journal article·2019-08Open access

Novel Microstructures Produced by Flash Sintering LaPO4/Al2O3Composites

Yingjie Yang, Martha L Mecartney

Microscopy and Microanalysis· Volume 25· Issue S2

Abstract

The material system LaPO 4 /Al 2 O 3 has promise as a high fracture toughness material because it resists crack propagation by interfacial debonding, as demonstrated by Al 2 O 3 fibers when coated by LaPO 4 [1] . Sintering Al 2 O 3 and LaPO 4 typically requires a furnace temperature of over 1600C for hours. A faster and more economical method to lower energy consumption and manufacturing cost is flash sintering [2] . Flash sintering applies an electric field and controls current flowing through a freestanding pressed powder sample, lowering the temperature and shortening time to sinter to seconds or minutes, providing an economical route to fabricate ceramics. Moreover, rapid heating to high temperatures during the flash and fast cooling can provide unique non-equilibrium microstructures and compositions [3] .
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Ferroelectric and Piezoelectric Materials

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References (4)

Show source-provided references
1. Funding by NSF Grant 1662791. SEM, TEM at the UC Irvine Materials Research Institute (IMRI).
2. Kok · J. Am. Ceram. Soc · 2019 · 102 · 64410.1111/jace.15927 ↗
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4. 10.1111/j.1551-2916.2010.04267.x10.1111/j.1551-2916.2010.04267.x ↗