journal article·2004

Synthesis of carbon nanotubes from a chlorine-containing precursor and their properties

S.Ya. Brichka, G.P. Prikhod'ko, Yu.I. Sementsov, A.V. Brichka, G.I. Dovbeshko, O.P. Paschuk

Carbon· Volume 42· Issue 12-13
Publisher page

Abstract

Abstract A template method for the synthesis of multi-wall carbon nanotubes from dichloromethane was investigated. The use of a non-thermally stable precursor allows for a low synthesis temperature (250 °C) in comparison with acetylene synthesis. Carbon nanotubes of different structure could be synthesised using different matrix geometries. Electron spectroscopy used for chemical analysis shows that the carbon nanotubes consist of carbon, oxygen (14.3 at.%), chlorine (0.25 at.%). The material has been characterised by surface enhanced IR spectroscopy in the reflectance-absorbance mode, and temperature-programmed desorption with mass-spectrometry control. The vibrations of CO, CC, CO, CC molecular groups as well as the collective modes of large entities containing these groups have been recorded.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Carbon Nanotubes in Composites · Fullerene Chemistry and Applications · Graphene research and applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (27)

Show source-provided references
1. Nanoparticles of layered compounds with hollow cage structures (inorganic fullerene-like structures)10.1021/cm9802189 ↗
2. Fullerenes, nanotubes, onions and related carbon structures10.1016/S0927-796X(95)00181-6 ↗
3. Nanotubes––A revolution in materials science and electronics10.1007/3-540-68117-5_6 ↗
4. Chemistry and Physics in one-dimension––synthesis and properties of nanowires and nanotubes10.1021/ar9700365 ↗
5. Nanotubes from carbon10.1021/cr970102g ↗
6. The methods of production of carbon nanotubes
7. Synthesis of carbon nanotube Fe-Al2O3 nanocomposite powders by selective reduction of different Al1·8Fe0·2O3 solid-solutions10.1039/a706726g ↗
8. Chemical-vapor-deposition of methane for single-walled carbon nanotubes10.1016/S0009-2614(98)00745-3 ↗
9. Preparation of aligned carbon nanotubes catalyzed by laser-etched cobalt thin-films10.1016/S0009-2614(98)00093-1 ↗
10. A new and easy method for making well-organized micrometer-sized carbon tubes and their regularly assembled structures10.1021/cm990032p ↗
11. Nitrogen-containing carbon nanotube growth from Ni phthalocyanine by chemical vapor deposition10.1016/S0008-6223(96)00142-X ↗
12. Matrix synthesis of N-containing carbon nanotubes10.1023/A:1016092101771 ↗
13. Fine-structure of boron-nitride nanotubes produced from carbon nanotubes by a substitution reaction10.1063/1.122680 ↗
14. Controlled production of aligned-nanotube bundles10.1038/40369 ↗
15. BsbondCN, CN and BN nanotubes produced by the pyrolysis of precursor molecules over Co catalysts10.1016/S0009-2614(98)00220-6 ↗
16. MoO3-promoted synthesis of multi-walled BN nanotubes from C-nanotube templates10.1016/S0009-2614(00)00480-2 ↗
17. MoO3 Large-scale synthesis and HRTEM analysis of single-walled B-doped and N-doped carbon nanotube bundles10.1016/S0008-6223(00)00058-0 ↗
18. Low-temperature growth and field emission of aligned carbon nanotubes by chemical vapor deposition10.1016/S0254-0584(01)00441-2 ↗
19. Preparation of ultrafine carbon tubes in nanochannels of an anodic aluminum-oxide film10.1021/cm960063+ ↗
20. Synthesis of carbon nanotube composites in nanochannels of an anodic aluminum-oxide film10.1246/bcsj.72.1957 ↗
21. Structure, thermal stability, and deformation of multibranched carbon nanotubes synthesized by CVD in the AAO template10.1021/jp002408o ↗
22. Electrochemical storage of lithium multiwalled carbon nanotubes10.1016/S0008-6223(98)00187-0 ↗
23. Some aspects of the surface chemistry of carbon blacks and other carbons10.1016/0008-6223(94)90031-0 ↗
24. Modification of the surface chemistry of activated carbons10.1016/S0008-6223(98)00333-9 ↗
25. Infrared active optical vibrations of graphite10.1016/0038-1098(77)90663-9 ↗
26. Saito · 1998
27. Ditchburn · 1965