journal article·2026-05-12Open access

Effect of Heat Treatment on Mechanical Properties and Fatigue Behaviors of a Selective Laser Melting Nickel-Based Superalloy

Zongxian Song, Zhiwei Gao, Lina Zhu, Hao Jin, Jian Zhao, Caiyan Deng

Metals· Volume 16· Issue 5

Abstract

This investigation elucidates the elevated-temperature (650 °C) monotonic mechanical response and very-high-cycle fatigue (VHCF) characteristics of Inconel 718 superalloys additively manufactured via selective laser melting (SLM), with a comparative assessment between the as-built and post-process heat-treated states. The results indicate that mechanical performance improves after heat treatment, primarily due to the formation of γ′ and γ″ precipitates, which interact with dislocations to strengthen the alloy. Relative to the as-built specimens, the fatigue strength of the specimen after heat treatment has increased by more than twice. For the as-built specimen, fatigue cracks nucleate at the specimen surface. However, in the high stress range, crack initiation in the heat-treated specimens consistently occurs at the free surface, whereas under low stress conditions, the crack initiation site transitions to the subsurface region encompassing internal defects. Post heat treatment, the fatigue crack trajectory adopts a markedly ductile and tortuous morphology, engendered by the concerted influence of grain-boundary (Laves/δ) precipitates that enforce repeated crack deflection, matrix-strengthening phases that homogenize plastic strain and the attendant reduction in local strain accumulation under the effect of cyclic load.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Additive Manufacturing Materials and Processes · Cellular and Composite Structures · High Temperature Alloys and Creep

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

School of Aeronautics and Astronautics, Tianjin Sino-German University of Applied Sciences, Tianjin 300350, China

Tianjin Key Laboratory of High Performance Precision Forming Manufacturing Technology and Equipment, School of Mechanical Engineering, Tianjin University of Technology and Education, Tianjin 300222, China

Wheel Rail Center, Tianjin Research Institute for Advanced Equipment, Tsinghua University, Tianjin 300300, China

School of Control and Mechanical Engineering, Tianjin Chengjian University, Tianjin 300384, China

School of Materials Science and Engineering, Tianjin University, Tianjin 300350, China

Funding

Tianjin Natural Science Foundation

References (43)

Show source-provided references
1. Heat treatment for selective laser melting of Inconel 718 alloy with simultaneously enhanced tensile strength and fatigue properties10.1016/j.jallcom.2022.165171 ↗
2. Microstructure and fatigue crack growth behavior of Inconel 718 superalloy manufactured by laser directed energy deposition10.1016/j.ijfatigue.2020.106005 ↗
3. Effect of standard heat treatment on the microstructure and mechanical properties of selective laser melting manufactured Inconel 718 superalloy10.1016/j.msea.2015.06.021 ↗
4. Microstructural evolution and fatigue cracking mechanisms of as-built and solution-aged Inconel 718 superalloy fabricated by selective laser melting at service temperature10.1016/j.engfailanal.2025.109996 ↗
5. Investigation of post-heat treatment on precipitation kinetics and mechanical properties Inconel 718 superalloy additively manufactured by selective laser melting10.1016/j.mtcomm.2025.111956 ↗
6. Effect of solution annealing on the microstructure, mechanical properties & residual stresses of selective laser melted Inconel 71810.1016/j.jallcom.2025.184656 ↗
7. Effect of annealing treatment on microstructure and residual stress evolution in a selective laser melted Ni-based superalloy10.1016/j.jmrt.2025.12.168 ↗
8. Effects of manufacturing defects and microstructure on the tensile and low cycle fatigue behavior of selective laser melting IN718 TPMS structures10.1016/j.tws.2026.114528 ↗
9. Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting10.1016/j.actamat.2011.12.032 ↗
10. Al-based functionally graded super-intermetallic compounds for the turbine blade of a high-performance jet engine10.1007/s42114-025-01499-4 ↗
11. Effect of heat treatment on the microstructure and mechanical properties of Inconel 718 processed by selective laser melting10.1016/j.msea.2015.05.035 ↗
12. Effect of heat treatment on the microstructure and mechanical anisotropy of selective laser-melted Inconel 718 alloy10.1016/j.mtcomm.2025.113453 ↗
13. Microstructural evolution and phase transformation of Inconel 718 alloys fabricated by selective laser melting under different heat treatment10.1016/j.jmapro.2019.02.029 ↗
14. The microstructure and mechanical properties of deposited-IN718 by selective laser melting10.1016/j.jallcom.2011.10.107 ↗
15. Crack initiation mechanisms during very high cycle fatigue of Ni-based single crystal superalloys at high temperature10.1016/j.actamat.2020.02.012 ↗
16. Fracture mechanism and life prediction of IN718 under very high cycle variable amplitude loading at high temperature10.1016/j.engfailanal.2025.109745 ↗
17. Competing crack initiation behaviors of a laser additively manufactured nickel-based superalloy in high and very high cycle fatigue regimes10.1016/j.ijfatigue.2020.105580 ↗
18. Effect of elevated temperature on high-cycle and very-high-cycle fatigue properties of Ni-based superalloy manufactured by selective laser melting10.1016/j.ijfatigue.2021.106250 ↗
19. Crack initiation mechanisms and life prediction of GH4169 superalloy in the high cycle and very high cycle fatigue regime10.1016/j.jmrt.2023.07.196 ↗
20. Stored energy density research on the fatigue crack initiation at twin boundary and life prediction of Inconel718 superalloy10.1016/j.ijfatigue.2023.107590 ↗
21. Fatigue behavior and microstructural evolution of additively manufactured Inconel 718 under cyclic loading at elevated temperature10.1016/j.ijfatigue.2020.105598 ↗
22. SAE International Group, and Alloy, N. (2009). Corrosion and Heat-Resistant, Bars, Forgings, and Rings 52.5Ni-19Cr-3.0Mo-5.1Cb (Nb)-0.90Ti-0.50Al-18Fe Consumable Electrode or Vacuum Induction Melted 1775 °F (968 °C) Solution and Precipitation Heat Treated, SAE International Group.
23. (2015). Metallic Materials-Tensile Testing-Part 2: Method of Test at Elevated Temperature (Standard No. GB/T 228.2 2015).
24. Effect of heat treatment on microstructure evolution of Inconel 718 alloy fabricated by selective laser melting10.1016/j.jallcom.2018.06.112 ↗
25. Microstructural and texture development in direct laser fabricated IN71810.1016/j.matchar.2013.12.012 ↗
26. Hot isostatic pressing of IN718 components manufactured by selective laser melting
27. Song, Z., Gao, W., Wang, D., Wu, Z., Yan, M., Huang, L., and Zhang, X. (2021). Very-High-Cycle Fatigue Behavior of Inconel 718 Alloy Fabricated by Selective Laser Melting at Elevated Temperature. Materials, 14.10.3390/ma14041001 ↗
28. Deformation mechanisms of D022 ordered intermetallic phase in superalloys10.1016/j.actamat.2016.07.055 ↗
29. Synergistic effects of γ′/γ″ precipitates and grain boundary engineering on high-temperature fatigue behavior in GH4169-CoZr superalloys: Multiscale mechanisms10.1016/j.ijfatigue.2025.109441 ↗
30. The effect of microstructures and precipitates (γ′, γ″, δ) on machinability of Inconel-718 nickel-based superalloy in turning process10.1016/j.jmapro.2022.08.004 ↗
31. Fatigue crack initiation and failure analysis of IN718 alloy after push–pull loading at room temperature and at 700 °C10.1016/j.engfailanal.2024.108977 ↗
32. Influence of defects and as-built surface roughness on fatigue properties of additively manufactured Alloy 71810.1016/j.msea.2018.08.072 ↗
33. Role of grain structure, grain boundaries, crystallographic texture, precipitates, and porosity on fatigue behavior of Inconel 718 at room and elevated temperatures10.1016/j.matchar.2019.01.028 ↗
34. Room and elevated temperature fatigue crack propagation behavior of Inconel 718 alloy fabricated by laser powder bed fusion10.1016/j.ijfatigue.2020.105802 ↗
35. Assessment of mechanical properties and fatigue performance of a selective laser melted nickel-base superalloy Inconel 71810.1016/j.msea.2019.05.007 ↗
36. Microstructural influence on fatigue crack propagation during high cycle fatigue testing of additively manufactured Alloy 71810.1016/j.matchar.2019.01.018 ↗
37. High-Cycle Fatigue Properties at Cryogenic Temperatures in INCONEL 718 Nickel-based Superalloy10.2320/matertrans.45.342 ↗
38. The role of δ phase for fatigue crack propagation behavior in a Ni base superalloy at room temperature10.1016/j.msea.2016.12.029 ↗
39. Effect of the δ phase on the deformation behavior in isothermal compression of superalloy GH416910.1016/j.msea.2011.02.081 ↗
40. Effect of thermal treatment on the fatigue crack propagation behavior of a new Ni-base superalloy10.1016/j.msea.2007.05.033 ↗
41. Failure mechanisms governing the high temperature torsional fatigue behavior of additively manufactured Inconel 71810.1016/j.engfailanal.2025.110255 ↗
42. Cubi, R.E., Gonçalves, R.L., Massi, M., Ribeiro, G.D., Reis, L., and Couto, A.A. (2026). Comparison of Microstructure and Fatigue Life of Laser Powder Bed Fusion and Forging/Rolling Inconel 718 Alloy After Solution Heat Treatment and Double Aging. Metals, 16.10.3390/met16010057 ↗
43. Additive manufacturing-based repair of IN718 superalloy and high-cycle fatigue assessment of the joint