journal article·2026-06-05Open access

Interlaboratory study on low-temperature testing of asphalt binders using the dynamic shear rheometer in Germany

Johannes Büchner, Nina Nytus, Michael P. Wistuba

Abstract

In 2023, a comprehensive interlaboratory study was conducted to analyse low-temperature asphalt binder characterisation in the dynamic shear rheometer (DSR). Participants from 17 German laboratories with 20 DSR devices from two manufacturers tested three representative asphalt binders (70/100, 10/40–65 and 40/100–165). The study included two approaches: temperature-frequency sweeps with 4 mm parallel-plate geometry from −30°C to 0°C and shear relaxation tests with 8 mm plates at −10°C. Key parameters such as the complex shear modulus (G*), the phase angle (δ), the relaxation viscosity (λREL) and the relaxation capacity (RELSRV) were extracted and statistically analysed in accordance with ISO 5725-2 standard. The results showed good repeatability within laboratories, regardless of instrument type. However, interlaboratory reproducibility was limited, primarily due to operator-related variability and calibration practices. Despite these challenges, both test protocols enabled consistent differentiation of asphalt binders and offer material-efficient, DSR-based alternatives to BBR testing.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Asphalt Pavement Performance Evaluation · Rheology and Fluid Dynamics Studies · Innovations in Concrete and Construction Materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Technische Universität Braunschweig

Ruhr University Bochum

Funding

German Road and Transportation Research Association

References (30)

Show source-provided references
1. 10.1617/s11527-020-01610-910.1617/s11527-020-01610-9 ↗
2. 10.1016/j.conbuildmat.2022.12992910.1016/j.conbuildmat.2022.129929 ↗
3. 10.24355/dbbs.084-202103181558-010.24355/dbbs.084-202103181558-0 ↗
4. Büchner J. & Wistuba M. P. (2022). Analysis of low temperature relaxation properties of asphalt binder and asphalt mastic using a dynamic shear rheometer. In I. Hoff H. Mork & R. Saba (Eds.) Eleventh international conference on the bearing capacity of roads railways and airfields 2. Proceedings of the June 28-30 2022 Trondheim Norway (pp. 508–516). CRC Press. https://doi.org/10.1201/9781003222897-4710.1201/9781003222897-47 ↗
5. 10.1080/14680629.2020.185129110.1080/14680629.2020.1851291 ↗
6. 10.1617/s11527-019-1412-310.1617/s11527-019-1412-3 ↗
7. 10.1515/ijpeat-2015-000410.1515/ijpeat-2015-0004 ↗
8. Elwardany, M. D., Planche, J.-P., & Adams, J. J. (2022). Sensitivity analysis for rheological determination of glass transition and crossover temperatures at various reference frequenciesH. Di Benedetto, H. Baaj, E. Chailleux, G. Tebaldi, C. Sauzéat, & S. Mangiafico (Eds.)Proceedings of the RILEM international symposium on bituminous materials: ISBM Lyon 2020, RILEM bookseries 27. December 14 - 16, 2020. https://doi.org/10.1007/978-3-030-46455-4_210
9. EN 14770. (2023). Bitumen and bituminous binders - Determination of complex shear modulus and phase angle using a Dynamic Shear Rheometer (DSR). European Committee for Standardization (CEN).
10. EN 14771. (2023). Bitumen and bituminous binders – Determination of the flexural creep stiffness –­ Bending Beam Rheometer (BBR). European Committee for Standardization (CEN).
11. EN 17643. (2022). Bitumen and bituminous binders – Determination of equi-shear modulus temperature and phase angle using a Dynamic Shear Rheometer (DSR) – BTSV test. European Committee for Standardization (CEN).
12. Gražulytė J. (2019). Bitumen stress relaxation modulus as an indicator of asphalt pavements resistance to low temperature cracking [Dissertation]. Vilniaus Gedimino technikos universiteto.
13. 10.1177/036119811985533210.1177/0361198119855332 ↗
14. ISO 5725-2. (2019). Accuracy (trueness and precision) of measurement methods and results – Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method. International Organization for Standardization (ISO).
15. 10.3389/fmats.2022.83144310.3389/fmats.2022.831443 ↗
16. 10.1520/JTE2021027710.1520/JTE20210277 ↗
17. 10.1016/j.conbuildmat.2018.05.16010.1016/j.conbuildmat.2018.05.160 ↗
18. 10.1016/j.ijprt.2016.08.01010.1016/j.ijprt.2016.08.010 ↗
19. 10.1016/j.conbuildmat.2022.13020210.1016/j.conbuildmat.2022.130202 ↗
20. Radenberg, M., & Staschkiewicz, M. (2021). Development of a test method to determine the low temperature performance of Bitumen. 7th E&E congress proceedings., Madrid, 16–18 June, 2021.
21. 10.1016/j.jclepro.2023.13909210.1016/j.jclepro.2023.139092 ↗
22. Riccardi, C., Cannone Falchetto, A., Wistuba, M. P., & Losa, M. (2017). Comparison of DSR and BBR tests for determining the Performance Grade (PG) of asphalt binder at low temperature. In A. Loizos, I. L. Al-Qadi, & T. Scarpas (Eds.), Bearing capacity of roads, railways and airfields. Proceedings of the 10th international conference on the bearing capacity of roads, railways and airfields, 28–30 June 2017, Athens (pp. 267–271). CRC Press.10.1201/9781315100333-35 ↗
23. Santosh, K., & Kim, Y.-R. (2019). Investigation of DSR test methods to determine binder low temperature properties: Final Report 26-1121-4041-001. Nebraska Department of Transportation (NDOT).
24. 10.24355/dbbs.084-202110271159-010.24355/dbbs.084-202110271159-0 ↗
25. 10.1080/14680629.2025.248284410.1080/14680629.2025.2482844 ↗
26. 10.1080/10298436.2023.229793210.1080/10298436.2023.2297932 ↗
27. 10.3141/2207-0610.3141/2207-06 ↗
28. TL Bitumen-StB. (2025). Technische Lieferbedingungen für Straßenbaubitumen und gebrauchsfertige Polymermodifizierte Bitumen. Forschungsgesellschaft für Straßen- und Verkehrswesen (FGSV). FGSV Verlag.
29. 10.1177/036119811983491210.1177/0361198119834912 ↗
30. 10.1016/j.conbuildmat.2020.11939610.1016/j.conbuildmat.2020.119396 ↗