage tolerance of Al-Cu-Mg-Li (Mn, Zr, Sc) alloys for age forming10.1016/j.msea.2005.11.023 ↗
53. Quantitative investigation of precipitation and mechanical behaviour for AA2024 friction stir welds10.1016/j.actamat.2005.02.007 ↗
54. The thermodynamics of and strengthening due to co-clusters: general theory and application to the case of Al-Cu-Mg alloys10.1016/j.actamat.2009.01.021 ↗
55. In-situ and simultaneous synchrotron-radiation small-angle and 100 scattering experiments on the low-temperature structure in As-quenched Al-Li alloy during heating10.1016/S1359-6462(97)00327-8 ↗
56. Nature of an endothermic peak of As-quenched Al-11.8 mol%Li alloys10.2320/matertrans1989.39.62 ↗
57. Experimental and modelling assessment of precipitation kinetics in an Al–Li–Mg alloy10.1016/j.actamat.2012.01.010 ↗
58. Microstructure mapping of a friction stir welded AA2050 Al–Li–Cu in the T8 state10.1080/14786435.2014.887862 ↗
59. On the validity of simple precipitate size measurements by Small-Angle Scattering in metallic systems10.1107/S0021889811003049 ↗
60. Comparative study on local and global mechanical properties of 2024 T351, 2024 T6 and 5251 0 friction stir welds10.1016/j.msea.2005.09.032 ↗
61. Cluster variation method calculation of the metastable aluminum lithium phase-diagram
62. On the [alpha](Al)/[delta]'(Al3Li) metastable solvus in aluminium-lithium alloys10.1016/S1359-6454(98)00263-8 ↗
63. In situ evaluation of the microstructure evolution during rapid hardening of an Al-2.5Cu-1.5Mg (wt.%) alloy10.1016/j.actamat.2011.01.027 ↗
64. Quantitative investigation of precipitation and mechanical behaviour for AA2024 friction stir welds10.1016/j.actamat.2005.02.007 ↗
65. The effect of minor solute additions on the precipitation path of an AlCuLi alloy10.1016/j.actamat.2016.05.050 ↗