journal article·2014-12

The impact of nano-milling on porous ZnO prepared from layered zinc hydroxide nitrate and zinc hydroxide carbonate

Dajana Japić, Marko Bitenc, Marjan Marinšek, Zorica Crnjak Orel

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Abstract

Abstract The preparation of ZnO nanoparticles with a multi-step process is reported. The preparation path included zinc hydroxide nitrate (ZnHN) or zinc hydroxide carbonate (ZnHC) precipitation, their thermal treatment and nano-milling. ZnO preparation was followed in detail by STEM, FT-IR, XRD and TG-MS analyses. In order to demonstrate the efficiency of the nano-milling process, the obtained ZnO nanoparticles were characterized with regard to their photo-catalytic activity of caffeine degradation. The smallest ZnO nanoparticles (∼20 nm) with the highest BET surface (∼80 m2 g−1) were prepared from ZnHC at 300 °C.
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Research context

OpenAlex topics: ZnO doping and properties · Advanced Photocatalysis Techniques · Layered Double Hydroxides Synthesis and Applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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