Electrospray deposition of isolated chemically synthesized magnetic nanoparticles
Source abstract
Abstract
The deposition of isolated magnetic nanoparticles onto a substrate was performed using electrohydrodynamic spraying. Two kinds of nanoparticles were sprayed, 11 nm CoFe carbide nanospheres and 10.5 nm Fe nanocubes. By studying carefully the evolution of the sprayed charged droplets and the mechanism of nanoparticle dispersion in them, we could optimize the nanoparticle concentration within the initial nanoparticle solution (i) to reduce the magnetic interaction and therefore prevent agglomeration and (ii) to obtain in a relatively short period (1 h) a deposit of isolated magnetic nanoparticles with a density of up to 400 nanoparticles per µm2. These results open great perspectives for magnetic measurements on single objects using advanced magnetometry techniques as long as spintronics applications based on single chemically synthesized magnetic nanoparticles.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Electrohydrodynamics and Fluid Dynamics · Mass Spectrometry Techniques and Applications · Diamond and Carbon-based Materials Research
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (42)
Show source-provided references
1. Bardotti L, Tournus F, Delagrange Benoit J M, Pierre-Louis O, Dupuis V (2014) Behavior of size selected iron–platinum clusters soft landed on carbon nanotubes. Appl Surf Sci 301:564–56710.1016/j.apsusc.2014.02.129 ↗
2. Bernand-Mantel A, Seneor P, Bouzehouane K, Fusil S, Deranlot C, Petroff F, Fert A (2009) Anisotropic magneto-coulomb effects and magnetic single-electron-transistor action in a single nanoparticle. Nat Phys 5:920–92410.1038/nphys1423 ↗
3. Bogani L, Wernsdorfer W (2008) Molecular spintronics using single-molecule magnets. Nat Mater 7:17910.1038/nmat2133 ↗
4. Cloupeau M, Prunet-Foch B (1990) Electrostatic spraying of liquids: main functioning modes. J Electrost 25:165–18410.1016/0304-3886(90)90025-Q ↗
5. De la Mora JF (1996) On the outcome of the coulombic fission of a charged isolated drop. J Colloid Interface Sci 178:209–21810.1006/jcis.1996.0109 ↗
6. Desvaux C, Amiens C, Fejes P, Renaud P, Respaud M, Lecante P, Snoeck E, Chaudret B (2005) Multimillimetre-large superlattices of air-stable iron–cobalt nanoparticles. Nat Mater 4:750–75310.1038/nmat1480 ↗
7. Duft D, Achtzehn T, Müller R, Huber BA, Leisner T (2003) Coulomb fission: Rayleigh jets from levitated microdroplets. Nature 421:12810.1038/421128a ↗
8. Duguay J, Tan RP, Loubat A, Lacroix L-M, Carrey J, Fazzini PF, Chaudret B, Respaud M (2014) Tuning deposition of magnetic metallic nanoparticles from periodic pattern to thin film entrainment by dip coating method. Langmuir 30:902810.1021/la404044e ↗
9. Dumeste F, Chaudret B, Amiens C, Renaud P, Fejes P (2004) Superlattices of iron nanocubes synthesized from Fe[N(SiMe3)2]2. Science 303:821–88210.1126/science.1092641 ↗
10. Farid M (2003) A new approach to modelling of single droplet drying. Chem Eng Sci 58:2985–299310.1016/S0009-2509(03)00161-1 ↗
11. Fenn BJ, Mann M, Meng CK, Wong SF, Whitehouse CM (1989) Electrospray ionization for mass spectrometry of large biomolecules. Science 246:64–7110.1126/science.2675315 ↗
12. Ganan-Calvo AM, Lasheras JC, Davila JD, Barrero A (1994) The electrostatic spray emitted from an electrified conical meniscus. J Aerosol Sci 25:1121–114210.1016/0021-8502(94)90205-4 ↗
13. Gañan-Calvo AM, Davila J, Barrero A (1997) Current and droplet size in the electrospraying of liquids. Scaling laws. J Aerosol Sci 28:249–27510.1016/S0021-8502(96)00433-8 ↗
14. Ganzhorn M, Klyatskaya S, Ruben M, Wernsdorfer W (2013) Strong spin–phonon coupling between a single-molecule magnet and a carbon nanotube nanoelectromechanical system. Nat Nanotechnol 8:16510.1038/nnano.2012.258 ↗
15. Gatel C, Bonilla FB, Meffre A, Snoeck E, Warot-Fonrose B, Chaudret B, Lacroix L-M, Blon T (2015) Size specific spin configurations in single iron nanomagnet: from flower to exotic vortices. Nano Lett 15:6952–695710.1021/acs.nanolett.5b02892 ↗
16. Gomez A, Tang K (1994) Charge and fission of droplets in electrostatic sprays. Phys Fluids 6:404–41410.1063/1.868037 ↗
17. Hartman RPA, Brunner DJ, Camelot DMA, Marijnissen JCM, Scarlett B (2000) Jet break-up in electrohydrodynamic atomization in the cone-jet mode. J Aerosol Sci 31:65–9510.1016/S0021-8502(99)00034-8 ↗
18. Hogan Jr CJ, Biswas P (2011) Porous film deposition by electrohydrodynamic atomization of nanoparticle sols. Aerosol Sci Technol 42:75–85
19. Iskandar F, Gradon L, Okuyama K (2003) Control of the morphology of nanostructured particles prepared by the spray drying of a nanoparticle sol. J Colloid Interface Sci 265:296–30310.1016/S0021-9797(03)00519-8 ↗
20. Jamet M, Wernsdorfer W, Thirion C, Mailly D, Dupuis V, Melinon P, Perez A (2001) Magnetic anisotropy of a single cobalt nanocluster. Phys Rev Lett 86:467610.1103/PhysRevLett.86.4676 ↗
21. Jaworek A, Sobczyk AT (2008) Electrospraying route to nanotechnology: an overview. J Electrost 66:197–21910.1016/j.elstat.2007.10.001 ↗
22. Konermann L (2009) A simple model for the disintegration of highly charged solvent droplets during electrospray ionization. J Am Soc Mass Spectrom 20:496–50610.1016/j.jasms.2008.11.007 ↗
23. Lacroix L-M, Ho D, Sun S (2010) Recent advances in magnetic nanoparticles for diagnostic and therapeutic applications. Curr Top Med Chem 10:118410.2174/156802610791384207 ↗
24. Lacroix L-M, Huls NF, Ho D, Sun X, Cheng K, Sun S (2011) Stable single crystalline bcc-Fe nanoparticles. Nano Lett 11:1641–164510.1021/nl200110t ↗
25. Lassagne B, Ugnati D, Respaud M (2011) Ultrasensitive magnetometers based on carbon nanotube mechanical resonators. Phys Rev Lett 107:13080110.1103/PhysRevLett.107.130801 ↗
26. Lenggoro IW, Xia B, Okuyama K, de la Mora JF (2002) Sizing of colloidal nanoparticles by electrospray and differential mobility analyzer methods. Langmuir 18:4584–459110.1021/la015667t ↗
27. Li KY, Tu H, Ray AK (2005) Charge limits on droplets during evaporation. Langmuir 21:3786–379410.1021/la047973n ↗
28. Liakakos N, Cormary B, Li X, Lecante P, Respaud M, Maron L, Falqui A, Genovese A, Vendier L, Koïnis S, Chaudret B, Soulantica K (2012) The big impact of a small detail: cobalt nanocrystal polymorphism as a result of precursor addition rate during stock solution preparation. J Am Chem Soc 134:17922–1793110.1021/ja304487b ↗
29. Liakakos N, Blon T, Achkar C, Vilar V, Cormary B, Tan RP, Benamara O, Chaboussant G, Ott F, Warot-Fonrose B, Snoeck E, Chaudret B, Soulantica K, Respaud M (2014) Solution epitaxial growth of cobalt nanowires on crystalline substrates for data storage densities beyond 1Tbit/in2. Nano Lett 14:348110.1021/nl501018z ↗
30. Lu A-H, Salabas EL, Schüth F (2007) Magnetic nanoparticles: synthesis, protection, functionalization, and application. Angew Chem Int Ed 46:122210.1002/anie.200602866 ↗
31. Mao S, Lu G, Chen J (2008) Coating carbon nanotubes with colloidal nanocrystals by combining an electrospray technique with directed assembly using an electrostatic field. Nanotechnology 19:45561010.1088/0957-4484/19/45/455610 ↗
32. Meffre A, Lachaize S, Gatel C, Respaud M, Chaudret B (2011) Use of long chain amine as a reducing agent for the synthesis of high quality monodisperse iron(0) nanoparticles. J Mater Chem 21:13464–1346910.1039/c1jm12127h ↗
33. Meffre A, Mehdaoui B, Kelsen V, Carrey J, Lachaize S, Fazzini PF, Respaud M, Chaudret B (2012) A simple chemical route toward monodisperse iron carbide nanoparticles displaying tunable magnetic and unprecedented hyperthermia properties. Nano Lett 12:4722–472810.1021/nl302160d ↗
34. Mezhericher M, Levy A, Borde I (2008) Heat and mass transfer of single droplet/wet particle drying. Chem Eng Sci 63:12–2310.1016/j.ces.2007.08.052 ↗
35. Na HB, Song IC, Hyeon T (2009) Inorganic nanoparticles for MRI contrast agents. Adv Mater 21:213310.1002/adma.200802366 ↗
36. Rayleigh L (1882) On the equilibrium of liquid conducting masses charged with electricity. Philos Mag 14:18410.1080/14786448208628425 ↗
37. Rod I, Kazakova O, Cox DC, Spasova M, Michael Farle M (2009) The route to single magnetic particle detection: a carbon nanotube decorated with a finite number of nanocubes. Nanotechnology 20:33530110.1088/0957-4484/20/33/335301 ↗
38. Seneor P, Bertrand-Mantel A, Petroff F (2007) Nanospintronics: when spintronics meets single electron physics. J Phys 19:165222
39. Smith DP (1986) The electrohydrodynamic atomization of liquids. IEEE Trans Ind Appl 1A–22:527–53510.1109/TIA.1986.4504754 ↗
40. Snoeck E, Gatel C, Lacroix L-M, Blon T, Lachaize S, Carrey J, Respaud M, Chaudret B (2008) Magnetic configurations of 30 nm iron nanocubes studied by electron holography. Nano Lett 8:4293–429610.1021/nl801998x ↗
41. Soulantica K, Maisonnat A, Fromen M-C, Casanove M-J, Chaudret B (2003) Templated synthesis of inorganic hollow spheres with a tunable cavity size onto core-shell gel particles. Angew Chem Int Ed 42:1945–194710.1002/anie.200250484 ↗
42. Suh J, Han B, Okuyama K, Choi M (2005) Highly charging of nanoparticles through electrospray of nanoparticle suspension. J Colloid Interface Sci 287:135–14010.1016/j.jcis.2005.01.078 ↗