Formation and self-assembly growth of palladium nanospheres into flowerlike microstructures using hydrogen peroxide as a sole reducing and shape-controlling agent
Source abstract
Abstract
A novel and facile green synthetic method for creating flowerlike palladium microstructures (FPdµSTs) using hydrogen peroxide (H2O2) as a sole reducing and shape-controlling agent was developed. FPdµSTs with particle size in the range of 1–5 μm were successfully synthesized. Morphology (size and shape) and complexity of the FPdµSTs could be tuned through the synthetic conditions (i.e., concentrations of H2PdCl4 and H2O2). H2O2 played an important role in creating palladium microstructures by reduction of H2PdCl4 under acidic condition. The time-dependent investigation on the particle growth suggested that the FPdµSTs evolved from spherical palladium nanoparticles with a particle size of 3 nm. The small particles, which were formed at the early stage of the reaction, aggregated and grew into complex flowerlike microstructures.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Nanomaterials for catalytic reactions · Catalytic Processes in Materials Science · Polyoxometalates: Synthesis and Applications
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
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