Simultaneously enhanced strength and ductility for 3D-printed stainless steel 316L by selective laser melting
Source abstract
Abstract
Laser-based powder-bed fusion additive manufacturing or three-dimensional printing technology has gained tremendous attention due to its controllable, digital, and automated manufacturing process, which can afford a refined microstructure and superior strength. However, it is a major challenge to additively manufacture metal parts with satisfactory ductility and toughness. Here we report a novel selective laser melting process to simultaneously enhance the strength and ductility of stainless steel 316L by in-process engineering its microstructure into a <011> crystallographic texture. We find that the tensile strength and ductility of SLM-built stainless steel 316L samples could be enhanced by ~16% and ~40% respectively, with the engineered <011> textured microstructure compared to the common <001> textured microstructure. This is because the favorable nano-twinning mechanism was significantly more activated in the <011> textured stainless steel 316L samples during plastic deformation. In addition, kinetic simulations were performed to unveil the relationship between the melt pool geometry and crystallographic texture. The new additive manufacturing strategy of engineering the crystallographic texture can be applied to other metals and alloys with twinning-induced plasticity. This work paves the way to additively manufacture metal parts with high strength and high ductility. A steel alloy with both high tensile strength and ductility has been three-dimensional (3D) printed by researchers in Singapore. Additive manufacturing builds 3D objects by adding materials layer by layer, a relatively simple process for plastics. However, this manufacturing process is much more difficult for metals, which are susceptible to defects and internal pores. This is particularly problematic when the final product needs excellent mechanical properties, such as hardness or strength. Xipeng Tan and co-workers from Nanyang Technological University used a specific laser scanning strategy to melt metallic powders and form a stainless steel alloy with a zig-zag crystallographic microstructure. The tensile strength and ductility of their stainless steel samples were increased by approximately 16% and 40%, respectively, compared to an alloy with the typical microstructure. A creative approach to substantially enhance both the strength and ductility of SLM-printed metal parts was successfully demonstrated on the ubiquitous marine-grade stainless steel 316L. The new discovery improves the strength and ductility of stainless steel parts by ~16% and 40% compared with the typical 3D printing process and conventional manufacturing methods. Control of the crystallographic texture is key for this breakthrough, which was achieved by tailoring the geometrical features of the melt pool involved in the laser-based 3D printing process. The desired <011> crystallographic texture favors the activation of the nano-twinning mechanism, which simultaneously enhances the strength and ductility.
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Research context
OpenAlex topics: Additive Manufacturing Materials and Processes · Additive Manufacturing and 3D Printing Technologies · High Entropy Alloys Studies
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (45)
Show source-provided references
1. Martin, J. H. et al. 3D printing of high-strength aluminium alloys. Nature 549, 365–369 (2017).10.1038/nature23894 ↗
2. Tan, X. et al. Revealing martensitic transformation and α/β interface evolution in electron beam three-dimensional-printed Ti-6Al-4V. Sci. Rep. 6, 26039 (2016).10.1038/srep26039 ↗
3. Geiger, F., Kunze, K. & Etter, T. Tailoring the texture of IN738LC processed by selective laser melting (SLM) by specific scanning strategies. Mater. Sci. Eng. A 661, 240–246 (2016).10.1016/j.msea.2016.03.036 ↗
4. Frazier, W. E. Metal additive manufacturing: a review. J. Mater. Eng. Perform. 23, 1917–1928 (2014).10.1007/s11665-014-0958-z ↗
5. Tan, X. et al. Graded microsctructure and mechanical properties of additive manufactured Ti-6Al-4V via electron beam melting. Acta Mater. 97, 1–16 (2015).10.1016/j.actamat.2015.06.036 ↗
6. Vrancken, B., Thijs, L., Kruth, J.-P. & Van Humbeeck, J. Heat treatment of Ti6Al4V produced by selective laser melting: microstructure and mechanical properties. J. Alloy. Compd. 541, 177–185 (2012).10.1016/j.jallcom.2012.07.022 ↗
7. Lam, L. P. et al. Phase analysis and microstructure characterisation of AlSi10Mg parts produced by selective laser melting. Virtual Phys. Prototyp. 10, 207–215 (2015).10.1080/17452759.2015.1110868 ↗
8. Xu, W. et al. Additive manufacturing of strong and ductile Ti–6Al–4V by selective laser melting via in situ martensite decomposition. Acta Mater. 85, 74–84 (2015).10.1016/j.actamat.2014.11.028 ↗
9. Mumtaz, K. A., Erasenthiran, P. & Hopkinson, N. High density selective laser melting of Waspaloy®. J. Mater. Process. Technol. 195, 77–87 (2008).10.1016/j.jmatprotec.2007.04.117 ↗
10. Kunze, K., Etter, T., Grässlin, J. & Shklover, V. Texture, anisotropy in microstructure and mechanical properties of IN738LC alloy processed by selective laser melting (SLM). Mater. Sci. Eng. A 620, 213–222 (2015).10.1016/j.msea.2014.10.003 ↗
11. Sun, Z., Tan, X., Tor, S. B. & Yeong, W. Y. Selective laser melting of stainless steel 316L with low porosity and high build rates. Mater. Des. 104, 197–204 (2016).10.1016/j.matdes.2016.05.035 ↗
12. Ishimoto, T., Hagihara, K., Hisamoto, K., Sun, S.-H. & Nakano, T. Crystallographic texture control of beta-type Ti–15Mo–5Zr–3Al alloy by selective laser melting for the development of novel implants with a biocompatible low Young’s modulus. Scr. Mater. 132, 34–38 (2017).10.1016/j.scriptamat.2016.12.038 ↗
13. Haase, C. et al. Exploiting process-related advantages of selective laser melting for the production of high-manganese steel. Materials 10, 56 (2017).10.3390/ma10010056 ↗
14. Zhou, X. et al. Textures formed in a CoCrMo alloy by selective laser melting. J. Alloy. Compd. 631, 153–164 (2015).10.1016/j.jallcom.2015.01.096 ↗
15. Thijs, L. et al. Strong morphological and crystallographic texture and resulting yield strength anisotropy in selective laser melted tantalum. Acta Mater. 61, 4657–4668 (2013).10.1016/j.actamat.2013.04.036 ↗
16. Carter, L. N., Martin, C., Withers, P. J. & Attallah, M. M. The influence of the laser scan strategy on grain structure and cracking behaviour in SLM powder-bed fabricated nickel superalloy. J. Alloy. Compd. 615, 338–347 (2014).10.1016/j.jallcom.2014.06.172 ↗
17. Thijs, L., Verhaeghe, F., Craeghs, T., Humbeeck, J. V. & Kruth, J.-P. A study of the microstructural evolution during selective laser melting of Ti–6Al–4V. Acta Mater. 58, 3303–3312 (2010).10.1016/j.actamat.2010.02.004 ↗
18. Yu, Q. et al. Strong crystal size effect on deformation twinning. Nature 463, 335–338 (2010).10.1038/nature08692 ↗
19. Wei, Y. et al. Evading the strength–ductility trade-off dilemma in steel through gradient hierarchical nanotwins. Nat. Commun. 5, 3580 (2014).10.1038/ncomms4580 ↗
20. Li, Z., Pradeep, K. G., Deng, Y., Raabe, D. & Tasan, C. C. Metastable high-entropy dual-phase alloys overcome the strength–ductility trade-off. Nature 534, 227–230 (2016).10.1038/nature17981 ↗
21. Lu, K., Lu, L. & Suresh, S. Strengthening materials by engineering coherent internal boundaries at the nanoscale. Science 324, 349–352 (2009).10.1126/science.1159610 ↗
22. Riemer, A. et al. On the fatigue crack growth behavior in 316L stainless steel manufactured by selective laser melting. Eng. Fract. Mech. 120, 15–25 (2014).10.1016/j.engfracmech.2014.03.008 ↗
23. Yan, C., Hao, L., Hussein, A., Young, P. & Raymont, D. Advanced lightweight 316L stainless steel cellular lattice structures fabricated via selective laser melting. Mater. Des. 55, 533–541 (2014).10.1016/j.matdes.2013.10.027 ↗
24. Obrtlík, K., Kruml, T. & Polák, J. Dislocation structures in 316L stainless steel cycled with plastic strain amplitudes over a wide interval. Mater. Sci. Eng. A 187, 1–9 (1994).10.1016/0921-5093(94)90325-5 ↗
25. Plimpton, S., et al. Crossing the Mesoscale No-Man’s Land via Parallel kinetic Monte Carlo. Sandia Report SAND2009-6226, Sandia National Laboratories, Albuquerque, NM 87185-1316, (2009).
26. Rodgers, T. M., Madison, J. D., Tikare, V. & Maguire, M. C. Predicting mesoscale microstructural evolution in electron beam welding. JOM 68, 1419–1426 (2016).10.1007/s11837-016-1863-8 ↗
27. Bachmann, F., Hielscher, R. & Schaeben, H. Texture Analysis with MTEX – Free and Open Source Software Toolbox., in Solid State Phenomena, edited by Klein, A. & Schwarzer, R.A. Trans. Tech. Publ., Switzerland, Vol. 160, pp. 63-68 (2010).10.4028/www.scientific.net/SSP.160.63 ↗
28. ASTM A240/A240M-16a. Standard Specification for Chromium and Chromium-nickel Stainless Steel Plate, Sheet, and Strip for Pressure Vessels and for General Applications. ASTM International, West Conshohocken, PA, 2016. ( http://www.astm.org ).
29. Ya, M., Xing, Y., Dai, F., Lu, K. & Lu, J. Study of residual stress in surface nanostructured AISI 316L stainless steel using two mechanical methods. Surf. Coat. Technol. 168, 148–155 (2003).10.1016/S0257-8972(03)00254-8 ↗
30. Laplanche, G., Kostka, A., Horst, O. M., Eggeler, G. & George, E. P. Microstructure evolution and critical stress for twinning in the CrMnFeCoNi high-entropy alloy. Acta Mater. 118, 152–163 (2016).10.1016/j.actamat.2016.07.038 ↗
31. El-Danaf, E., Kalidindi, S. R. & Doherty, R. D. Influence of grain size and stacking-fault energy on deformation twinning in fcc metals. Metall. Mater. Trans. A 30, 1223–1233 (1999).10.1007/s11661-999-0272-9 ↗
32. Byun, T. S. On the stress dependence of partial dislocation separation and deformation microstructure in austenitic stainless steels. Acta Mater. 51, 3063–3071 (2003).10.1016/S1359-6454(03)00117-4 ↗
33. Rosa, D. M., Spinelli, J. E., Ferreira, I. L. & Garcia, A. Cellular/dendritic transition and microstructure evolution during transient directional solidification of Pb-Sb alloys. Metall. Mater. Trans. A 39, 2161–2174 (2008).10.1007/s11661-008-9542-1 ↗
34. Zhang, K., Zou, J., Grosdidier, T., Dong, C. & Yang, D. Improved pitting corrosion resistance of AISI 316L stainless steel treated by high current pulsed electron beam. Surf. Coat. Technol. 201, 1393–1400 (2006).10.1016/j.surfcoat.2006.02.008 ↗
35. Liu, W. & DuPont, J. N. Effects of melt-pool geometry on crystal growth and microstructure development in laser surface-melted superalloy single crystals. Acta Mater. 52, 4833–4847 (2004).
36. Niendorf, T. et al. Highly anisotropic steel processed by selective laser melting. Metall. Mater. Trans. B 44, 794–796 (2013).10.1007/s11663-013-9875-z ↗
37. Gutierrez-Urrutia, I., Zaefferer, S. & Raabe, D. The effect of grain size and grain orientation on deformation twinning in a Fe–22wt.% Mn–0.6wt.% C TWIP steel. Mater. Sci. Eng. A 527, 3552–3560 (2010).10.1016/j.msea.2010.02.041 ↗
38. Beladi, H. et al. Orientation dependence of twinning and strain hardening behaviour of a high manganese twinning induced plasticity steel with polycrystalline structure. Acta Mater. 59, 7787–7799 (2011).10.1016/j.actamat.2011.08.031 ↗
39. Yang, P., Xie, Q., Meng, L., Ding, H. & Tang, Z. Dependence of deformation twinning on grain orientation in a high manganese steel. Scr. Mater. 55, 629–631 (2006).10.1016/j.scriptamat.2006.06.004 ↗
40. Karaman, I., Sehitoglu, H., Gall, K., Chumlyakov, Y. I. & Maier, H. Deformation of single crystal Hadfield steel by twinning and slip. Acta Mater. 48, 1345–1359 (2000).10.1016/S1359-6454(99)00383-3 ↗
41. Christian, J. W. & Mahajan, S. Deformation twinning. Prog. Mater. Sci. 39, 1–157 (1995).10.1016/0079-6425(94)00007-7 ↗
42. Wang, Y., et al. Additively manufactured hierarchical stainless steels with high strength and ductility. Nat. Mater. 17, 63–71 (2017).10.1038/nmat5021 ↗
43. Liu, L., et al. Dislocation network in additive manufactured steel breaks strength-ductility trade-off. Mater. Today, in press (2018).10.1016/j.mattod.2017.11.004 ↗
44. Salmi, A. & Atzeni, E. History of residual stresses durin gthe production phases of AlSi10Mg parts processed by powder bed additive manufacturing technology. Virtual Phys. Prototyp. 12, 153–160 (2017).10.1080/17452759.2017.1310439 ↗
45. Yadroitsev, I., Gusarov, A., Yadroitsava, I. & Smurov, I. Single track formation in selective laser melting of metal powders. J. Mater. Process. Technol. 210, 1624–1631 (2010).10.1016/j.jmatprotec.2010.05.010 ↗