journal article·2010-10

Hydrothermal synthesis of micrometer sized HgMoO4 flowers formed by nanorods

Run-Ping Jia, Ying-Qiang Zhang

Journal of Nanoparticle Research· Volume 12· Issue 8
Publisher page

Abstract

Micrometer sized HgMoO4 flowers formed by nanorods were prepared by a selected hydrothermal method using a mixture of ethanol and water as a reaction medium, which were characterized by scanning electron microscopy, X-ray diffractometer (XRD), FT-IR spectrometry, photoluminescence spectrometry, and UV–visible spectrometry. Results indicated that the micrometer sized flowers consisted of mercury molybdate nanorods, and the monoclinic wolframite-type structure of the flowers was confirmed by both XRD and FT-IR spectrometry. A blue shift of the photoluminescence peaks and a broadening of XRD peaks were observed, which increased with ethanol fraction in the reaction medium.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Pigment Synthesis and Properties · Gas Sensing Nanomaterials and Sensors · Luminescence Properties of Advanced Materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (15)

Show source-provided references
1. Blasse G, Heuval GPM (1974) Luminescence of mercuric molybdate and tungstate. J Lumin 9:74–7810.1016/0022-2313(74)90074-X ↗
2. Granqvist CG, Azens A, Hjelm A et al (1998) Recent advances in electrochromics for smart windows applications. Sol Energy 63:199–21610.1016/S0038-092X(98)00074-7 ↗
3. Jia RP, Wu QS, Ding YP (2007) Ultrasonic preparation and optical properties of HgWO4 nanoshuttles. Nano 2:15–1910.1142/S1793292007000313 ↗
4. Jia RP, Ouyang CF, Li YS et al (2008) Preparation and optical properties of HgWO4 nanorods by hydrothermal method coupled with ultrasonic technique. J Nanopart Res 10:215–21910.1007/s11051-007-9222-x ↗
5. Klissurski D, Mancheva M, Iordanova R et al (2006) Mechanochemical synthesis of nanocrystalline nickel molybdates. J Alloys Compd 422:53–5710.1016/j.jallcom.2005.11.073 ↗
6. Kraus H, Mikhailik VB, Ramachers Y et al (2005) Feasibility study of a ZnWO4 scintillator for exploiting materials signature in cryogenic wimp dark matter searches. Phys Lett B 610:37–4410.1016/j.physletb.2005.01.095 ↗
7. Mikhailik VB, Kraus H, Wahl D et al (2006) Optical and luminescent studies of ZnMoO4 using vacuum ultraviolet synchrotron radiation. Nucl Instrum Methods A 562:513–51610.1016/j.nima.2006.03.005 ↗
8. Phuruangrat A, Thongtem T, Thongtem S (2009) Preparation, characterization and photoluminescence of nanocrystiline calcium molybdate. J Alloys Compd 481:568–57210.1016/j.jallcom.2009.03.037 ↗
9. Ryu JH, Choi BG, Yoon JW et al (2007) Synthesis of CaMoO4 nanoparticles by plused laser ablation in deionized water and optical properties. J Lumin 124:67–7010.1016/j.jlumin.2006.01.368 ↗
10. Spassky DA, Ivanov SN, Kolobanov VN et al (2004) Optical and luminescent properties of the lead and barium molybdates. Radiat Meas 38:607–61010.1016/j.radmeas.2004.03.019 ↗
11. Tanaka K (2001) Cathode luminescence of samarium, europium, and gadolinium ion doped scintillator CdWO4 single crystals studied with X-ray photoelectron spectroscopy. J Appl Phys 89:5449–545310.1063/1.1365429 ↗
12. Trimble C, DeVries M, Hale JS et al (1999) Infrared emittance modulation devices using electrochromic crystalline tungsten oxide, polymer conductor, and nickel oxide. Thin Solid Films 26:355–356
13. Wang HL, Ma XD, Qian XF et al (2004) Selective synthesis of CdWO4 short nanorods and nanofibers and their self-assembly. J Solid State Chem 177:4588–459610.1016/j.jssc.2004.09.012 ↗
14. Yang J, Zhang CM, Wang LL et al (2008) Hydrothermal synthesis and luminescent and properties of LuBO3:Tb3+ microflowers. J Solid State Chem 181:2672–268010.1016/j.jssc.2008.06.045 ↗
15. Zorenko Y, Pashkovsky M, Voloshinovski A et al (2006) The luminescence of CaWO4: Bi single crystals. J Lumin 116:43–5110.1016/j.jlumin.2005.01.017 ↗