An investigation of the mixed water/formamide solvent on the synthesis of cadmium nitroprusside particles and its behavior in the electrochemical sensing of isoniazid
Source abstract
Abstract
Size-controlled cadmium nitroprussides, with particles in the micron meter or submicron size range (0.050–1.15 micron), (CdNPs) were prepared from total and varied compositions of water and formamide solvent in the complexation reaction of cadmium and nitroprusside ions. Four analytical systems (CdNP-1, CdNP-2, CdNP-3, and CdNP-4) were set up. The coordinated materials were investigated by spectroscopic and analytical techniques such as Raman spectroscopy, ultraviolet-visible spectroscopy (UV-Vis), X-ray diffraction (XRD), scanning electron microscopy (SEM), and cyclic voltammetry (CV). The CVs of the modified graphite paste electrode with CdNP-1, CdNP-2, CdNP-3, and CdNP-4 (10% m/m) exhibited a defined redox pair with formal potential (Eθ′) = 0.63 ± 0.02 V (ν = 20 mV s−1; KNO3 1.0 M). The dependence of particle size on the isoniazid electro-oxidation was verified by CdNP-3 and CdNP-4 microparticles.
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Research context
OpenAlex topics: Analytical Chemistry and Sensors · Electrochemical sensors and biosensors · Conducting polymers and applications
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References (42)
Show source-provided references
1. Absalan G, Akhond M, Soleimani M, Ershadifar H (2016) Efficient electrocatalytic oxidation and determination of isoniazid on carbon ionic liquid electrode modified with electrodeposited palladium nanoparticles. J Electroanal Chem 761:1–7. https://doi.org/10.1016/j.jelechem.2015.11.04110.1016/j.jelechem.2015.11.041 ↗
2. Azad UP, Prajapati N, Ganesan V (2015) Selective determination of isoniazid using bentonite clay modified electrodes. Bioelectrochemistry. 101:120–125. https://doi.org/10.1016/j.bioelechem.2014.08.01110.1016/j.bioelechem.2014.08.011 ↗
3. Benavente A, De Morán JA, Piro OE, Castellano EE, Aymonino PJ (1997) Crystal and anion structure, TGA, DTA, and infrared and Raman spectra of manganese(II) nitroprusside dihydrate, Mn [Fe(CN)5NO]·2H2O. J Chem Crystallogr 27:343–352. https://doi.org/10.1007/BF0257656610.1007/BF02576566 ↗
4. Benetton SA, Kedor-Hackmann ERM, Santoro MIRM, Borges VM (1998) Visible spectrophotometric and first-derivative UV spectrophotometric determination of rifampicin and isoniazid in pharmaceutical preparations. Talanta. 47:639–643. https://doi.org/10.1016/S0039-9140(98)00111-810.1016/S0039-9140(98)00111-8 ↗
5. Bergamini MF, Santos DP, Zanoni MVB (2010) Determination of isoniazid in human urine using screen-printed carbon electrode modified with poly-l-histidine. Bioelectrochemistry. 77:133–138. https://doi.org/10.1016/j.bioelechem.2009.07.01010.1016/j.bioelechem.2009.07.010 ↗
6. De Oliveira PR, Oliveira MM, Zarbin AJG, Marcolino-Junior LH, Bergamini MF (2012) Flow injection amperometric determination of isoniazid using a screen-printed carbon electrode modified with silver hexacyanoferrates nanoparticles. Sensors Actuators B Chem 171–172:795–802. https://doi.org/10.1016/j.snb.2012.05.07310.1016/j.snb.2012.05.073 ↗
7. Do Carmo DR, Da Silva RM, Stradiotto NR (2002) Estudo eletroquímico de Fe[Fe(CN)5NO] em eletrodo de pasta de grafite. Eclética Química 27:197–210. https://doi.org/10.1590/S0100-4670200200020001710.1590/S0100-46702002000200017 ↗
8. Do Carmo DR, Da Silva RM, Stradiotto NR (2003) Electrocatalytic, and voltammetric determination of sulfhydryl compounds through iron nitroprusside modified graphite paste electrode. J Braz Chem Soc 14:616–620. https://doi.org/10.1590/S0103-5053200300040001910.1590/S0103-50532003000400019 ↗
9. Do Carmo DR, Gabriel S, Silvestrini DR, Bicalho UO, Cumba LR (2012) Voltammetric study of the copper pentacyanonitrosylferrate adsorbed on the silica modified with a poly(propylene)imine hexadecylamine dendrimer for determination of nitrite. Int J Electrochem 2012:1–8. https://doi.org/10.1155/2012/52759610.1155/2012/527596 ↗
10. Do Carmo DR, Souza MM, Bicalho UO, Dos Santos VS, Souza JP, Silvestrini DR (2015) Direct preparation and characterization of copper pentacyanonitrosylferrate nanoparticles. J Nanomater 2015:1–6. https://doi.org/10.1155/2015/50242410.1155/2015/502424 ↗
11. Do Carmo DR, Fernandes DS, Cumba LR, Magossi MS, Dos Santos VS (2016) Solvent mixture effect in the zinc hexacyanoferrate (III) nanoparticles: synthesis, characterization and voltammetric application. Mater Res Bull 84:370–377. https://doi.org/10.1016/j.materresbull.2016.08.03410.1016/j.materresbull.2016.08.034 ↗
12. El-Kommos ME, Yanni AS (1988) Spectrophotometric determination of isoniazid using 6,7-dichloroquinoline-5,8-dione. Analyst. 113:1091–1095. https://doi.org/10.1039/an988130109110.1039/an9881301091 ↗
13. Fang P-F, Cai H-L, Li H-D, Zhu R-H, Tan Q-Y, Gao W, Xu P, Liu Y-P, Zhang W-Y, Chen Y-C, Zhang F (2010) Simultaneous determination of isoniazid, rifampicin, levofloxacin in mouse tissues and plasma by high-performance liquid chromatography-tandem mass spectrometry. J Chromatogr B 878:2286–2291. https://doi.org/10.1016/j.jchromb.2010.06.03810.1016/j.jchromb.2010.06.038 ↗
14. Ghalsasi PP, Ghalsasi PS, Muthu DVS (2017) Back-bonding signature with high pressure: Raman studies on silver nitroprusside. Inorg Chem 56:9669–9675. https://doi.org/10.1021/acs.inorgchem.7b0115110.1021/acs.inorgchem.7b01151 ↗
15. Ghoneim MM, El-Baradie KY, Tawfik A (2003) Electrochemical behavior of the antituberculosis drug isoniazid and its square-wave adsorptive stripping voltammetric estimation in bulk form, tablets and biological fluids at a mercury electrode. J Pharm Biomed Anal 33:673–685. https://doi.org/10.1016/S0731-7085(03)00311-X10.1016/S0731-7085(03)00311-X ↗
16. Gómez A, Reguera E, Cranswick LMD (2001) The structure of two orthorhombic nitroprussides: Cd[Fe(CN)5NO]·2H2O and Zn[Fe(CN)5NO]·2H2O. Polyhedron. 20:165–170. https://doi.org/10.1016/S0277-5387(00)00564-710.1016/S0277-5387(00)00564-7 ↗
17. Habibi E, Heidari H (2017) High-sensitive amperometric hydrazine sensor based on chemically synthesized zinc nitroprusside nanoparticle-supported carbon ceramic electrode. J Iran Chem Soc 14:1301–1308. https://doi.org/10.1007/s13738-017-1080-610.1007/s13738-017-1080-6 ↗
18. Hu Y-Q, Zhang S, Zhao F, Gao C, Feng L-S, Lv ZS, Xu Z, Wu X (2017) Isoniazid derivatives and their anti-tubercular activity. Eur J Med Chem 133:255–267. https://doi.org/10.1016/j.ejmech.2017.04.00210.1016/j.ejmech.2017.04.002 ↗
19. Johll ME, Williams DG, Johnson DC (1997) Activated pulsed amperometric detection of cysteine at platinum electrodes in acidic media. Electroanalysis. 9:1397–1402. https://doi.org/10.1002/elan.114009180510.1002/elan.1140091805 ↗
20. Karlaganis G, Peretti E, Lauterburg BH (1987) Analysis of isoniazid, acetyl hydrazine and [15N2]acetylhydrazine in serum by capillary gas chromatography-ammonia chemical ionization mass spectrometry. J Chromatogr B Biomed Sci Appl 420:171–177. https://doi.org/10.1016/0378-4347(87)80169-X10.1016/0378-4347(87)80169-X ↗
21. Koopmans PP, Tan Y, Van Ginneken CAM, Gribnau FWJ (1984) High-performance liquid chromatographic determination of hydrochlorothiazide in plasma and urine. J Chromatogr B Biomed Sci Appl 307:445–450. https://doi.org/10.1016/S0378-4347(00)84120-110.1016/S0378-4347(00)84120-1 ↗
22. Lobo AO, Martin AA, Antunes EF, Trava-Airoldi VJ, Corat EJ (2005) Caracterização de materiais carbonosos por espectroscopia Raman. Rev Bras Apl Vácuo 24:98
23. Magossi MS, Fernandes DS, Do Carmo DR (2019) Synthesis of a novel hybrid nanocomposite based on copper pentacyanonitrosylferrate and octa(aminopropyl)silsesquioxane and its behavior on l-cysteine electrooxidation. Solid State Sci 95:105931. https://doi.org/10.1016/j.solidstatesciences.2019.10593110.1016/j.solidstatesciences.2019.105931 ↗
24. Majidi MR, Jouyban A, Asadpour-Zeynali K (2006) Voltammetric behavior and determination of isoniazid in pharmaceuticals by using overoxidized polypyrrole glassy carbon modified electrode. J Electroanal Chem 589:32–37. https://doi.org/10.1016/j.jelechem.2006.01.01610.1016/j.jelechem.2006.01.016 ↗
25. Manoharan PT, Gray HB (1965) Electronic structure of nitroprusside ion. J Am Chem Soc 87:3340–3348. https://doi.org/10.1021/ja01093a01110.1021/ja01093a011 ↗
26. Moussa LA, Khassouani C, Soulaymani R, Jana M, Cassanas G, Alric R, Hüe B (2002) Therapeutic isoniazid monitoring using a simple high-performance liquid chromatographic method with ultraviolet detection. J Chromatogr B 766:181–187. https://doi.org/10.1016/S0378-4347(01)00434-010.1016/S0378-4347(01)00434-0 ↗
27. Mullica DF, Tippin DB, Sappenfield EL (1991) The crystal structure analysis of iron nitroprusside, Fe[Fe(CN)5NO]·3H2O. J Crystallogr Spectrosc Res 21:81–85. https://doi.org/10.1007/BF0115898010.1007/BF01158980 ↗
28. Osiry H, Cano A, Reguera L, Lemus-Santana AA, Reguera E (2015) Mercury (I) nitroprusside: a 2D structure supported on homometallic interactions. J Solid State Chem 221:79–84. https://doi.org/10.1016/j.jssc.2014.09.02110.1016/j.jssc.2014.09.021 ↗
29. Razmi H, Heidari K (2005) Preparation and electrochemistry of cadmium pentacyanonitrosylferrate film modified glassy carbon electrode. Electrochim Acta 50:4048–4056. https://doi.org/10.1016/j.electacta.2004.12.03810.1016/j.electacta.2004.12.038 ↗
30. Razmi H, Heidari H (2009a) Nafion/lead nitroprusside nanoparticles modified carbon ceramic electrode as a novel amperometric sensor for l-cysteine. Anal Biochem 388:15–22. https://doi.org/10.1016/j.ab.2009.01.03610.1016/j.ab.2009.01.036 ↗
31. Razmi H, Heidari H (2009b) Nanomolar detection of hydrogen peroxide at a new polynuclear cluster of tin pentacyanonitrosylferrate nanoparticle-modified carbon ceramic electrode. Anal Biochem 392:126–132. https://doi.org/10.1016/j.ab.2009.05.04710.1016/j.ab.2009.05.047 ↗
32. Razmi H, Mohammad-Rezaei R (2010) Non-enzymatic hydrogen peroxide sensor using an electrode modified with iron pentacyanonitrosylferrate nanoparticles. Microchim Acta 171:257–265. https://doi.org/10.1007/s00604-010-0426-x10.1007/s00604-010-0426-x ↗
33. Reguera E, Dago A, Gómez A, Bertrán JF (1996) Structural changes in insoluble metal nitroprussides on ageing. Polyhedron. 15:3139–3145. https://doi.org/10.1016/0277-5387(95)00582-X10.1016/0277-5387(95)00582-X ↗
34. Reguera E, Marín E, Calderón A, Rodríguez-Hernández J (2007) Photo-induced charge transfer in Prussian blue analogues as detected by photoacoustic spectroscopy. Spectrochim Acta Part A Mol Biomol Spectrosc 68:191–197. https://doi.org/10.1016/j.saa.2006.11.01310.1016/j.saa.2006.11.013 ↗
35. Rodríguez-Hernández J, Reguera L, Lemus-Santana AA, Reguera E (2015) Silver nitroprusside: atypical coordination within the metal nitroprussides series. Inorg Chim Acta 428:51–56. https://doi.org/10.1016/j.ica.2014.12.02310.1016/j.ica.2014.12.023 ↗
36. Si X, Jiang L, Wang X, Ding Y, Luo L (2015) Determination of isoniazid content via cysteic acid/graphene modified glassy carbon electrode. Anal Methods 7:793–798. https://doi.org/10.1039/C4AY02013H10.1039/C4AY02013H ↗
37. Souza TR, De Sá AC, Franco FS, Barbosa PFP, Andrade RDA, da Costa FM, Carvalho KA, de Oliveira DR, Cumba LR, Paim LL, Vieira EG, Do Carmo DR (2020) Voltammetric behavior of a chemically modified carbon paste electrode with cadmium nitroprusside prepared in different water to formamide ratios. Int J Electrochem Sci 15:774–787. https://doi.org/10.20964/2020.01.5410.20964/2020.01.54 ↗
38. Torres-Garcia E, Balmaseda J, del Castillo LF, Reguera E (2006) Thermal evolution of microporous nitroprussides on their dehydration process. J Therm Anal Calorim 86:371–377. https://doi.org/10.1007/s10973-005-7385-110.1007/s10973-005-7385-1 ↗
39. Vo V, Van MN, Lee HI, Kim JM, Kim Y, Kim SJ (2008) A new route for obtaining Prussian blue nanoparticles. Mater Chem Phys 107:6–8. https://doi.org/10.1016/j.matchemphys.2007.07.00210.1016/j.matchemphys.2007.07.002 ↗
40. Yan X, Bo X, Guo L (2011) Electrochemical behaviors and determination of isoniazid at ordered mesoporous carbon modified electrode. Sensors Actuators B Chem 155:837–842. https://doi.org/10.1016/j.snb.2011.01.05810.1016/j.snb.2011.01.058 ↗
41. Yan H, XiaoH XQ, Liu J, Sun L, Zhou Y, Zhang Y, Chao L, Chen C, Yao S (2015) Simultaneous electroanalysis of isoniazid and uric acid at poly(sulfosalicylic acid)/electroreduced carboxylated graphene modified glassy carbon electrode. Sensors Actuators B Chem 207:167–176. https://doi.org/10.1016/j.snb.2014.10.00210.1016/j.snb.2014.10.002 ↗
42. Yun Xia H, Ya HX (2005) Determination of isoniazid using a gold electrode by differential pulse voltammetry. Anal Lett 38:1405–1416. https://doi.org/10.1081/AL-20006221510.1081/AL-200062215 ↗