journal article·2010-05

Preparation and characterization of Ag nanoparticle-embedded polymer electrospun nanofibers

Guoping Dong, Xiudi Xiao, Xiaofeng Liu, Bin Qian, Zhijun Ma, Song Ye, Danping Chen, Jianrong Qiu

Journal of Nanoparticle Research· Volume 12· Issue 4
Publisher page

Abstract

Poly (vinyl alcohol) (PVA) and poly (vinyl pyrrolidone) (PVP) nanofibers embedding Ag nanoparticles (5–18 nm) have been prepared successfully by electrospinning at room temperature. Scanning electron microscope (SEM), X-ray diffraction (XRD), high-resolution transmission electron microscopy (HRTEM), Fourier transform IR spectra (FTIR), and Raman scattering were used to characterize the structure and properties of Ag nanoparticle-embedded PVA and PVP nanofibers before and after heat treatment at different temperature. The antibacterial activity of Ag nanoparticle-embedded PVP nanofibers after heat treatment was also tested, which indicated that the biological activity of yeast cells was effectively inhibited by these Ag nanoparticle-embedded PVP nanofibers.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Electrospun Nanofibers in Biomedical Applications · Conducting polymers and applications · Polymer Nanocomposite Synthesis and Irradiation

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (26)

Show source-provided references
1. Boccara AC, Fournier D, Kumar A, Pandey GC (1997) Nondestructive evaluation of carbon fiber by mirage-FTIR spectroscopy. J Appl Polym Sci 63:1785–1791. doi: 10.1002/(SICI)1097-4628(19970328)63:13<1785::AID-APP11>3.0.CO;2-Y10.1002/(SICI)1097-4628(19970328)63:13<1785::AID-APP11>3.0.CO;2-Y ↗
2. Bognitzki M, Czado W, Frese T, Schaper A, Hellwig M, Steinhart M, Greiner A, Wendorff JH (2001) Nanostructured fibers via electrospinning. Adv Mater 13:70–72. doi: 10.1002/1521-4095(200101)13:1<70::AID-ADMA70>3.0.CO;2-H10.1002/1521-4095(200101)13:1<70::AID-ADMA70>3.0.CO;2-H ↗
3. Duan YY, Jia J, Wang SH, Yan W, Jin L, Wang ZY (2007) Preparation of antimicrobial poly (epsilon-caprolactone) electrospun nanofibers containing silver-loaded zirconium phosphate nanoparticles. J Appl Polym Sci 106:1208–1214. doi: 10.1002/app.2678610.1002/app.26786 ↗
4. Escribano R, Sloan J (2001) Raman spectroscopy of carbon-containing particles. Vib Spectrosc 26:179–186. doi: 10.1016/S0924-2031(01)00106-010.1016/S0924-2031(01)00106-0 ↗
5. Formo E, Lee E, Campbell D, Xia YN (2008) Functionalization of electrospun TiO2 nanofibers with Pt nanoparticles and nanowires for catalytic applications. Nano Lett 8:668–672. doi: 10.1021/nl073163v10.1021/nl073163v ↗
6. Hong KH (2007) Preparation and properties of electrospun poly (vinyl alcohol)/silver fiber web as wound dressings. Polym Eng Sci 47:43–49. doi: 10.1002/pen.2066010.1002/pen.20660 ↗
7. Jana NR, Gearheart L, Murphy CJ (2001) Wet chemical synthesis of silver nanorods and nanowires of controllable aspect ratio. Chem Commun (Camb) 7:617–618. doi: 10.1039/b100521i10.1039/b100521i ↗
8. Jin WJ, Lee HK, Jeong EH, Park WH, Youk JH (2005) Preparation of polymer nanofibers containing silver nanoparticles by using poly (N-vinylpyrrolidone). Macromol Rapid Commun 26:1903–1907. doi: 10.1002/marc.20050056910.1002/marc.200500569 ↗
9. Jin M, Zhang XT, Nishimoto S, Liu ZY, Tryk DA, Murakami T, Fujishima A (2007a) Large-scale fabrication of Ag nanoparticles in PVP nanofibres and net-like silver nanofibre films by electrospinning. Nanotechnology 18:075605. doi: 10.1088/0957-4484/18/7/07560510.1088/0957-4484/18/7/075605 ↗
10. Jin WJ, Jeon HJ, Kim JH, Youka JH (2007b) A study on the preparation of poly (vinyl alcohol) nanofibers containing silver nanoparticles. Synth Met 157:454–459. doi: 10.1016/j.synthmet.2007.05.01110.1016/j.synthmet.2007.05.011 ↗
11. Li D, Xia YN (2004) Electrospinning of nanofibers: reinventing the wheel? Adv Mater 16:1151–1170. doi: 10.1002/adma.20040071910.1002/adma.200400719 ↗
12. Li D, McCann JT, Gratt M, Xia YN (2004) Photocatalytic deposition of gold nanoparticles on electrospun nanofibers of titania. Chem Phys Lett 394:387–391. doi: 10.1016/j.cplett.2004.07.04410.1016/j.cplett.2004.07.044 ↗
13. Li ZY, Huang HM, Shang TC, Yang F, Zheng W, Wang C, Manohar SK (2006) Facile synthesis of single-crystal and controllable sized silver nanoparticles on the surfaces of polyacrylonitrile nanofibres. Nanotechnology 17:917–920. doi: 10.1088/0957-4484/17/3/05010.1088/0957-4484/17/3/050 ↗
14. Misra A, Tyagi PK, Singh MK, Misra DS (2006) FTIR studies of nitrogen doped carbon nanotubes. Diam Relat Mater 15:385–388. doi: 10.1016/j.diamond.2005.08.01310.1016/j.diamond.2005.08.013 ↗
15. Moran-Mirabal JM, Slinker JD, DeFranco JA, Verbridge SS, Ilic R, Flores-Torres S, Abruna H, Malliaras GG, Craighead HG (2007) Electrospun light-emitting nanofibers. Nano Lett 7:458–463. doi: 10.1021/nl062778+10.1021/nl062778+ ↗
16. Patel AC, Li SX, Wang C, Zhang WJ, Wei Y (2007) Electrospinning of porous silica nanofibers containing silver nanoparticles for catalytic applications. Chem Mater 19:1231–1238. doi: 10.1021/cm061331z10.1021/cm061331z ↗
17. Piperno S, Lozzi L, Rastelli R, Passacantando M, Santucci S (2006) PMMA nanofibers production by electrospinning. Appl Surf Sci 252:5583–5586. doi: 10.1016/j.apsusc.2005.12.14210.1016/j.apsusc.2005.12.142 ↗
18. Rafizah WAW, Ismail AF (2008) Effect of carbon molecular sieve sizing with poly (vinyl pyrrolidone) K-15 on carbon molecular sieve-polysulfone mixed matrix membrane. J Membr Sci 307:53–61. doi: 10.1016/j.memsci.2007.09.00710.1016/j.memsci.2007.09.007 ↗
19. Shao CL, Yang XH, Guan HY, Liu YC, Gong J (2004) Electrospun nanofibers of NiO/ZnO composite. Inorg Chem Commun 7:625–627. doi: 10.1016/j.inoche.2004.03.00610.1016/j.inoche.2004.03.006 ↗
20. Song HW, Yu HQ, Pan GH, Bai X, Dong B, Zhang XT, Hark SK (2008) Electrospinning preparation, structure, and photoluminescence properties of YBO3: Eu3+ nanotubes and nanowires. Chem Mater 20:4762–4767. doi: 10.1021/cm800786410.1021/cm8007864 ↗
21. Tachikawa T, Ishigaki T, Li JG, Fujitsuka M, Majima T (2008) Defect-mediated photoluminescence dynamics of Eu3+-doped TiO2 nanocrystals revealed at the single-particle or single-aggregate level. Angew Chem Int Ed 47:5348–5352. doi: 10.1002/anie.20080052810.1002/anie.200800528 ↗
22. Wang YZ, Li YX, Yang ST, Zhang GL, An DM, Wang C, Yang QB, Chen XS, Jing XB, Wei Y (2006) A convenient route to polyvinyl pyrrolidone/silver nanocomposite by electrospinning. Nanotechnology 17:3304–3307. doi: 10.1088/0957-4484/17/13/03710.1088/0957-4484/17/13/037 ↗
23. Wu J, Coffer JL (2007) Emissive erbium-doped silicon and germanium oxide nanofibers derived from an electrospinning process. Chem Mater 19:6266–6276. doi: 10.1021/cm702226x10.1021/cm702226x ↗
24. Xu XY, Yang QB, Wang YZ, Yu HJ, Chen XS, Jing XB (2006) Biodegradable electrospun poly (l-lactide) fibers containing antibacterial silver nanoparticles. Eur Polym J 42:2081–2087. doi: 10.1016/j.eurpolymj.2006.03.03210.1016/j.eurpolymj.2006.03.032 ↗
25. Zaporojtchenko V, Podschun R, Schurmann U, Kulkarni A, Faupel F (2006) Physico-chemical and antimicrobial properties of co-sputtered Ag-Au/PTFE nanocomposite coatings. Nanotechnology 17:4904–4908. doi: 10.1088/0957-4484/17/19/02010.1088/0957-4484/17/19/020 ↗
26. Zhang YW, Peng HS, Huang W, Zhou YF, Yan DY (2008) Facile preparation and characterization of highly antimicrobial colloid Ag or Au nanoparticles. J Colloid Interface Sci 325:371–376. doi: 10.1016/j.jcis.2008.05.06310.1016/j.jcis.2008.05.063 ↗