journal article·2012-05Open access

Three-dimensional reconstruction of aerogels from TEM images

Florence Despetis, Nadjette Bengourna, Berangere Lartigue, Sandra Spagnol, Nathalie Olivi-Tran

Journal of Non-Crystalline Solids· Volume 358· Issue 9

Abstract

The knowledge of the internal structure of porous materials is of main importance to compute their physical properties. This article focuses on base-catalyzed and colloidal silica aerogels, which are fractal materials and we use an original method for the reconstruction of these aerogels from TEM images. The method used is iterative and leads to the same fractal dimension as the real material, computed from the internal two-point correlation function. Unlike the reconstruction of porous materials found in literature, our method is based on the distribution of matter and not of the porous network, and has the additional advantage of being only half statistical, i.e. only the coordinates in the z direction are statistically obtained while the coordinates x and y of the elements of matter are accurately obtained from TEM images of our samples
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Aerogels and thermal insulation · Theoretical and Computational Physics · Mesoporous Materials and Catalysis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (17)

Show source-provided references
1. Spagnol · Europhys. Lett. · 2007 · 78 · 4600510.1209/0295-5075/78/46005 ↗
2. Cule · J. Appl. Phys. · 1999 · 86 · 342810.1063/1.371225 ↗
3. Yeong · Phys. Rev. E · 1998 · 58 · 22410.1103/PhysRevE.58.224 ↗
4. Yeong · Phys. Rev. E · 1998 · 57 · 49510.1103/PhysRevE.57.495 ↗
5. Levitz · J. Chem. Phys. · 1991 · 95 · 615110.1063/1.461583 ↗
6. Levitz · Adv. Colloid Interface Sci. · 1998 · 76–77 · 7110.1016/S0001-8686(98)00042-6 ↗
7. Manwart · Phys. Rev. E · 2000 · 62 · 89310.1103/PhysRevE.62.893 ↗
8. Bourgeois · Chem. Eng. Technol. · 2010 · 33 · 129010.1002/ceat.201000097 ↗
9. Politis · Microporous Mesoporous Mater. · 2008 · 110 · 9210.1016/j.micromeso.2007.09.024 ↗
10. Kolb · Phys. Rev. Lett. · 1983 · 51 · 112310.1103/PhysRevLett.51.1123 ↗
11. Meakin · Phys. Rev. Lett. · 1983 · 51 · 111910.1103/PhysRevLett.51.1119 ↗
12. C.J.Brinker and G.W.Scherer, Sol gel science: The Physics and Chemistry of Sol–Gel processing, Academic Press (1989) Elsevier Science (USA).
13. Levitz · Europhys. Lett. · 1997 · 39 · 59310.1209/epl/i1997-00394-5 ↗
14. Levitz · J. Phys. Chem. · 1993 · 97 · 381310.1021/j100117a030 ↗
15. Hasmy · J. Phys. Condens. Matter · 1998 · 10 · 494710.1088/0953-8984/10/23/003 ↗
16. Olivi-Tran · J. Phys. Condens. Matter · 1999 · 11 · 797110.1088/0953-8984/11/41/302 ↗
17. Hasmy · Phys. Rev. E · 1999 · 59 · 301210.1103/PhysRevE.59.3012 ↗