Flame spray synthesis under a non-oxidizing atmosphere: Preparation of metallic bismuth nanoparticles and nanocrystalline bulk bismuth metal
Source abstract
Abstract
Metallic bismuth nanoparticles of over 98% purity were prepared by a modified flame spray synthesis method in an inert atmosphere by oxygen-deficient combustion of a bismuth-carboxylate based precursor. The samples were characterized by X-ray diffraction, thermal analysis and scanning electron microscopy confirming the formation of pure, crystalline metallic bismuth nanoparticles. Compression of the as-prepared powder resulted in highly dense, nanocrystalline pills with strong electrical conductivity and bright metallic gloss.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: nanoparticles nucleation surface interactions · Coagulation and Flocculation Studies · Laser-Ablation Synthesis of Nanoparticles
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (55)
Show source-provided references
1. Alivisatos A.P. (1996). Science 271:933–93710.1126/science.271.5251.933 ↗
2. Arabi-Katbi O.I., Pratsinis S.E., Morrison P.W., Megaridis C.M. (2001). Comb. Flame 124:56010.1016/S0010-2180(00)00227-3 ↗
3. Balan L., Schneider R., Billaud D., Fort Y., Ghanbaja J. (2004) Nanotechnology 15:94010.1088/0957-4484/15/8/011 ↗
4. Baribeau J.M., Rowell N.L., Lockwood D.J. (2005). J. Mater. Res. 20:327810.1557/jmr.2005.0405 ↗
5. Black, M.R., Y.M. Lin, S.B. Cronin, O. Rabin & M.S.␣Dresselhaus, 2002. Phys. Rev. B 6510.1103/PhysRevB.65.195417 ↗
6. Brochin F., Devaux X., Ghanbaja J., Scherrer H. (1999). Nanostruct. Mater. 11:110.1016/S0965-9773(98)00155-X ↗
7. Chen I.W., Wang X.H. (2000). Nature 404:16810.1038/35004548 ↗
8. Costa-Krämer J.L., García N., Olin H. (1997). Phys. Rev. B 55:1291010.1103/PhysRevB.55.12910 ↗
9. Dellinger T.M., Braun P.V., (2004). Chem. Mat. 16:220110.1021/cm0349194 ↗
10. Dresselhaus M.S., Dresselhaus G., Sun X., Zhang Z., Cronin S.B., Koga T. (1999). Phys. Solid State 41:67910.1134/1.1130849 ↗
11. Fang J.Y., Stokes K.L., Wiemann J., Zhou W.L. (2000). Mater. Lett. 42:11310.1016/S0167-577X(99)00169-X ↗
12. Fang, J.Y., K.L. Stokes, W.L.L. Zhou, W.D. Wang & J. Lin, 2001. Chem. Commun. 187210.1039/b106105b ↗
13. Foos E.E., Stroud R.M., Berry A.D., Snow A.W., Armistead J.P. (2000). J. Am. Chem. Soc. 122:711410.1021/ja001118i ↗
14. Fu R.L., Xu S., Lu Y.N., Zhu J.J. (2005). Cryst. Growth Des. 5:137910.1021/cg049686n ↗
15. Gallo C.F., Chandrasekhar B.S., Sutter P.H. (1963). J. Appl. Phys. 34:14410.1063/1.1729056 ↗
16. Giesen B., Orthner H.R., Kowalik A., Roth P. (2004). Chem. Eng. Sci. 59:220110.1016/j.ces.2004.02.013 ↗
17. Grass, R.N., E.K. Athanassiou & W.J. Stark, 2005. EP Patent application 05 019287.1
18. Grass, R.N. & W.J. Stark, 2005. Chem. Commun. 176710.1039/b419099h ↗
19. Harman T.C., Taylor P.J., Walsh M.P., LaForge B.E. (2002). Science 297:222910.1126/science.1072886 ↗
20. Height M.J., Howard J.B., Tester J.W., Sande J.B.V. (2004) Carbon 42:229510.1016/j.carbon.2004.05.010 ↗
21. Heremans J., Thrush C.M., Lin Y.M., Cronin S., Zhang Z., Dresselhaus M.S., Mansfield J.F. (2000). Phys. Rev. B 61:292110.1103/PhysRevB.61.2921 ↗
22. Huber, M., W.J. Stark, S. Loher, M. Maciejewski, F. Krumeich & A. Baiker, 2005. Chem. Commun. 64810.1039/b411725e ↗
23. Johannessen T., Jenson J.R., Mosleh M., Johansen J., Quaade U., Livbjerg H. (2004). Chem. Eng. Res. Des. 82:144410.1205/cerd.82.11.1444.52025 ↗
24. Jossen R., Pratsinis S.E., Stark W.J., Madler L. (2005). J. Am. Ceram. Soc. 88:138810.1111/j.1551-2916.2005.00249.x ↗
25. Keskinen H., Makela J.M., Vippola M., Nurminen M., Liimatainen J., Lepisto T., Keskinen J. (2004). J. Mater. Res. 19:154410.1557/JMR.2004.0207 ↗
26. Knipping J., Wiggers H., Kock B.F., Hulser T., Rellinghaus B., Roth P. (2004). Nanotechnology 15:166510.1088/0957-4484/15/11/051 ↗
27. Kruis F.E., Fissan H., Peled A. (1998). J. Aerosol. Sci. 29:51110.1016/S0021-8502(97)10032-5 ↗
28. Laine R.M., Marchal J., Sun H.P., Pan X.Q. (2005). Adv. Mater. 17:83010.1002/adma.200401001 ↗
29. Lide D.R., 1997. CRC Handbook of Chemistry and Physics, 78th edn. CRC Press
30. Loher S., Stark W.J., Maciejewski M., Baiker A., Pratsinis S.E., Reichhardt D., Maspero F., Krumeich F., Günther D. (2005). Chem. Mater. 17:3610.1021/cm048776c ↗
31. Madler L., Kammler H.K., Mueller R., Pratsinis S.E., (2002a). J. Aerosol. Sci. 33:36910.1016/S0021-8502(01)00159-8 ↗
32. Madler L., Pratsinis S.E. (2002). J. Am. Ceram. Soc. 85:171310.1111/j.1151-2916.2002.tb00340.x ↗
33. Madler L., Stark W.J., Pratsinis S.E. (2002b). J. Mater. Res. 17:135610.1557/JMR.2002.0202 ↗
34. Madler L., Stark W.J., Pratsinis S.E. (2002c). J. Appl. Phys. 92:653710.1063/1.1518132 ↗
35. Makela J.M., Keskinen H., Forsblom T., Keskinen J. (2004). J. Mater. Sci. 39:278310.1023/B:JMSC.0000021454.15740.e6 ↗
36. Moisala A., Nasibulin A.G., Kauppinen E.I. (2003). J. Phys.-Condes. Matter 15:S301110.1088/0953-8984/15/42/003 ↗
37. Mueller R., Madler L., Pratsinis S.E. (2003). Chem. Eng. Sci. 58:196910.1016/S0009-2509(03)00022-8 ↗
38. Nasibulin A.G., Ahonen P.P., Richard O., Kauppinen E.I., Altman I.S. (2001). J. Nanopart. Res. 3:38510.1023/A:1012508407420 ↗
39. Nasibulin A.G., Shurygina L.I., Kauppinen E.I. (2005). Colloid J. 67:110.1007/s10595-005-0041-4 ↗
40. Rosner D.E. (2005). Ind. Eng. Chem. Res. 44:604510.1021/ie0492092 ↗
41. Sanders P.G., Youngdahl C.J., Weertman J.R. (1997). Mater. Sci. Eng. A-Struct. Mater. Prop. Microstruct. Process. 234:7710.1016/S0921-5093(97)00185-8 ↗
42. Sandler S.I. (1999). Chemical and Engineering Thermodynamics. John Wiley & Sons, New York
43. Sandhu A., Kurosawa K., Dede M., Oral A. (2004). Jpn. J. Appl. Phys. Part 1 43:77710.1143/JJAP.43.777 ↗
44. Schiotz J., Vegge T., Di Tolla F.D., Jacobsen K.W. (1999). Phys. Rev. B 60:1197110.1103/PhysRevB.60.11971 ↗
45. Stark W.J., Grunwaldt J.D., Maciejewski M., Pratsinis S.E., Baiker A. (2005). Chem. Mat. 17:335210.1021/cm050538+ ↗
46. Stark W.J., L. Madler, M. Maciejewski, S.E. Pratsinis & A.␣Baiker 2003. Chem. Commun. 588–58910.1039/b211831a ↗
47. Suh Y.J., Jang H.D., Chang H.K., Hwang D.W., Kim H.C. (2005). Mater. Res. Bull. 40:210010.1016/j.materresbull.2005.07.004 ↗
48. Suryanarayana C. (1995). Int. Mater. Rev. 40:4110.1179/095066095790151106 ↗
49. Toprak M.S., Zhang Y., Jo Y., Kim D.K., Muhammed M. (2005). Solid State Phenom. 101–102:19710.4028/www.scientific.net/SSP.101-102.197 ↗
50. Tsantilis S., Kammler H.K., Pratsinis S.E. (2002). Chem. Eng. Sci. 57:2139–215610.1016/S0009-2509(02)00107-0 ↗
51. Vander Wal R.L., Ticich T.M., Curtis V.E. (2000). Chem. Phys. Lett. 323:21710.1016/S0009-2614(00)00522-4 ↗
52. Wang Y.W., Hong B.H., Kim K.S. (2005). J. Phys. Chem. B 109:706710.1021/jp046423v ↗
53. Wegner K., Walker B., Tsantilis S., Pratsinis S.E. (2002). Chem. Eng. Sci. 57:175310.1016/S0009-2509(02)00064-7 ↗
54. Zachariah M.R., Huzarewicz S. (1991). Combust. Flame 87:10010.1016/0010-2180(91)90030-F ↗
55. Zhao Y.B., Zhang Z.J., Dang H.X. (2004). Mater. Lett. 58:79010.1016/j.matlet.2003.07.013 ↗