journal article·2022-11Open access

Creep behavior of an additively manufactured 9Cr steel in the as-built condition

Lizhen Tan, Weicheng Zhong, Ying Yang, Kevin G. Field, Niyanth Sridharan, Andrew T. Nelson

Abstract

Limited studies have evaluated the creep behavior of additively manufactured (AM) ferritic-martensitic (FM) steels. This work investigated the creep behavior of a 9Cr FM steel fabricated by powder blown directed energy deposition (DED) technique. The creep testing at 550–650 °C and 150 MPa for the specimens along the deposition direction in the as-built condition, together with corresponding microstructural characterization, revealed a threshold temperature between 600 and 625 °C, below which the steel has creep resistance comparable with Grade 91 cross-welds and noticeably greater than 9Cr-1Mo steel. The threshold temperature distinguishes the creep behavior in two regimes differentiated in creep activation energy, creep deformation, and failure mechanism. Unlike the creep rupture surface ∼45° from the loading direction when tested above the threshold temperature, the creep rupture for testing below the threshold temperature resembles type IV failure in the cross-welds of ferritic steels. The DED-induced layer structure in the as-built steel played a significant role on the change of creep behavior.
Source: expertdata · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Nuclear Materials and Properties · Fusion materials and technologies

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (40)

Show source-provided references
1. Corrosion and stress corrosion cracking in supercritical water10.1016/j.jnucmat.2007.05.017 ↗
2. Microstructure control for high strength 9Cr ferritic-martensitic steels10.1016/j.jnucmat.2011.12.011 ↗
3. Low-activation ferritic and martensitic steels for fusion application10.1016/S0022-3115(96)00327-3 ↗
4. Ferritic and tempered martensitic steels
5. Klueh · 2001
6. Re-evaluation of stress rupture factors for Grade 91 weldments based on the extended database with the data collected in Japan
7. Scientific, technological and economic issues in metal printing and their solutions10.1038/s41563-019-0408-2 ↗
8. Additive manufacturing of metals10.1016/j.actamat.2016.07.019 ↗
9. Additive manufacturing of metallic components – process, structure and properties10.1016/j.pmatsci.2017.10.001 ↗
10. Additive manufacturing of steels: a review of achievements and challenges10.1007/s10853-020-05109-0 ↗
11. Metal additive manufacturing: a review of mechanical properties10.1146/annurev-matsci-070115-032024 ↗
12. Microstructures and mechanical properties of a modified 9Cr ferritic-martensitic steel in the as-built condition after additive manufacturing10.1016/j.jnucmat.2020.152742 ↗
13. Williams · 2009
14. Atomic number and crystallographic contrast images with the SEM: a review of backscattered electron techniques10.1180/minmag.1987.051.359.02 ↗
15. Microstructure and mechanical properties of stainless steel CX manufactured by direct metal laser sintering10.1016/j.msea.2017.10.045 ↗
16. About the information depth of backscattered electron imaging10.1111/jmi.12542 ↗
17. Fiji: an open-source platform for biological-image analysis10.1038/nmeth.2019 ↗
18. Microstructure and mechanical properties of high Mn-containing ferritic-martensitic alloys exposed to cyclical thermal treatment10.1016/j.msea.2021.141143 ↗
19. Effect of prior austenite grain size refinement by thermal cycling on the microstructural features of as-quenched lath martensite10.1007/s11661-016-3525-4 ↗
20. The role of the austenite grain size in the martensitic transformation in low carbon steels10.1016/j.matdes.2019.107625 ↗
21. Round robin crystal orientation measurement using EBSD for damage assessment10.1299/mej.16-00077 ↗
22. Tensile deformation mechanism and micro-void nucleation of Ti-55531 alloy with bimodal microstructure10.1016/j.jmrt.2020.11.008 ↗
23. Stability of MX-type strengthening nanoprecipitates in ferritic steels under thermal aging, stress and ion irradiation10.1016/j.actamat.2014.03.015 ↗
24. Creep rupture behavior of welded Grade 91 steel10.1016/j.msea.2016.05.065 ↗
25. Sawada · 1997
26. Creep deformation behavior 9Cr-1Mo ferritic steel10.2355/isijinternational.41.Suppl_S73 ↗
27. Creep deformation in a modified 9Cr-1 Mo steel10.1179/026708303225009436 ↗
28. Modelling the effects of alloying elements on precipitation in ferritic steels10.1016/S0921-5093(02)00418-5 ↗
29. Interpretation of creep behaviour of a 9Cr–Mo–Nb–V–N (T91) steel using threshold stress concept10.1179/026708399101505428 ↗
30. Assessment of long-term creep rupture strength of T91 steel by multiregion rupture data analysis10.1115/1.4032647 ↗
31. Creep behavior of modified 9Cr–1Mo ferritic steel10.1016/j.jnucmat.2011.02.024 ↗
32. Diffusion behavior of creep-resistant steels
33. Transition from power-law to viscous creep behaviour of p-91 type heat-resistant steel10.1016/S0921-5093(97)00364-X ↗
34. A model based creep equation for 9Cr–1Mo–0.2V (P91 type) steel10.1179/174328407X161187 ↗
35. Review of type IV cracking of weldments in 9–12%Cr creep strength enhanced ferritic steels10.1179/1743280412Y.0000000016 ↗
36. Type IV cracking in ferritic power plant steels10.1179/174328406X148778 ↗
37. Identification of microstructural zones and thermal cycles in a weldment of modified 9Cr-1Mo steel10.1007/s10853-006-0704-5 ↗
38. Effect of heat treatment on precipitation kinetics in high-Cr ferritic steels10.2355/isijinternational.42.779 ↗
39. Neumann · 2009
40. Diffusion of vanadium in iron and in Fe-Cr alloys