journal article·2015

Nanocrystal size distribution analysis from transmission electron microscopy images

Martijn van Sebille, Laurens J. P. van der Maaten, Ling Xie, Karol Jarolimek, Rudi Santbergen, René A. C. M. M. van Swaaij, Klaus Leifer, Miro Zeman

Nanoscale· Volume 7· Issue 48
Publisher page

Abstract

We propose a method, with minimal bias caused by user input, to quickly detect and measure the nanocrystal size distribution from transmission electron microscopy (TEM) images using a combination of Laplacian of Gaussian filters and non-maximum suppression. We demonstrate the proposed method on bright-field TEM images of an a-SiC:H sample containing embedded silicon nanocrystals with varying magnifications and we compare the accuracy and speed with size distributions obtained by manual measurements, a thresholding method and PEBBLES. Finally, we analytically consider the error induced by slicing nanocrystals during TEM sample preparation on the measured nanocrystal size distribution and formulate an equation to correct this effect.
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Research context

OpenAlex topics: Advanced Electron Microscopy Techniques and Applications · Force Microscopy Techniques and Applications · Ion-surface interactions and analysis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Photovoltaic Materials and Devices

Delft University of Technology

2628 CD Delft, The Netherlands

Pattern Recognition Laboratory

Applied Materials Science

Uppsala University

752 37 Uppsala, Sweden

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