Response surface methodology optimization and anti-age properties in paper protection of carboxymethyl cellulose grafted with β –cyclodextrin
Source abstract
Abstract
Abstract In order to protect the paper, increase the mechanic performance and delay the aging of paper, CMC- β -CD was synthesized by carboxymethyl cellulose as substrate, epichlorohydrin (ECH) as crosslinking agent, sodium hydroxide (NaOH) as catalyst and solvent, and water as medium, β -Cyclodextrin as grafter, through single factor experiment and response surface method, suitable conditions for the synthesis of CMC- β -CD was obtained; The structure of the synthesized CMC- β -CD was characterized by infrared spectroscopy and SEM and the mechanic properties were evaluated. The results showed that when the mass ratio of CMC- β -CD was 7:15, reaction temperature was 40 °C, and pH was 6.0, the optimum synthetic conditions was obtained. And good anti-age properties was also obtained by thermal aging tests. This paper provides some theoretical guidance for the protection of paper cultural relics.
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Research context
OpenAlex topics: Advanced Cellulose Research Studies · Cultural Heritage Materials Analysis · Material Properties and Processing
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
School of Chemical Engineering , Zhengzhou University , Zhengzhou , 450001 , China
References (28)
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