journal article·2007-07

Microstructural and mechanical property changes in the Ta-base T-111 alloy following thermal aging

Keith J. Leonard, Jeremy T. Busby, Steven J. Zinkle

Journal of Nuclear Materials· Volume 366· Issue 3
Publisher page

Abstract

Abstract The microstructural changes occurring in the Ta-base T-111 (Ta–8W–2Hf) alloy during 1100 h thermal aging at 1098, 1248 and 1398 K under inert atmosphere and the influence on mechanical properties are reported. Electrical resistivity, hardness and tensile properties are compared between the as-annealed and aged conditions. Microstructural evaluations were performed by optical, scanning electron microscopy and transmission electron microscopy. An increase in the amount of grain boundary precipitation with increasing aging temperature was found to decrease the electrical resistivity and material strength. Precipitation at the grain boundaries was found to be a mixture of monoclinic and cubic structures, suggesting the development of mixed Hf oxides, carbides and nitrides. Precipitate development caused pronounced embrittlement of the alloy following aging at 1398 K.
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Research context

OpenAlex topics: Metal and Thin Film Mechanics · Advanced materials and composites · Advanced Materials Characterization Techniques

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