Preparation of CMC-β-CD-sulfaguanidine and its application for protection of paper
Source abstract
Abstract
Abstract CMC-β-CD-sulfaguanidine was synthesized by saturated aqueous solution method with β-CD as carrier and sulfaguanidine as inclusion compounds based on the preparation of CMC-β-CD, through single factor and orthogonal experiment, suitable conditions for the synthesis of CMC-β-CD-sulfaguanidine was obtained. The structure of the synthesized CMC-β-CD-sulfaguanidine was characterized by infrared spectroscopy, UV spectroscopy and SEM. The inclusion compounds was applied to paper reinforcement. By testing the effects of different mass concentrations of sulfaguanidine solution on the tensile strength, tearing strength, folding times, whiteness, glossiness and antibacterial properties of the paper, the suitable conditions for coating paper were found. The results show that when inclusion concentration of 3 mg/mL is coated on the paper, its mechanical properties are improved, the glossiness is slightly increased, and the whiteness is basically unchanged, at the same time, the paper has certain antibacterial properties. CMC-β-CD-SG studied in this paper has the functions of strengthening, slow-releasing, anti-mildew and antibacterial for paper, which is an innovation of paper protection material, provides the theoretical basis and data reference, as well as a new research idea and technical approach for the development of products for paper protection.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Advanced Cellulose Research Studies · Enzyme-mediated dye degradation · Biopolymer Synthesis and Applications
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
School of Chemical Engineering , Zhengzhou University , Zhengzhou 450001 , China
School of Mechanical and Power Engineering , Zhengzhou University , Zhengzhou , China
References (22)
Show source-provided references
1. Cao, X.Z. and Jin, Z.Y. (2003). Method for the preparation of cyclodextrin inclusion compounds. Food Ind. Sci. Technol. 2003: 158–160.
2. Chen, L., Chao, J.B., and Ma, L.H. (2000). Preparation of hydroxypropyl cyclodextrin solid encapsulants of haloperidol and study of their properties. Chin. J. Magn. Reson. 17: 203–210.
3. Dresler, C., Saladino, M.L., Demirbag, C., Caponetti, E., Chillura Martino, D.F., and Alduina, R. (2017). Development of controlled release systems of biocides for conservation of cultural heritage. Int. Biodeterior. Biodegrad. 125: 150–156, https://doi.org/10.1016/j.ibiod.2017.09.007.10.1016/j.ibiod.2017.09.007 ↗
4. Feng, Z.Z., Qi, Y.P., Hou, A.Q., Li, Y., Yu, Y.F., and Zhan, Y.Z. (2020). Study on cellulose solution reinforced deteriorated paper. China Adhesives 29: 33–37.
5. Girardi, F., Bergamonti, L., Isca, C., Predieri, G., Graff, C., Lottici, P.P., Cappelletto, E., Ataollahi, N., and Di Maggio, R. (2017). Chemical-physical characterization of ancient paper with functionalized polyamidoamines (PAAS). Cellulose 24: 1057–1068, https://doi.org/10.1007/s10570-016-1159-8.10.1007/s10570-016-1159-8 ↗
6. Gong, W.Q., Mu, H.L., and Hao, H.Y. (2015). Preparation and bacteriostatic effect of carvacro-β-cyclodextrin inclusion compound. Chin. J. Food Sci. 15: 114–119.
7. He, L., Liu, Y., and Wen, X.Y. (2021). Preparation, evaluation and characterization of netopytam/β-cyclodextrin inclusion complexes. Adv. Modern Bio-Med. 21: 233–238.
8. Huang, X.S., Lin, S.M., Lin, N.T., Li, P.R., and Li, D.W. (2021). Exploration of the inclusion process of lemongrass volatile oil with β-cyclodextrin. Guangdong Chem. Ind. 48: 36–37.
9. Li, Z.P., OuYang, Y.Z., and Zhang, A.H. (2003). Preparation and bacteriostatic study of berberine β-cyclodextrin inclusion compound. Fine Chem. Intermed. 46–48+63.
10. Li, F., Mao, Y., and Wang, Y. (2013). Preparation of the inclusion complex of Natamycin-hydroxypropyl-β-cyclodextrin and its antibacterial properties. Chin. Food Addit.: 127–131.
11. Lisuzzo, L., Cavallaro, G., Milioto, S., and Lazzara, G. (2021). Halloysite nanotubes filled with MgO for paper reinforcement and deacidification. Appl. Clay Sci. 213: 106231, https://doi.org/10.1016/j.clay.2021.106231.10.1016/j.clay.2021.106231 ↗
12. Lu, P. (2022). Preparation and application of carboxymethyl cellulose grafted β-cyclodextrin encapsulated sulfaguanidine. Zhengzhou University, Zhengzhou.
13. Oh, S.Y., Yoo, D.I., Shin, Y., Kim, H.C., Kim, H.Y., Chung, Y.S., Park, W.H., and Youk, J.H. (2005). Crystalline structure analysis of cellulose treated with sodium hydroxide and carbon dioxide by means of X-ray diffraction and FTIR spectroscopy. Carbohydr. Res. 340: 2376–2391, https://doi.org/10.1016/j.carres.2005.08.007.10.1016/j.carres.2005.08.007 ↗
14. Poggi, G., Sistach, M.C., Marin, E., Garcia, J.F., Giorgi, R., and Baglioni, P. (2016). Calcium hydroxide nanoparticles in hydroalcoholic gelatin solutions (GeolNan) for the deacidification and strengthening of papers containing iron gall ink. J. Cult. Herit. 18: 250–257, https://doi.org/10.1016/j.culher.2015.10.005.10.1016/j.culher.2015.10.005 ↗
15. Sun, M., Wang, J., Zhang, H., Zhang, B., Fan, Z., and Su, B. (2015). Measurement of the reversible rate of conservation materials for ancient murals. J. Cult. Herit. 16: 49–56, https://doi.org/10.1016/j.culher.2014.01.010.10.1016/j.culher.2014.01.010 ↗
16. Wang, X.M. (2020). Research on the reinforcement and protection of paper by epoxycyclohexane-modified chitosan. Zhengzhou University, ZhengZhou.
17. Wang, Y., Mao, Y., and Li, F. (2013). Study on antibacterial activity and stability of Natamycin-hydroxypropyl-β-cyclodextrin inclusion complex. Food Ind. Sci. Technol. 34: 285–289.
18. Zhang, L. (2013). Preparation and performance evaluation of a new organoguanidine fungicide. J. Chem. Ind. 27: 27–29.
19. Zhao, G.W., Liao, Z.G., Liang, X.L., and Zhan, X.H. (2009). Preparation of Mucuna pruriens volatile oil/β-cyclodextrin inclusion compounds by saturated solution method. Jiangxi Tradit. Chin. Med. 40: 73–75.
20. Zhao, N., Li, W.Z., Fu, L.N., Shi, J.J., and Zhang, Z.R. (2021). Preparation of hydroxypropyl-β-cyclodextrin inclusion compounds for aspirin. Chem. Technol. 29: 11–15.
21. Zhong, W.J., Shi, L., and Liu, Y.L. (2021). Preparation and characterization of β-cyclodextrin inclusion compounds of aniridiazetan. China Med. Herald 18: 31–34.
22. Zhou, Y.X., Tang, M.L., and Yin, H.A. (2006). Preparation of volatile oil-β-cyclodextrin inclusion compounds of Rhizoma Atractylodis Macrocephala and Rhizoma Atractylodis Macrocephala. Guangzhou Chem. 31: 20–23+36.