Preparation of monodispersed Pd nanoparticles by laser ablation at air–suspension interface
Source abstract
Abstract
A novel route to produce nanocolloid of single nano-sized particles was developed. Pd particles are stirred in water. Then laser ablation was conducted using a second harmonic light from Nd:YAG laser system focused on the air–liquid interface. We could obtain yellow nanocolloid. Pd nanoparticles have been stably dispersed in water without any chemical reagents for >1 year. Large absorption below 500 nm could be confirmed. The surface condition of colloidal particles was analyzed by X-ray photoelectron spectroscopy (XPS) of dried particles on Si wafer and pH measurement of nanocolloid. The range of pH value of nanocolloid was from 2 to 3. On the other hand, NO3 and NO2 were detected on the dried sample by XPS spectrum. In addition, transmission electron microscopy and dynamic light scattering (DLS) methods revealed a very narrow size distribution. The size distribution in the range from 0.5 to 1.5 nm was confirmed by DLS method. The size distribution and stability of Pd nanocolloid could be explained by chemical reaction between air, water, and Pd target due to excitation by pulsed laser irradiation and production of active particles in the laser-induced plasma.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Laser-Ablation Synthesis of Nanoparticles · Gold and Silver Nanoparticles Synthesis and Applications · Nanoparticles: synthesis and applications
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (33)
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