journal article·2017-12

Fabrication and optical characterizations of lead calcium titanate borosilicate glasses

Sangeeta Das, Abhishek Madheshiya, S.S. Gautam, C.R. Gautam

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Abstract

Abstract Different glass samples were prepared in the system 59[(Pb x Ca 1 − x )O·TiO 2 ]-40[2SiO 2 ·B 2 O 3 ]-1Fe 2 O 3 (0 ≤ x ≤ 0.7) employing a rapid melt-quenching technique. The IR structural and optical properties were evaluated using X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy and ultraviolet-visible (UV–VIS) spectroscopy. The amorphous nature of the glass samples were confirmed using XRD and SEM analysis. The Archimedes principle was used to calculate the density of all glass samples. The density increased with decrease in CaO content and the trend of molar volume reciprocal to the density. The band gap energy of the prepared glass samples are in the range of 1.25–2.37 eV and decrease with an increase in the concentrations of PbO.
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OpenAlex topics: Glass properties and applications · Luminescence Properties of Advanced Materials · Nuclear materials and radiation effects

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References (45)

Show source-provided references
1. Glass and glass-ceramics, functional material, preparation
2. Synthesis and structural properties of lead strontium titanate borosilicate glasses with addition of chromium trioxide and graphene nanoplatlets10.1080/00387010.2013.874531 ↗
3. Glasses as engineering materials: a review10.1016/j.matdes.2010.11.057 ↗
4. Agarwal, study of structural, optical and transport properties of semiconducting Fe2O3-PbO-B2O3 glasses
5. J. Kaewkhao, W. Siriprom, S. Insiripong, T. Ratana, C. Kedkaew, P. Limsuwan, Structural and magnetic properties of glass doped with iron oxide, 2nd Int. Symp. on Adv. Magn. Mater. Appl. (ISAMMA 2010), J. Phys. Conf. Ser. 266 (2011) 1–5.10.1088/1742-6596/266/1/012012 ↗
6. Electrical and spectroscopic properties of Fe2O3 doped Na2SO4-BaO-P2O5 glass system10.1016/j.jnoncrysol.2012.08.032 ↗
7. Structural and physical properties of Fe2O3-doped lead vanadate glass
8. Electrical properties of semiconducting barium-vanadate glasses doped with Fe2O310.1016/0022-3093(86)90089-X ↗
9. Structural and optical studies of Fe2O3 doped barium strontium titanate borosilicate glasses
10. SiO2-TiO2-B2O3-BaO glass-ceramic system with Fe2O3 or CuO additives as photocatalyst10.1016/j.jece.2016.06.020 ↗
11. Influence of Fe2O3 on the physical, structural and electrical properties of sodium lead borate glasses10.1007/s40145-014-0107-z ↗
12. Optical study of lead borosilicate glasses10.1016/j.physb.2010.02.055 ↗
13. J. Non-Cryst. Solids · 2009 · 335 · 2323
14. Semi-quantitative analysis for FTIR spectra of Al2O3-PbO-B2O3-SiO2 glasses10.1016/j.jnoncrysol.2011.10.037 ↗
15. Role of titanium ions on the physical and structural properties of calcium zinc bismuth phosphate glass ceramics10.1016/j.jnoncrysol.2015.12.010 ↗
16. Electrical properties of titanium dioxide semiconductors10.1103/PhysRev.91.793 ↗
17. Crystallization and dielectric study of (Pb,Sr)TiO3 borosilicate glass ceramics10.1007/s12034-013-0489-5 ↗
18. On crystallization behaviour of perovskite glass ceramics10.1179/1743676113Y.0000000134 ↗
19. Dielectric behaviour of perovskite glass ceramics10.1007/s10854-014-2311-6 ↗
20. Synthesis, crystallization and dielectric behaviour of lead bismuth titanate borosilicate glasses with addition of 1% La2O310.1155/2015/498254 ↗
21. Effect of donor and acceptor dopants on crystallization, microstructural and dielectric behaviors of barium strontium titanate glass ceramics10.1016/j.jallcom.2016.02.117 ↗
22. Synthesis and optical properties of SiO2-Al2O3-MgO-K2CO3-CaO-MgF2-La2O3 glasses10.1007/s12034-016-1197-8 ↗
23. Synthesis, structural and X-ray absorption spectroscopy of (PbxBi1−x).TiO3borosilicate glass and glass ceramics
24. Manual of Weighing Applications, Part 1, Density. http://www.dcu.ie/sites/default/files/mechanical_engineering/pdfs/manuals/DensityDeterminationManual.pdfManual.pdf.
25. Density and molar volume studies of phosphate glasses
26. FTIR measurements of SiO2 glass prepared by sol-gel technique
27. Microwave preparation of SiO2-B2O3-Na2O-K2O-CaO-Fe2O3-TiO2 glass system
28. Optical and structural investigation of Eu3+ ions in Nd3+ co-doped magnesium lead borosilicate glasses10.1016/j.jallcom.2012.12.162 ↗
29. Structure and spectroscopy of rare earth-doped lead phosphate glasses10.1016/j.jallcom.2013.10.106 ↗
30. Structural influence of PbO by means of FTIR and acoustics on calcium alumino-borosilicate glass system10.1016/j.jnoncrysol.2010.01.010 ↗
31. Synthesis and optical characterization of (Pb,Bi)TiO3 borosilicate glass system
32. Thermal and structural properties of Nd2O3-doped calcium boroaluminate glasses10.1016/S1002-0721(16)60057-1 ↗
33. Chemical durability and structural analysis of PbO–B2O3 glasses and testing for simulated radioactive wastes10.1016/j.jnucmat.2013.10.025 ↗
34. Raman spectra and optical properties of selected Bi2O3-PbO-B2O3-GeO2 glasses10.1016/j.optmat.2008.10.024 ↗
35. Spectroscopic and dielectric investigations on the role of molybdenum ions in lead niobium germanosilicate glasses10.1016/j.jnoncrysol.2016.04.008 ↗
36. Optical band gap studies on (55–x)Na2O-xPbO-45P2O5 (SLP) glass system10.1016/S0925-3467(00)00033-1 ↗
37. Optical spectroscopic analysis of high density lead borosilicate glasses
38. Compositional dependence of optical band gap and refractive index in lead and bismuth borate glasses10.1016/j.materresbull.2015.03.033 ↗
39. UV–vis spectroscopic studies of gamma irradiated lead sodium borosilicate glasses10.1016/j.molstruc.2013.12.036 ↗
40. T.G.V. M. Rao, A.R. Kumar, K. Neeraja, N. Veeraiah, M.R. Reddy, Optical and structural investigation of Dy3+–Nd3+ co-doped in magnesium lead borosilicate glasses, Spectrochim. Acta A Mol. Biomol. Spectrosc. 118 (2014) 744–751.10.1016/j.saa.2013.09.061 ↗
41. Effect of modifiers field strength on optical, structural and mechanical properties of lanthanum borosilicate glasses10.1016/j.jnoncrysol.2012.06.006 ↗
42. Linear and non-linear optics and FTIR characteristics of borosilicate glasses doped with gadolinium ions10.1016/j.optmat.2013.05.023 ↗
43. Structural characterization of borate glasses containing zinc and manganese oxides10.4236/jmp.2011.29129 ↗
44. Structural and optical properties of 30Li2O-55B2O3-5ZnO xTiO2-(10−x)V2O5, (0≤x≤10) glasses10.1016/j.jnoncrysol.2015.02.004 ↗
45. Effect of MgO on bioactivity, hardness, structural and optical properties of SiO2-K2O-CaO-MgO glasses10.1016/j.ceramint.2015.08.128 ↗