journal article·2019-03Open access

Porosity Determination of Carbon and Glass Fibre Reinforced Polymers Using Phase-Contrast Imaging

Christian Gusenbauer, Michael Reiter, Bernhard Plank, Dietmar Salaberger, Sascha Senck, Johann Kastner

Abstract

This paper presents multi-modal image data of different fibre reinforced polymer samples acquired with a desktop Talbot-Lau grating interferometer (TLGI) X-ray computed tomography (XCT) system and compare the results with images acquired using conventional absorption-based XCT. Two different fibre reinforced polymer samples are investigated: (i) a carbon fibre reinforced polymer (CFRP) featuring a copper mesh embedded near the surface for lightning conduction and (ii) a short glass fibre reinforced polymer (GFRP) sample. The primary goal is the non-destructive detection of internal defects such as pores and the quantification of porosity. TLGI provides three imaging modalities including attenuation contrast (AC) due to absorption, differential phase contrast (DPC) due to refraction and dark-field contrast (DFC) due to scattering. In the case of the CFRP sample, DPC is less prone to metal streak artefacts improving the detection of pores that are located close to metal components. In addition, results of a metal artefact reduction (MAR) method, based on sinogram inpainting and an image fusion concept for AC, DPC and DPC, are presented. In the case of the GFRP sample, DPC between glass fibres and matrix is lower compared to AC while DPC shows an increased contrast between pores and its matrix. Porosity for the CFRP sample is determined by applying an appropriate global thresholding technique while an additional background removal is necessary for the GFRP sample.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Advanced X-ray Imaging Techniques · Advanced X-ray and CT Imaging · Medical Imaging Techniques and Applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (32)

Show source-provided references
1. David, C., Nöhammer, B., Solak, H.H., Ziegler, E.: Differential x-ray phase contrast imaging using a shearing interferometer. Appl. Phys. Lett. 81, 3287–3289 (2002)10.1063/1.1516611 ↗
2. Momose, A., Kawamoto, S., Koyama, I., Hamaishi, Y., Takai, K., Suzuki, Y.: Demonstration of X-ray talbot interferometry. Jpn. J. Appl. Phys. 42, 866–868 (2003)10.1143/JJAP.42.L866 ↗
3. Pfeiffer, F., Weitkamp, T., Bunk, O., David, C.: Phase retrieval and differential phase-contrast imaging with low-brilliance X-ray sources. Nat. Phys. 2, 258–261 (2006)10.1038/nphys265 ↗
4. Rutishauser, S., Bednarzik, M., Zanette, I., Weitkamp, T., Börner, M., Mohr, J., David, C.: Fabrication of two-dimensional hard X-ray diffraction gratings. Microelectron. Eng. 101, 12–16 (2013)10.1016/j.mee.2012.08.025 ↗
5. Fu, J., Hu, X., Velroyen, A., Bech, M., Jiang, M., Pfeiffer, F.: 3D algebraic iterative reconstruction for cone-beam x-ray differential phase-contrast computed tomography. PLoS One. 10(3), e0117502 (2015). https://doi.org/10.1371/journal.pone.011750210.1371/journal.pone.0117502 ↗
6. Scholkmann, F., Revol, V., Kaufmann, R., Baronowski, H., Kottler, C.: A new method for fusion, denoising and enhancement of x-ray images retrieved from Talbot-Lau grating interferometry. Phys. Med. Biol. 59, 1425–1440 (2014)10.1088/0031-9155/59/6/1425 ↗
7. Revol, V., Plank, B., Kaufmann, R., Kastner, J., Kottler, C., Neels, A.: Laminate fibre structure characterisation of carbon fibre-reinforced polymers by X-ray scatter dark field imaging with a grating interferometer. NDT&E Int. 58, 64–71 (2013)10.1016/j.ndteint.2013.04.012 ↗
8. Yang, F., Prade, F., Griffa, M., Jerjen, I., Di Bella, C., Herzen, J., Sarapata, A., Pfeiffer, F., Lura, P.: Dark-field X-ray imaging of unsaturated water transport in porous materials. Appl. Phys. Lett. 105, 154105 (2014)10.1063/1.4898783 ↗
9. Hannesschläger, C., Revol, V., Plank, B., Salaberger, D., Kastner, J.: Fibre structure characterisation of injection moulded short fibre-reinforced polymers by X-ray scatter dark field tomography. Case Stud. Nondestruct. Test. Eval. 3, 34–41 (2015)10.1016/j.csndt.2015.04.001 ↗
10. Gusenbauer, C., Leiss-Holzinger, E., Senck, S., Mathmann, K., Kastner, J., Hunger, S., Birkfellner, W.: Characterization of medical and biological samples with a Talbot-Lau grating interferometer µXCT in comparison to reference methods. Nondestruct. Test. Eval, Case Stud (2016). https://doi.org/10.1016/j.csndt.2016.02.00110.1016/j.csndt.2016.02.001 ↗
11. Revol, V., Jerjen, I., Kottler, C., Schütz, P., Kaufmann, R., Lüthi, T., Sennhauser, U., Straumann, U., Urban, C.: Sub-pixel porosity revealed by x-ray scatter dark field imaging. J. Appl. Phys. 110, 044912 (2011)10.1063/1.3624592 ↗
12. Lauridsen, T., Willner, M., Bech, M., Pfeiffer, F., Feidenhans, R.: Detection of sub-pixel fractures in X-ray dark-field tomography. Appl. Phys. A 121(3), 1243–1250 (2015)10.1007/s00339-015-9496-2 ↗
13. Bech, M., Bunk, O., Donath, T., Feidenhans’l, R., David, C., Pfeiffer, F.: Quantitative x-ray dark-field computed tomography. Phys. Med. Biol. 55(18), 5529–5539 (2010)10.1088/0031-9155/55/18/017 ↗
14. Prade, F., Schaff, F., Senck, S., Prade, F., Pfeiffer, F.: Nondestructive characterization of fiber orientation in short fiber reinforced polymer composites with X-ray vector radiography. NDT and E Int. 86, 65–72 (2017)10.1016/j.ndteint.2016.11.013 ↗
15. Malecki, A., Potdevin, G., Biernath, T., Eggl, E., Willer, K., Lasser, T., Maisenbacher, J., Gibmeier, J., Wanner, A., Pfeiffer, F.: X-ray tensor tomography. EPL 105, 38002 (2014)10.1209/0295-5075/105/38002 ↗
16. Gresil, M., Revol, V., Kitsianos, K., Kanderakis, G., Koulalis, I., Sauer, M., Trétout, H., Madrigal, A.: EVITA Project: comparison between traditional non-destructive techniques and phase contrast x-ray imaging applied to aerospace carbon fibre reinforced polymer. Appl. Compos. Mater. 24(2), 513–524 (2017)10.1007/s10443-016-9540-1 ↗
17. Stampanoni, M., Wang, Z., Thüring, T., David, C., Rössl, E., van Stevendaal, U., Köhler, T., Trippel, M., Singer, G., Kubik-Huch, R.A., Hohl, M.K., Hauser, N.: Toward clinical differential phase contrast mammography: preliminary evaluations and image processing schemes. J. Instrum. (2013). https://doi.org/10.1088/1748-0221/8/05/C0500910.1088/1748-0221/8/05/C05009 ↗
18. Kastner, J., Plank, B., Salaberger, D., Sekelja, J.: Defect and Porosity Determination of Fibre Reinforced Polymers by X-ray Computed Tomography, 2nd International Symposium on NDT in Aerospace, Hamburg, Germany, 2010
19. Gagné, M., Therriault, D.: Lightning strike protection of composites. Prog. Aerosp. Sci. 64, 1–16 (2014)10.1016/j.paerosci.2013.07.002 ↗
20. Talbot, H.F.: Phil. Mag. 3(9), 401–407 (1836)
21. Lau, E.: Annual Physics 437, 417–423 (1948)10.1002/andp.19484370709 ↗
22. Yashiro, W., Terui, Y., Kawabata, K., Momose, A.: On the origin of visibility contrast in x-ray Talbot interferometry. Opt. Express 18(16), 16890–16901 (2010)10.1364/OE.18.016890 ↗
23. Gusenbauer, C., Hunger, S., Senck, S., Kastner, J.: Characterization of Tooth Samples with a Talbot-Lau Grating Interferometer μXCT Desktop Device, Proceedings of 4th International Conference on Image Formation in X-Ray Computed Tomography, Bamberg, Germany (2016)
24. Gusenbauer, C., Reiter, M., Plank, B., Senck, S., Hannesschläger, C., Renner, S., Kaufmann, R., Kastner, J.: Multi-modal Talbot-Lau grating interferometer XCT data for the characterization of carbon fibre reinforced polymers with metal components, Proceedings of 7th Conference on Industrial Computed Tomography, Leuven, Belgium (2017)
25. Pfeiffer, F., Bech, M., Bunk, O., Kraft, P., Eikenberry, E.F., Brönnimann, C., Grünzweig, C., David, C.: Hard-X-ray dark-field imaging using a grating interferometer. Nat. Mater. 7, 134–137 (2008)10.1038/nmat2096 ↗
26. Kalender, W.A., Hebel, R., Ebersberger, J.: Reduction of CT artifacts caused by metallic implants. Radiology 164(2), 576–577 (1987)10.1148/radiology.164.2.3602406 ↗
27. Meyer, E., Raupach, R., Lell, M., Schmidt, B., Kachelrieß, M.: Normalized metal artifact reduction (NMAR) in computed tomography. Med. Phys. 37, 5482–5493 (2010)10.1118/1.3484090 ↗
28. Gusenbauer, C., Reiter, M., Salaberger, D., Kastner, J.: Comparison of Metal Artefact Reduction Algorithms from Medicine Applied to Industrial XCT Applications, Proceedings of 19th World Conference on Non-Destructive Testing 2016, Munich, Germany (2016)
29. Momose, A., Takeda, T., Itai, Y., Hirano, K.: Phase-contrast X-ray computed tomography for observing biological soft tissues. Nat. Med. 2(5), 596 (1996)10.1038/nm0596-596 ↗
30. Plank, B., Rao, G., Kastner, J.: Evaluation of CFRP-Reference Samples for Porosity made by Drilling and Comparison with Industrial Porosity Samples by Means of Quantitative X-ray Computed Tomography—Proceedings 7th International Symposium for NDT in Aerospace, pp. 10. Bremen, Deutschland (2015)
31. Fehringer, A., Mechlem, K., Epple, M., Allner, S., Hehn, L., Pfeiffer, F., Noël, P.B.: Ultra-fast cone-beam SIR on 2 k-cubed data, The 4th International Conference on Image Formation in X-Ray Computed Tomography, Bamberg, Germany (2016)
32. Kawakami, H., Feraboli, P.: Lightning strike damage resistance and tolerance of scarf-repaired mesh-protected carbon fiber composites. Composit. Part A 42, 1247–1262 (2011)10.1016/j.compositesa.2011.05.007 ↗