journal article·2005-03-01Open access

Measuring the surface stress polar dependence

J. J. Métois, A. Saúl, P. Müller

Nature Materials· Volume 4· Issue 3

Abstract

While measurements of the polar dependence of the surface free energy are easily available, measurements of the whole polar dependence of the surface stress of a crystal do not exist. In this paper is presented a new procedure that allows, for the first time, the experimental determination of the surface stress polar dependence of a crystal. For this purpose (1) electromigration is used to control the kinetic faceting of surface orientations that belong to the equilibrium shape of the crystal and (2) for each destabilised surface, the period of faceting as well as the crystallographic angles of the appearing facets are measured by AFM. The so-obtained data lead to a set of equations whose mathematical solution, compatible with physical constraints, gives access to the surface stress polar dependence of the whole crystal and thus to a better understanding of surface stress properties.
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Research context

OpenAlex topics: Force Microscopy Techniques and Applications · Surface and Thin Film Phenomena · Copper Interconnects and Reliability

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