journal article·2022-04Open access

Unveiling microstructure-property correlations in nuclear materials with high-energy synchrotron X-ray techniques

Xuan Zhang

Abstract

Understanding the microstructure-property correlation is critical for the performance evaluation of in-service materials and the development of advanced materials for nuclear reactor applications. Experimental studies are challenging for nuclear materials which are often hazardous. Recent developments in high-energy synchrotron X-ray (HEX) techniques offer the potential to address this challenge, by providing direct observations of internal responses to external stimuli in bulk-like materials, through in situ or 3D measurements. In this review, developments in HEX techniques are introduced and recent applications in nuclear materials are presented. The results offer unprecedented insights into materials performance and provide unique input to computational models.
Source: expertdata · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Nuclear Materials and Properties · Nuclear Physics and Applications · X-ray Diffraction in Crystallography

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (52)

Show source-provided references
1. Materials challenges in nuclear energy10.1016/j.actamat.2012.11.004 ↗
2. Small-scale mechanical testing on nuclear materials: bridging the experimental length-scale gap10.1016/j.scriptamat.2017.04.026 ↗
3. Prasitthipayong · 2017
4. iRadMat: a thermo-mechanical testing system for in situ high-energy X-ray characterization of radioactive specimens10.1063/1.4974246 ↗
5. Infrastructure development for radioactive materials at the NSLS-II10.1016/j.nima.2017.10.053 ↗
6. Characterization of radioactive materials using the MARS beamline at the synchrotron SOLEIL10.1016/j.jnucmat.2011.08.017 ↗
7. Nuclear Science User Facilities. https://nsuf.inl.gov/).
8. Tuszynski · 2021
9. High-energy synchrotron x-ray study of deformation-induced martensitic transformation in a neutron-irradiated Type 316 stainless steel10.1016/j.actamat.2020.08.057 ↗
10. Investigation of deformation and microstructural evolution in Grade 91 ferritic–martensitic steel by in situ high-energy X-rays10.1016/j.actamat.2013.10.003 ↗
11. Structural characterization of nanoscale intermetallic precipitates in highly neutron irradiated reactor pressure vessel steels10.1016/j.scriptamat.2015.10.019 ↗
12. In situ high-energy X-ray diffraction study of tensile deformation of neutron-irradiated polycrystalline Fe-9%Cr alloy10.1016/j.actamat.2016.12.038 ↗
13. In-situ high-energy X-ray characterization of neutron irradiated HT-UPS stainless steel under tensile deformation10.1016/j.actamat.2018.07.008 ↗
14. X-ray characterization of anisotropic defect formation in SiC under irradiation with applied stress10.1016/j.scriptamat.2021.113785 ↗
15. 120GeV neutrino physics graphite target damage assessment using electron microscopy and high-energy x-ray diffraction10.1103/PhysRevAccelBeams.22.041001 ↗
16. In-situ synchrotron X-ray study of microstructural evolution during creep deformation in Grade 91 steel10.1016/j.msea.2018.09.033 ↗
17. In situ synchrotron analysis of phase transformation at high temperatures in ODS ferritic steel10.1007/s10853-020-04360-9 ↗
18. Strain evolution in Zr-2.5 wt% Nb observed with synchrotron X-ray diffraction10.1016/j.matchar.2018.09.022 ↗
19. Miao · 2021
20. In situ high-energy X-ray study of deformation mechanisms in additively manufactured 316L stainless steel10.1016/j.jnucmat.2021.152874 ↗
21. In situ X-ray characterization of uranium dioxide during flash sintering10.1016/j.mtla.2018.07.006 ↗
22. Sample environment for in situ synchrotron corrosion studies of materials in extreme environments10.1063/1.4964101 ↗
23. Characterization of Kanthal APMT and T91 oxidation at beyond design-basis accident temperatures10.1016/j.corsci.2020.108598 ↗
24. Lattice strain mapping of cracks and indentations in UO2 using synchrotron microdiffraction10.1016/j.jnucmat.2019.151943 ↗
25. Non-destructive characterization of engineering materials using high-energy X-rays at the advanced photon source10.1080/08940886.2017.1316125 ↗
26. Proton irradiated graphite grades for a long baseline neutrino facility experiment10.1103/PhysRevAccelBeams.20.071002 ↗
27. Characterization of neutron-irradiated HT-UPS steel by high-energy X-ray diffraction microscopy10.1016/j.jnucmat.2015.11.063 ↗
28. High-energy X-ray diffraction microscopy study of deformation microstructures in neutron-irradiated polycrystalline Fe-9%Cr10.1016/j.jnucmat.2018.06.004 ↗
29. Exploring new links between crystal plasticity models and high-energy X-ray diffraction microscopy10.1016/j.cossms.2019.07.002 ↗
30. High-energy X-ray diffraction microscopy in materials science10.1146/annurev-matsci-070616-124125 ↗
31. Multigrain crystallography and three-dimensional grain mapping
32. Materials discovery and design: by means of data science and optimal learning
33. Forward modeling method for microstructure reconstruction using X-ray diffraction microscopy: single-crystal verification10.1063/1.2400017 ↗
34. Study of 3-D stress development in parent and twin pairs of a hexagonal close-packed polycrystal: part I – in-situ three-dimensional synchrotron X-ray diffraction measurement10.1016/j.actamat.2015.04.020 ↗
35. Study of 3-D stress development in parent and twin pairs of a hexagonal close-packed polycrystal: part II – crystal plasticity finite element modeling10.1016/j.actamat.2015.04.025 ↗
36. Crystallographic character of grain boundaries resistant to hydrogen-assisted fracture in Ni-base alloy 72510.1038/s41467-018-05549-y ↗
37. Non-destructive characterization of UO2+x nuclear fuels10.1017/S155192951700102X ↗
38. Crystal plasticity model validation using combined high-energy Diffraction microscopy data for a Ti-7Al specimen10.1007/s11661-016-3868-x ↗
39. The application of synchrotron micro-computed tomography to characterize the three-dimensional microstructure in irradiated nuclear fuel10.1016/j.jnucmat.2020.152161 ↗
40. 4D synchrotron X-ray microtomography of fracture in nuclear graphite after neutron irradiation and radiolytic oxidation10.1016/j.carbon.2020.06.051 ↗
41. X-ray diffraction contrast tomography: a novel technique for three-dimensional grain mapping of polycrystals. II. The combined case10.1107/S0021889808001726 ↗
42. In situ synchrotron X-ray tomography of 304 stainless steels undergoing chlorine-induced stress corrosion cracking10.1016/j.corsci.2020.108687 ↗
43. X-Ray microcomputed tomography in additive manufacturing: a review of the current technology and applications10.1089/3dp.2018.0060 ↗
44. Creep behavior of 316L stainless steel manufactured by laser powder bed fusion10.1016/j.jnucmat.2021.152847 ↗
45. Damage evolution and failure mechanisms in additively manufactured stainless steel10.1016/j.msea.2015.10.073 ↗
46. Three-dimensional grain mapping by X-ray diffraction contrast tomography and the use of Friedel pairs in diffraction data analysis10.1063/1.3100200 ↗
47. Observations of intergranular stress corrosion cracking in a grain-mapped polycrystal10.1126/science.1156211 ↗
48. Study on the morphology of bulk hydrides by synchrotron X-ray tomography10.1016/j.matchar.2017.11.013 ↗
49. A rotational and axial motion system load frame insert for in situ high energy x-ray studies10.1063/1.4927855 ↗
50. X-ray characterization of the micromechanical response ahead of a propagating small fatigue crack in a Ni-based superalloy10.1016/j.actamat.2019.08.005 ↗
51. Starting a new era of nuclear innovation with Argonne's activated materials lab. https://www.ans.org/news/article-3176/starting-a-new-era-of-nuclear-innovation-with-argonnes-activated-materials-lab/, 2021).
52. High-fidelity geometry generation from CT data using convolutional neural networks