journal article·2019-10

Surface and structural characterization of amorphous Fe,Co-based melt-spun ribbons subjected to heat treatment processes

Sultan Öztürk, Kürşat İcin, Merve Gençtürk, Metin Göbülük, Uğur Topal, Peter Svec

Publisher page

Abstract

Abstract In this paper, the effect of the heat treatment process on the surface morphology, crystallization process and magnetic properties of Fe38Co38Mo8B15Cu ribbons produced by melt spinning was investigated. Number of protrusions uniformly distributed on surfaces of as-quenched ribbons were identified by atomic force microscopy (AFM). AFM results also indicated that variation of surface morphology of density, size, and shape of protrusions along the ribbon surface. According to magnetic force microscopy (MFM) analysis, the magnetic domain walls were not observed for annealing temperatures of 300 °C–360 °C. After annealing at 420 °C, the domains grow wider and align parallel to each other. Minor amounts of bcc-FeCo nano-sized crystalline grains which homogeneously and randomly distributed to the residual amorphous matrix were observed by the transmission electron microscopy (TEM). The crystalline grains are enlarged and became more visible. The best coercivity and saturation magnetization values were obtained at 360–420 °C.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Metallic Glasses and Amorphous Alloys

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (40)

Show source-provided references
1. Surface morphology of Fe79Mo8Cu1B12 ribbons characterised by atomic force microscopy
2. Magnetic domain patterns in bilayered ribbons studied by magnetic force microscopy and magneto-optical Kerr microscopy10.1155/2018/8308460 ↗
3. Phase transformations of Fe73.5Cu1Nb3Si15.5B7 amorphous alloy upon thermal treatment10.1016/j.jallcom.2010.05.145 ↗
4. AFM and Mössbauer spectrometry investigation of the nanocrystallization process in Fe–Mo–Cu–B rapidly quenched alloy10.1088/0953-8984/19/21/216219 ↗
5. Soft magnetic properties and giant magneto-impedance effect of Fe73. 5−xCrxSi13. 5B9Nb3Au1 (x = 1–5) alloys10.1016/j.jmmm.2006.03.066 ↗
6. Structure and magnetic properties of amorphous and nanocrystalline Fe40Co40Cu0. 5Zr9Al2Si4B4. 5 alloys10.1016/j.jmmm.2003.12.1315 ↗
7. Magnetic and structural characterization of Mo-Hitperm alloys with different Fe/Co ratio10.1016/j.jallcom.2010.10.113 ↗
8. Effect of planar flow melt spinning parameters on ribbon formation in soft magnetic Fe68.5Si18.5B9Nb3Cu1 alloy10.1007/s11663-011-9476-7 ↗
9. AFM surface morphology and magnetic properties of nanocrystalline Fe71Nb3.7Cu1Al3Mn0.8Si13.5B7 ribbons10.1016/j.apsusc.2004.03.254 ↗
10. Nanocrystallization of metallic glasses10.1016/S0022-3093(01)00627-5 ↗
11. The influence of annealing on the structural and soft magnetic properties of (Fe0. 4Co0. 6) 79Nb3B18 Nanocrystalline alloys10.3390/ma11112171 ↗
12. Microstructure and magnetic properties of Mo containing Nanoperm-type alloys
13. Bistable FeCoMoB microwires with nanocrystalline microstructure and increased Curie temperature10.1088/0022-3727/43/4/045002 ↗
14. The structure of rapidly quenched Fe–Co–B–Si based systems and the influence of addition of Cu and P10.1016/j.jallcom.2013.12.044 ↗
15. Grain size refinement in nanocrystalline Hitperm-type glass-coated microwires10.1016/j.jmmm.2015.12.034 ↗
16. Structure and magnetic properties of (Fe 0.5 Co 0.5) 88 Zr 7 B 4 Cu 1 nanocrystalline alloys10.1063/1.369007 ↗
17. Soft magnetic composite materials (SMCs)10.1016/j.jmatprotec.2007.02.034 ↗
18. Influence of heat treatment on magnetostrictions and electrical properties of (Fe1Co1) 76Mo8Cu1B1510.1016/j.jmmm.2008.04.168 ↗
19. Modern soft magnets: amorphous and nanocrystalline materials10.1016/j.actamat.2012.10.040 ↗
20. Amorphous and nanocrystalline materials for applications as soft magnets10.1016/S0079-6425(99)00002-X ↗
21. Planar flow melt spinning of soft magnetic amorphous ribbons
22. The effect of the melt spinning processing parameters on the martensitic transformation in Ti50–Ni35–Cu15 shape memory alloys10.1016/j.scriptamat.2004.06.023 ↗
23. The effect of the melt spinning processing parameters on the solidification structures in Ti–30at.% Ni–20at.% Cu shape memory alloys10.1016/j.msea.2006.05.169 ↗
24. An experimantal study of process behavior in planar flow melt spinning
25. Effects of manufacturing parameters in planar flow casting process on ribbon formation and puddle evolution of Fe–Si–B alloy10.2355/isijinternational.ISIJINT-2015-349 ↗
26. High thermal stability of soft magnetic (Fe,Co)–Mo–B–C–P–Si metallic glasses10.1016/j.jallcom.2009.08.114 ↗
27. Magnetic properties and surface roughness of Fe64Co21B15 amorphous ribbons quenched from different melt temperatures10.1016/S0921-5093(96)10639-0 ↗
28. XRD and AFM studies on nanostructured zinc aluminum oxide thin films prepared by multi-target magnetron sputtering
29. Eaton · 2010
30. Surface morphology in amorphous Fe–Mo–Cu–B ribbon system10.1016/j.jnoncrysol.2007.01.068 ↗
31. Influence of preparation conditions on the morphology of Fe78Si9B13 ribbons
32. Effect of surface features on magnetic anisotropy for amorphous FeBSi ribbons10.1016/0304-8853(90)90708-X ↗
33. EXAFS analysis of nanocrystallization process in Fe85Zr7B6Cu2 alloys by using cumulant method10.1016/j.physb.2005.03.037 ↗
34. Mössbauer and MFM investigations of surface magnetism in NANOPERM Nanocrystalline alloys10.12693/APhysPolA.126.124 ↗
35. Enhancement of crystallization in FeMoCuB metallic glass by deposition of Co layer10.1016/j.jallcom.2016.05.184 ↗
36. Thermal and microstructural stability of the soft magnetic Fe60Co18Nb6B15Cu1 alloy10.1016/j.jnoncrysol.2006.12.097 ↗
37. Study on soft magnetic properties of Fe36Co36B19.2Si4.8Nb4 metallic glass10.1088/1757-899X/382/2/022074 ↗
38. Magnetic microstructure of NANOPERM-type nanocrystalline alloys
39. Magnetic field annealing of FeCo-based amorphous alloys to enhance thermal stability and Curie temperature
40. Annealing temperature effect on microstructure, magnetic and microwave properties of Fe-based amorphous alloy powders10.1016/j.jmmm.2012.04.036 ↗