journal article·2025-02-17Open access

Control of Grain Boundary Formation in Atomically Resolved Nanocrystalline Carbon Monolayers: Dependence on Electron Energy

Christopher Leist, Max Makurat, Andy Jiao, Xue Liu, Grégory F Schneider, Ute Kaiser

Microscopy and Microanalysis· Volume 31· Issue 1

Abstract

Abstract In this study, we explore the dynamics of grain boundaries in nanocrystalline carbon monolayers, focusing on their variation with electron beam energy and electron dose rate in a spherical and chromatic aberration-corrected transmission electron microscope. We demonstrate that a clean surface, a high-dose rate, and a 60 keV electron beam are essential for precise local control over the dynamics of grain boundaries. The structure of these linear defects has been evaluated using neural network-generated polygon mapping.
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Research context

OpenAlex topics: Graphene research and applications · Diamond and Carbon-based Materials Research · Ion-surface interactions and analysis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Central Facility for Materials Science Electron Microscopy, Universität Ulm , Einsteinallee 11, 89081 Ulm ,

Institute for Quantum Optics (IQO), Ulm University , Einsteinallee 11, 89081 Ulm ,

Leiden Institute of Chemistry, Faculty of Science, Leiden University , Einsteinweg 55, 2333CC Leiden ,

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