An Experimental Study on Nano-Carbon Films as an Anti-Wear Protection for Drilling Tools
Source abstract
Abstract
Carbon thin films of 50–100 nm thickness were synthesized by Pulsed Laser Deposition in vacuum at different laser fluences from 2 to 6 J/cm2. The deposited films were characterized by Raman spectroscopy for compositional assessment, scanning electron microscopy for morphology/thickness evaluations, and X-ray reflectivity for density, thickness, and roughness determinations. The films were ~100 nm thin, smooth, droplet-free, made of a-C:H type of diamond-like carbon. The mechanical properties of synthesized films were studied by nanoindentation and adhesion tests. The films that were obtained at low laser fluences (2, 3 J/cm2) had better mechanical properties as compared to those synthesized at higher fluences. The mean values of hardness were around 20 GPa, while the friction coefficient was 0.06. The deposition conditions of carbon thin films that displayed the best mechanical properties were further used to coat commercial drills. Both uncoated and coated drills were tested on plates that were made of three types of steel: Stainless steel 304, general use AISI 572 Gr 65 steel (OL60), and AISI D3 tool steel (C120). All of the drill edges and tips were studied by optical and scanning electron microscopes. The coated samples were clearly found to be more resistant, and displayed less morphological defects than their uncoated counterparts when drilling stainless steel and OL60 plates. In the case of C120 steel, carbon coatings failed because of the high friction between drill and the metal plate resulting in tip edges blunting that occurred during processing.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Diamond and Carbon-based Materials Research · Metal and Thin Film Mechanics · Advanced materials and composites
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
National Institute for Lasers, Plasma and Radiation Physics (INFLPR), 077125 Magurele, Romania
Department of Materials Science, Faculty of Materials Science and Engineering, Transilvania University of Brasov, 500068 Brasov, Romania
National Institute for Research and Development in Microtechnologies, RO-077190 Voluntari, Romania
Funding
National Program · CNCS‒UEFISCDI · CNCS-UEFISCDI · PRO-DD
References (39)
Show source-provided references
1. Diamond-like amorphous carbon10.1016/S0927-796X(02)00005-0 ↗
2. Microstructure and property of diamond-like carbon films with Al and Cr co-doping deposited using a hybrid beams system10.1016/j.apsusc.2015.11.025 ↗
3. The role of ambient gas and pressure on the structuring of hard diamond-like carbon films synthesized by pulsed laser deposition10.3390/ma8063284 ↗
4. High energy radial deposition of diamond-like carbon coatings10.3390/coatings5030326 ↗
5. Performance of carbide tools coated with DLC in the drilling of SAE 323 aluminum alloy10.1016/j.surfcoat.2015.09.061 ↗
6. Tribological behavior of Al–6.5%, –12%, –18.5% Si alloys during machining using CVD diamond and DLC coated tools10.1016/j.surfcoat.2015.08.073 ↗
7. Ciniero, A., Le Rouzic, J., and Reddyhoff, T. (2017). The use of triboemission imaging and charge measurements to study DLC coating failure. Coatings, 7.10.3390/coatings7080129 ↗
8. Deposition of silicon-doped diamond-like carbon films by plasma-enhanced chemical vapor deposition using an intermittent supply of organosilane10.1016/j.diamond.2014.10.010 ↗
9. Multi-layer haemocompatible diamond-like carbon coatings obtained by combined radio frequency plasma enhanced chemical vapor deposition and magnetron sputtering10.1007/s10856-013-5026-y ↗
10. Deposition of diamond-like carbon thin films by the high power impulse magnetron sputtering method10.1016/j.diamond.2017.01.007 ↗
11. History of diamond-like carbon films—From first experiments to worldwide applications10.1016/j.surfcoat.2014.01.031 ↗
12. Coating thickness effects on diamond coated cutting tools10.1016/j.surfcoat.2009.06.011 ↗
13. Diamond-like carbon-coated Ti6Al4V: Influence of the coating thickness on the structure and the abrasive wear resistance10.1016/S0043-1648(01)00587-7 ↗
14. Yang, D. (2016). Applications of Laser Ablation—Thin Film Deposition, Nanomaterial Synthesis and Surface Modification, InTech.10.5772/62615 ↗
15. Pulsed laser deposition of hard and superhard carbon thin films from C60 targets10.1016/j.diamond.2009.10.010 ↗
16. Pulsed laser deposition of diamond-like carbon wear protective coatings: A review10.1016/S0257-8972(97)00007-8 ↗
17. High intensity femtosecond laser deposition of diamond-like carbon thin films10.1063/1.371043 ↗
18. Eason, R. (2007). Pulsed Laser Deposition of Thin Films: Applications-Led Growth of Functional Materials, Wiley.10.1002/0470052120 ↗
19. Reduction of droplet of tantalum oxide using double slit in pulsed laser deposition10.1016/S0042-207X(02)00701-7 ↗
20. Evidence for volume boiling during laser ablation of single crystalline targets10.1016/S0169-4332(98)00608-4 ↗
21. Experimental observations and modeling of nanoparticle formation in laser-produced expanding plasma10.1063/1.2936267 ↗
22. Femtosecond pulsed laser deposition and optical properties of diamond-like amorphous carbon films embedded with SP-bonded carbon chains10.1016/j.diamond.2008.03.024 ↗
23. Plasma-assisted chemical vapor deposition process for depositing smooth diamond coatings on titanium alloys at moderate temperature10.1016/S0925-9635(00)00335-6 ↗
24. Stress and adhesion in DLC coatings on 316L stainless steel deposited by a neutral beam source10.1016/j.jmatprotec.2003.10.003 ↗
25. Interpretation of Raman spectra of disordered and amorphous carbon10.1103/PhysRevB.61.14095 ↗
26. Micro-Raman studies on DLC coatings10.1002/adem.200500006 ↗
27. Spectroscopic analysis of a-C and a-CNx films prepared by ultrafast high repetition rate pulsed laser deposition10.1063/1.1874300 ↗
28. Nanomechanical insights into the deformation behavior of austenitic alloys with different stacking fault energies and austenitic stability10.1016/j.msea.2011.05.068 ↗
29. Fischer-Cripps, A.C. (2011). Nanoindentation, Springer. [3rd ed.].10.1007/978-1-4419-9872-9 ↗
30. The importance of contact radius for substrate independent property measurement of thin films10.1557/PROC-522-27 ↗
31. (2017, October 03). Carbon—Graphite Materials. Available online: https://www.azom.com/properties.aspx?ArticleID=516.
32. Structural and mechanical properties of Ta-C films grown by pulsed laser deposition10.1209/epl/i2000-00297-5 ↗
33. Structure and mechanical properties of low stress tetrahedral amorphous carbon films prepared by pulsed laser deposition10.1140/epjb/e20020031 ↗
34. Laser fluence dependence of the elastic properties of diamond-like carbon films prepared by pulsed-laser deposition10.1016/j.apsusc.2007.01.021 ↗
35. Tribological behavior of diamond-like carbon thin films deposited by the pulse laser technique at different substrate temperatures10.1016/j.triboint.2016.07.013 ↗
36. Influence of Cr content on the micro-structural and tribological properties of PLD grown nanocomposite DLC-Cr thin films10.1016/j.matchemphys.2015.10.031 ↗
37. Enhancing the nanoscratch resistance of pulsed laser deposited DLC films through molybdenum-doping10.1016/j.surfcoat.2017.09.048 ↗
38. Investigating the feasibility of DLC-coated twist drills in deep-hole drilling10.1007/s00170-008-1912-8 ↗
39. Tribological property and drilling application of Ti–C:H and Cr–C:H coatings on high-speed steel substrates10.1016/j.vacuum.2005.10.005 ↗