journal article·2016-06

Microstructure of HIPed and SPSed 9Cr-ODS steel and its effect on helium bubble formation

Chenyang Lu, Zheng Lu, Rui Xie, Chunming Liu, Lumin Wang

Publisher page

Abstract

Abstract Two 9Cr-ODS steels with the same nominal composition were consolidated by hot isostatic pressing (HIP, named COS-1) and spark plasma sintering (SPS, named COS-2). Helium ions were implanted into COS-1, COS-2 and non-ODS Eurofer 97 steels up at 673 K. Microstructures before and after helium ion implantations were carefully characterized. The results show a bimodal grain size distribution in COS-2 and a more uniform grain size distribution in COS-1. Nanoscale clusters of GP-zone type Y–Ti–O and Y 2 Ti 2 O 7 pyrochlore as well as large spinel Mn(Ti)Cr 2 O 4 particles are all observed in the two ODS steels. The Y–Ti-enriched nano-oxides in COS-1 exhibit higher number density and smaller size than in COS-2. The Y–Ti-enriched nano-oxides in fine grains of COS-2 show higher number density and smaller size than that in coarse grains of COS-2. Nano-oxides effectively trap helium atoms and lead to the formation of high density and ultra-fine helium bubbles.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Fusion materials and technologies · Nuclear Materials and Properties · Nuclear materials and radiation effects

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (36)

Show source-provided references
1. Recent Developments in irradiation-resistant steels10.1146/annurev.matsci.38.060407.130315 ↗
2. Implications of fundamental radiation damage studies in the research and development of materials for a fusion reactor10.1016/S0022-3115(96)00486-2 ↗
3. Alloying design of oxide dispersion strengthened ferritic steel for long life FBRs core materials10.1016/0022-3115(93)90200-I ↗
4. Classical thermodynamic approach to void nucleation in irradiated materials10.1179/174892406X142714 ↗
5. Helium bubble distributions in a nanostructured ferritic alloy10.1016/j.jnucmat.2012.11.049 ↗
6. Helium entrapment in a nanostructured ferritic alloy10.1016/j.scriptamat.2011.07.024 ↗
7. Irradiation-tolerant nanostructured ferritic alloys: transforming helium from a liability to an asset10.1007/s11837-010-0144-1 ↗
8. A review of refractory metal alloys and mechanically alloyed-oxide dispersion strengthened steels for space nuclear power systems10.1016/j.jnucmat.2004.10.118 ↗
9. Microstructure refinement and strengthening mechanisms of a 12Cr ODS steel processed by equal channel angular extrusion10.1016/j.jallcom.2013.04.198 ↗
10. The effect of dual Fe+/He+ ion beam irradiation on microstructural changes in FeCrAl ODS alloys10.1016/j.jallcom.2012.11.113 ↗
11. Ion-irradiation effects on dissimilar friction stir welded joints between ODS alloy and ferritic stainless steel10.1016/j.jallcom.2013.11.123 ↗
12. Helium cavity formation research on oxide dispersed strengthening (ODS) ferritic steels utilizing dual-ion irradiation facility10.1016/j.fusengdes.2005.09.049 ↗
13. Evaluation of helium effects on swelling behavior of oxide dispersion strengthened ferritic steels under ion irradiation10.1016/j.jnucmat.2007.03.016 ↗
14. Microstructure of a 14Cr-ODS ferritic steel before and after helium ion implantation10.1016/j.jnucmat.2014.06.065 ↗
15. Helium solubility and bubble formation in a nanostructured ferritic alloy10.1016/j.jnucmat.2013.10.048 ↗
16. Comparisons of radiation damage in He ion and proton irradiated immiscible Ag/Ni nanolayers10.1016/j.jnucmat.2013.04.069 ↗
17. Radiation damage in helium ion irradiated nanocrystalline Fe10.1016/j.jnucmat.2011.10.052 ↗
18. Unusual size-dependent strengthening mechanisms in helium ion-irradiated immiscible coherent Cu/Co nanolayers10.1016/j.actamat.2014.10.061 ↗
19. Transmission electron microscopy characterization of the nanofeatures in nanostructured ferritic alloy MA95710.1016/j.actamat.2012.03.012 ↗
20. Pre- and post-deformation microstructures of oxide dispersion strengthened ferritic steels10.1016/j.jnucmat.2007.03.141 ↗
21. TEM characterization of structure and composition of nanosized ODS particles in reduced activation ferritic–martensitic steels10.1016/j.jnucmat.2004.04.083 ↗
22. Interfacial strained structure and orientation relationships of the nanosized oxide particles deduced from elasticity-driven morphologyin oxide dispersion strengthened materials10.1016/j.actamat.2011.09.042 ↗
23. Recent progress in developing and qualifying nanostructured ferritic alloys for advanced fission and fusion applications10.1007/s11837-014-1207-5 ↗
24. Morphology, structure, and chemistry of nanoclusters in a mechanically alloyed nanostructured ferritic steel10.1007/s10853-012-6249-x ↗
25. Atomic structure of nanoclusters in oxide-dispersion-strengthened steels10.1038/nmat3150 ↗
26. Effect of heat treatment on microstructure and hardness of Eurofer 97, Eurofer ODS and T92 steels10.1016/j.jnucmat.2008.12.152 ↗
27. A review of advantages of high-efficiency X-ray spectrum imaging for analysis of nanostructured ferritic alloys10.1016/j.jnucmat.2014.11.134 ↗
28. Core/shell structures of oxygen-rich nanofeatures in oxide-dispersion strengthened Fe–Cr alloys10.1063/1.3000965 ↗
29. New insights into the structure of ODS particles in the ODS-Eurofer alloy10.1016/j.jnucmat.2008.12.174 ↗
30. Formation mechanism and the role of nanoparticles in Fe–Cr ODS steels developed for radiation tolerance10.1103/PhysRevB.82.184103 ↗
31. High-temperature tensile properties of nano-oxide dispersion strengthened ferritic steels produced by mechanical alloying and spark plasma sintering10.1007/s11661-013-1719-6 ↗
32. Characteristic results and prospects of the 13Cr–1W–0.3Ti–0.3Y2O3 ODS steel10.1016/j.jnucmat.2008.12.167 ↗
33. Role of alloying elements in nanostructured ferritic steels10.1179/1743284710Y.0000000039 ↗
34. Analytical characterization of oxide dispersion strengthened steels for fusion reactors10.1179/1743284710Y.0000000013 ↗
35. Stability of non-stoichiometric clusters in the MA957 ODS ferritic alloy10.1016/j.jnucmat.2010.12.056 ↗
36. Trapping helium in Y2Ti2O7 compared to in matrix iron: a first principles study10.1063/1.4871282 ↗