Synthesis of thoria nano-particles at low temperature through base electrogeneration on steel 316L surface: Effect of current density
Source abstract
Abstract
Abstract The strategy developed in this study, offers significant advantages (simplicity and cleanness of method and also a product purity and new morphology of the product) over the conventional routes for the synthesis of ThO2 nanostructure. The effect of current density on morphology was studied. The synthesized powder was characterized by means of Powder X-ray Diffraction (PXRD), Transmission Electron Microscopy (TEM, Phillips EM 2085) Brunauer-Emmett-Teller (BET) and Fourier Transform Infrared (FT-IR) spectroscopy. The results show that the current density has a great effect on the morphology of the samples. The average size of the particles decreases as the applied current density increases and the average size of the samples decreases from 50 to 15 nm when the current density increases from 2 to 5 mA cm−2.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Electrocatalysts for Energy Conversion · Electrophoretic Deposition in Materials Science · Advanced battery technologies research
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (38)
Show source-provided references
1. Yousefi · Prog. Nucl. Energ · 2015 · 85 · 63110.1016/j.pnucene.2015.08.006 ↗
2. Yousefi · Process. Saf. Environ. · 2015 · 98 · 21110.1016/j.psep.2015.07.011 ↗
3. Nenoff · J. Nucl. Mater. · 2013 · 442 · 16210.1016/j.jnucmat.2013.08.027 ↗
4. Nenoff · Chem. Mater. · 2011 · 23 · 518510.1021/cm2020669 ↗
5. Lombardi · Prog. Nucl. Energ · 2001 · 38 · 39510.1016/S0149-1970(00)00143-8 ↗
6. Hubert · J. Nucl. Mater · 2001 · 297 · 20610.1016/S0022-3115(01)00604-3 ↗
7. Shi · Top. Catal. · 2002 · 18 · 25910.1023/A:1013846823785 ↗
8. Purohit · J. Nucl. Mater · 2003 · 323 · 3610.1016/j.jnucmat.2003.08.036 ↗
9. Anantharaman · J. Nucl. Mater · 2008 · 383 · 11910.1016/j.jnucmat.2008.08.042 ↗
10. Emsley · 2001 · 441
11. Schade · Int. J. Refract. Met. H. · 2010 · 28 · 64810.1016/j.ijrmhm.2010.05.003 ↗
12. Marques · J. Am. Ceram. Soc. · 1991 · 74 · 59810.1111/j.1151-2916.1991.tb04066.x ↗
13. Jing Li,Yan Chen and Yong Cai Zhang, 2nd International Conference on Electronic & Mechanical Engineering and Information Technology (EMEIT-2012). Page: 1365–1368.
14. Ananthasivan · J. Nucl. Mater · 2013 · 434 · 22310.1016/j.jnucmat.2012.11.040 ↗
15. A contribution to the Ru – Sn system10.1016/S0022-3115(02)01155-8 ↗
16. Preparation of high-density oxide and vibratory compaction in fuel tubes
17. Balakrishna · Nat. Sci. · 2012 · 4 · 943
18. Mohseni · Int. J. Chem., Mol. Nucl. Mater. Metall. Eng. · 2015 · 9( · 967
19. Shen · Adv. Funct. Mater · 2010 · 20 · 370810.1002/adfm.201001264 ↗
20. Fabert · Prog. Nucl. Energ · 2014 · 72( · 4410.1016/j.pnucene.2013.10.009 ↗
21. Ananthasivan · J. Nucl. Mater · 2002 · 306 · 110.1016/S0022-3115(02)01229-1 ↗
22. Grabs · Cryst. Growth Des. · 2012 · 12 · 146910.1021/cg201563h ↗
23. Zhugea · Mater. Let. · 2003 · 57 · 277610.1016/S0167-577X(02)01373-3 ↗
24. Joseph · J. Nucl. Mater · 2000 · 281 · 12910.1016/S0022-3115(00)00241-5 ↗
25. Ohga · Prog. Nucl. Energ · 2007 · 49 · 54610.1016/j.pnucene.2007.08.008 ↗
26. Yousefi · Curr. Appl. Phys. · 2012 · 12 · 19310.1016/j.cap.2011.05.038 ↗
27. Yousefi · J. Solid State Chem. · 2012 · 190 · 20210.1016/j.jssc.2012.01.062 ↗
28. Yousefi · Prog. Nucl. Energy · 2015 · 85 · 60010.1016/j.pnucene.2015.08.002 ↗
29. Gupta · Mater. Res. Bull. · 2014 · 49 · 29710.1016/j.materresbull.2013.09.010 ↗
30. Tok · J. Mater. Process. Tech. · 2007 · 190 · 21710.1016/j.jmatprotec.2007.02.042 ↗
31. Safwat, Mahmoud · Solid State Sci. · 2002 · 4 · 22110.1016/S1293-2558(01)01229-8 ↗
32. Nguyen · J. Phys. Chem. B · 2011 · 115 · 1216010.1021/jp2068304 ↗
33. Fan · Nat. Mater. · 2008 · 7 · 98410.1038/nmat2302 ↗
34. Yousefi · Curr. Appl. Phys. · 2012 · 12 · 54410.1016/j.cap.2011.08.018 ↗
35. Yousefi · Mat. Sci. Semicon. Proc. · 2013 · 16 · 86810.1016/j.mssp.2013.01.012 ↗
36. Yousefi · J. Taiwan Inst. Chem. E · 2012 · 43 · 61410.1016/j.jtice.2012.01.003 ↗
37. Zhitomirsky · Adv. Colloid. Interfac. · 2002 · 97 · 27910.1016/S0001-8686(01)00068-9 ↗
38. Zhitomirsky · Am. Ceram. Soc. Bul. · 2000 · 79 · 57