journal article·2012-01

Analysis of rapid method for the quality index of phenolic resins and benefit

Y. Dong, S. Y. Qu

Publisher page

Abstract

The traditional analytical methods used to determine phenolic resin are slow and produce environmentally unfriendly waste. In this work, Near-infrared (NIR) spectroscopy has been applied for resin content of phenolic resins. The partial least square regression was used to develop the calibration model of the resin content. 8 samples were withdrawn at different time stages for analysis with the proposed quantitative models; the data thus obtained were compared with those provided by reference methods. The maximal predicted error and the standard deviation of the differences were 0.96 and 0.51% for resin content. The results of the paired t -test revealed that there was no significant difference between the NIR method and the reference method. NIR spectroscopy is an effective choice for the accurate, expeditious analyzing quality of phenolic resin.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Spectroscopy and Chemometric Analyses · Cultural Heritage Materials Analysis · Spectroscopy Techniques in Biomedical and Chemical Research

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (10)

Show source-provided references
1. Reghunadhan, N.P., Advances in Addition-Cure Phenolic Resins, Prog. Polym. Sci., 2004, no. 29, pp. 404–410.10.1016/j.progpolymsci.2004.01.004 ↗
2. Mohamed, O., Abdalla, A.L., and Temisha, M., Boron-Modified Phenolic Resins for High Performance Applications, Polymer, 2003, no. 44, pp. 7353–7359.10.1016/j.polymer.2003.09.019 ↗
3. Maurus, B. and Koni, G. Phenolic Resins for Can Coatings: I. Phenol-Based Resole Analysed by GC-MS, GC-GC, NPLC-GC and SEC, LWT-Food. Sci. Techno, 2006, no. 39, pp. 633–646.10.1016/j.lwt.2005.04.008 ↗
4. Sadhra, S., Gray, C.N., and Fouldsi, S., High-Performance Liquid Chromatography of Unmodifed Rosin and Its Applications in Contact Dermatology, J. Chromatography, 1997, no. 700, pp. 101–110.10.1016/S0378-4347(97)00293-4 ↗
5. Smith, P.A., Son, P.S., Callaghan, P.M., Jederberg, W.W., Uhlmann, K.K., and Still, K.R., Sampling and Analysis of Airborne Resin Acids and Solvent-Soluble Material Derived from Heated Colophony (Rosin) Flux: a Method to Quantify Exposure to Sensitizing Compounds Liberated During Electronics Soldering, Toxicology, 1996, no. 111, pp. 225–238.10.1016/0300-483X(96)03379-3 ↗
6. Rodríguez-Guadarrama, L.A., Application of Online Near Infrared Spectroscopy to Study the Kinetics of Anionic Polymerization of Butadiene, Euro. Polym. J., 2007, no. 43, pp. 928–937.10.1016/j.eurpolymj.2006.12.026 ↗
7. Garrido, M., Larrechi, M.S., and Rius, F.X., Validation of the Concentration Profiles Obtained from the Near Infrared/Multivariate Curve Resolution Monitoring of Reactions of Epoxy Resins Using High Performance Liquid Chromatography As a Reference Method, Anal. Chimi. Acta, 2007, no. 585, pp. 277–285.10.1016/j.aca.2007.01.006 ↗
8. Blanco, M. and Villaescusa, V., Use of NIR Spectroscopy in the Production of Modified Industrial Resins, Talanta, 2007, no. 71, pp. 1333–1338.10.1016/j.talanta.2006.07.028 ↗
9. Marengoa, E., Bobbaa, M., and Robotti, E., Hydroxyl and Acid Number Prediction in Polyester Resins by Near Infrared Spectroscopy and Artificial Neural Networks, Anal. Chim. Acta, 2004, no. 511, pp. 313–322.10.1016/j.aca.2004.01.053 ↗
10. Judge, M.D., The Application of Near-Infrared Spectroscopy for the Quality Control Analysis of Rocket Propellant Fuel Pre-Mixes, Talanta, 2004, no. 62, pp. 675–679.10.1016/j.talanta.2003.08.037 ↗