journal article·2010-09

Formation of helium induced nanostructure ‘fuzz’ on various tungsten grades

M.J. Baldwin, R.P. Doerner

Journal of Nuclear Materials· Volume 404· Issue 3
Publisher page

Abstract

Abstract The response of a variety of W material grades to nanostructure ‘fuzz’ formation is explored. W targets are exposed to He or D 2 –0.2He plasmas in PISCES-B at 900–1320 K to below sputter threshold He + ions of energy 25–60 eV for up to 2.2 × 10 4 s. SEM and XPS reveal nanoscopic reorganization of the W surface to a layer of ‘fuzz’ of porosity ∼90% as determined by a ‘fuzz’ removal/weight loss method. The variability of ‘fuzz’ growth is examined at 1120 K for 1 h durations: SR, SC and doped W grades – La 2 O 3 (1% wt.), Re (5% and 10% wt.), and TiC (1.5% wt.) developed 2–3 μm thick ‘fuzz’ layers, while a VPS grade developed a layer 4 μm thick. An RC grade revealed additional ‘fuzz’ at deep (>100 μm) grain boundaries. However, heat treatment up to 1900 K produced reintegration of ‘fuzz’ with the bulk and He release at ∼1000 K and ∼1400–1800 K due to depopulation from vacancy complexes.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Fusion materials and technologies · Advanced materials and composites · Nuclear Materials and Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (32)

Show source-provided references
1. Brooks · Nucl. Fusion · 2009 · 49 · 03500710.1088/0029-5515/49/3/035007 ↗
2. Tokunaga · J. Nucl. Mater. · 2005 · 337–339 · 88710.1016/j.jnucmat.2004.10.137 ↗
3. Doerner · Nucl. Fusion · 2009 · 49 · 03500210.1088/0029-5515/49/3/035002 ↗
4. Keys · Phys. Rev. · 1968 · 176 · 85110.1103/PhysRev.176.851 ↗
5. Najmabadi · Fusion Eng. Des. · 2006 · 80 · 310.1016/j.fusengdes.2005.11.003 ↗
6. Noda · J. Nucl. Mater. · 1997 · 241–243 · 22710.1016/S0022-3115(96)00507-7 ↗
7. Nagata · J. Nucl. Mater. · 2002 · 307–311 · 151310.1016/S0022-3115(02)01269-2 ↗
8. Tokunaga · J. Nucl. Mater. · 2004 · 329–333 · 75710.1016/j.jnucmat.2004.04.178 ↗
9. Nishijima · J. Nucl. Mater. · 2003 · 313–316 · 9710.1016/S0022-3115(02)01368-5 ↗
10. Ye · J. Nucl. Mater. · 2003 · 313–316 · 7210.1016/S0022-3115(02)01349-1 ↗
11. Nishijima · J. Nucl. Mater. · 2004 · 329–333 · 102910.1016/j.jnucmat.2004.04.129 ↗
12. Tokunaga · J. Nucl. Mater. · 2003 · 313–316 · 9210.1016/S0022-3115(02)01362-4 ↗
13. Takamura · Plasma Fusion Res. · 2006 · 51 · 1
14. N. Yoshida, H. Iwakiri, Damage structure of tungsten under He particle loading, in: Proc. 1st Int. Symposium and 1st Korea–Japan Workshop on Edge Plasma and Surface Component Interactions in Steady State Magnetic Fusion Devices, Toki, Japan, 20–22 May 2007.
15. Baldwin · Nucl. Fusion · 2008 · 48 · 03500110.1088/0029-5515/48/3/035001 ↗
16. K. Tokunaga, M.J. Baldwin, R.P. Doerner, D. Nishijima, H. Kurishita, T. Fujiwara, K. Araki, Y. Miyamoto, N. Yoshida, N. Ohno, Y. Ueda, Nanoscopic morphology formation on tungsten induced by D–He mixture plasma exposure, in: 25th Symposium on Fusion Technology, Rostock, Germany, 15–19 September 2008.
17. Baldwin · J. Nucl. Mater. · 2009 · 390–391 · 88610.1016/j.jnucmat.2009.01.247 ↗
18. H Maier, H Greuner et al., personal communication.
19. C.D. Wagner, W.M. Riggs, L.E. Davis, J.F. Moulder, G.E. Mullenberg, Handbook of X-ray Photoelectron Spectroscopy, Published by Perkin-Elmer Corp., Eden Prairie, MN, USA, 1979.
20. W. Eckstein, IPP Report 9/17, 1998.
21. Miyamoto · Nucl. Fusion · 2009 · 49 · 06503510.1088/0029-5515/49/6/065035 ↗
22. Kurishita · Mater. Sci. Eng. A · 2008 · 477 · 16210.1016/j.msea.2007.05.009 ↗
23. N. Yoshida, in: Proc. 1st Int. Symposium and 1st Korea–Japan Workshop on Edge Plasma and Surface Component Interactions in Steady State Magnetic Fusion Devices, Toki, Japan, 20–22 May 2007.
24. Amano · J. Appl. Phys. · 1984 · 56 · 98310.1063/1.334039 ↗
25. Kajita · Nucl. Fusion · 2009 · 49 · 09500510.1088/0029-5515/49/9/095005 ↗
26. Nishijima · Nucl. Fusion · 2005 · 45 · 66910.1088/0029-5515/45/7/016 ↗
27. Bowden · Nature · 1969 · 222 · 97710.1038/222977b0 ↗
28. Lassner · 1999
29. Wilson · Phys. Rev. B. · 1981 · 24 · 561610.1103/PhysRevB.24.5616 ↗
30. Kornelsen · J. Nucl. Mater. · 1980 · 92 · 7910.1016/0022-3115(80)90144-0 ↗
31. Tokitani · J. Nucl. Mater. · 2005 · 337–339 · 93710.1016/j.jnucmat.2004.07.054 ↗
32. Zenobia · J. Nucl. Mater. · 2009 · 389 · 21310.1016/j.jnucmat.2009.02.004 ↗