journal article·2021-12

HF-free and fast fabrication of long, rectangular microchannels in fused silica: Novel femtosecond laser irradiation geometry

Rajasimha Kurnoothala, Krishna Chaitanya Vishnubhatla, Shailesh Srivastava

Optical Materials· Volume 122
Publisher page

Abstract

Abstract We report the fabrication of truly rectangular buried microchannels of record lengths in fused silica, using a novel femtosecond laser irradiation geometry, at 1030 nm, followed by chemical etching in hot KOH alone. As the result of a judicious choice of the laser parameters and writing geometry, an effective chemical etching rate of 500 μm per hour in the laser irradiated region is achieved, competing with the traditional and hazardous HF based etching, and faster than all earlier reports with KOH. This has resulted in the longest reported (6 mm) rectangular, microchannels, in a record etching time of 6 h. Linear and Cross microchannels have been fabricated with mean surface roughness less than 200 nm of the sidewalls. These results have been validated using an optical microscope, SEM and AFM imaging. The use of fused silica, the much eased safety concerns with KOH, the simplicity of our method, together with the enhanced ability to image from the top surface of smooth, rectangular, buried micro-channels, will motivate microfluidics for Optofluidic lab-on-chip applications, especially for biomedical diagnostics.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Laser Material Processing Techniques · Laser-induced spectroscopy and plasma · Advanced Surface Polishing Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (48)

Show source-provided references
1. Micromachining a miniaturized capillary electrophoresis-based chemical analysis system on a chip10.1126/science.261.5123.895 ↗
2. Ultra-high-speed DNA fragment separations using microfabricated capillary array electrophoresis chips10.1073/pnas.91.24.11348 ↗
3. High-speed separations on a microchip10.1021/ac00079a029 ↗
4. Integrated microdevice for DNA restriction fragment analysis10.1021/ac951230c ↗
5. Control and detection of chemical reactions in microfluidic systems10.1038/nature05062 ↗
6. Microfluidic diagnostic technologies for global public health10.1038/nature05064 ↗
7. The capability of ECDM in creating effective microchannel on the PDMS10.1016/j.precisioneng.2020.11.004 ↗
8. Experimental investigations and analytical modeling of multi-pass CO2 laser processing on PMMA10.1016/j.precisioneng.2017.02.010 ↗
9. Serial immunoassays in parallel on a microfluidic chip for monitoring hormone secretion from living cells10.1021/ac061425s ↗
10. Femtosecond laser microstructuring: an enabling tool for optofluidic lab-on-chips10.1002/lpor.201000031 ↗
11. Fabrication and multifunction integration of microfluidic chips by femtosecond laser direct writing10.1039/c3lc50160d ↗
12. Applications of femtosecond laser induced self-organized planar nanocracks inside fused silica glass10.1002/lpor.200710031 ↗
13. Writing waveguides in glass with a femtosecond laser
14. Infrared photosensitivity in silica glasses exposed to femtosecond laser pulses10.1364/OL.24.001311 ↗
15. Nucci · 2014
16. Femtosecond laser fabricated monolithic chip for optical trapping and stretching of single cells
17. Optofluidic chip for single cell trapping and stretching fabricated by a femtosecond laser10.1002/jbio.201000011 ↗
18. A 3D mammalian cell separator biochip10.1039/c2lc20939j ↗
19. Monolithic cell counter based on 3D hydrodynamic focusing in microfluidic channels
20. Femtosecond laser fabrication of microfluidic channels for organic photonic devices
21. Ultrafast optofluidic gain switch based on conjugated polymer in femtosecond laser fabricated microchannels10.1063/1.3076120 ↗
22. Fabrication of microchannels in glass using focused femtosecond laser radiation and selective chemical etching10.1007/s00339-006-3590-4 ↗
23. Polarization-selective etching in femtosecond laser-assisted microfluidic channel fabrication in fused silica10.1364/OL.30.001867 ↗
24. Towards fast femtosecond laser micromachining of glass, effect of deposited energy
25. Fabrication of long microchannels with circular cross section using astigmatically shaped femtosecond laser pulses and chemical etching10.1063/1.2203335 ↗
26. Femtosecond laser-assisted three-dimensional microfabrication10.1364/OL.26.000277 ↗
27. Control of the cross-sectional shape of a hollow microchannel embedded in photostructurable glass by use of a femtosecond laser10.1364/OL.28.000055 ↗
28. Three-dimensional micromachining of glass using femtosecond laser for lab-on-a-chip device manufacture10.1007/s00339-005-3225-1 ↗
29. Femtosecond laser micromachining in transparent materials10.1038/nphoton.2008.47 ↗
30. Examination of etching agent and etching mechanism on femotosecond laser microfabrication of channels inside vitreous silica substrates10.1021/jp900915r ↗
31. Laser-inscribed glass microfluidic device for non-mixing flow of miscible solvents
32. Fabrication of high-aspect ratio, micro-fluidic channels and tunnels using femtosecond laser pulses and chemical etching10.1364/OPEX.12.002120 ↗
33. Shape control of microchannels fabricated in fused silica by femtosecond laser irradiation and chemical etching10.1364/OE.17.008685 ↗
34. Hybrid chemical etching of femtosecond laser irradiated structures for engineered microfluidic devices10.1088/0960-1317/23/8/085002 ↗
35. Single- and multi-scan femtosecond laser writing for selective chemical etching of cross section patternable glass micro-channels10.1007/s00339-011-6675-7 ↗
36. Selective, laser-induced etching of fused silica at high scan-speeds using KOH10.2961/jlmn.2014.02.0009 ↗
37. Optimization of selective laser-induced etching (SLE) for fabrication of 3D glass microfluidic device with multi-layer micro channels10.1186/s40486-019-0094-5 ↗
38. Femtosecond laser induced selective etching in fused silica: optimization of the inscription conditions with a high-repetition-rate laser source10.1364/OE.26.029669 ↗
39. Fabrication of microchannels in fused silica using femtosecond Bessel beams10.1063/1.4929649 ↗
40. Femtosecond laser micromachining_ photonic and microfluidic devices in transaprent materials
41. Facile fabrication of integrated microfluidic SERS substrate by femtosecond laser sintering of silver nano particles10.1016/j.optmat.2020.110518 ↗
42. Selective laser-induced etching of 3D precision quartz glass components for microfluidic applications-up-scaling of complexity and speed10.3390/mi8040110 ↗
43. KOH Etching (byu.Edu).
44. Single femtosecond laser beam induced nanogratings in transparent media - mechanisms and applications
45. Ultra-sensitive nanofiber fluorescence detection in a microfluidic chip10.3390/s150304890 ↗
46. Microfluidic surface plasmon resonance sensors: from principles to point-of-care applications
47. Localized surface plasmon resonance biosensor integrated with microfluidic chip10.1007/s10544-009-9306-8 ↗
48. Portable microfluidic integrated plasmonic platform for pathogen detection10.1038/srep09152 ↗