Effect of growth rates and temperature gradients on the lamellar spacing and the undercooling in the directionally solidified Pb–Cd eutectic alloy
Source abstract
Abstract
Abstract Lead–cadmium of high (99.99%) purity eutectic alloy was melted in a graphite crucible under vacuum atmosphere. These regular eutectic alloys were directionally solidified upward with a constant growth rate of 8.3 μm/s, and different temperature gradients G (∼1.6–6.4 K/mm range), and also with a constant temperature gradient (∼6.4 K/mm) and different growth rates V (8.3–165.5 μm/s range) in the Bridgman-type directional solidification furnace. The lamellar spacings λ were measured from both transverse section and longitudinal section of the specimen. The variations of λ with respect to G and V were determined by using linear regression analysis. The dependence of λ on ΔTe (the extremum undercooling) was also analysed. The variation of ΔTe with V at constant G and with G at constant V were investigated. According to these results, it has been found that λ decreases with the increasing values of G and V. Also ΔTe increases with increasing V for a constant G and with the increasing G for a given V, respectively. The results obtained in this work have been compared with the Jackson–Hunt eutectic theory and the previous experimental results.
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Research context
OpenAlex topics: Solidification and crystal growth phenomena · Aluminum Alloy Microstructure Properties · Metallurgical Processes and Thermodynamics
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (69)
Show source-provided references
1. M.C. Flemings, Solidification Processing, McGraw-Hill, New York, 1974.10.1007/BF02643923 ↗
2. R. Elliott, Eutectic Solidification Processing, Butterworths, London, 1983.10.1016/B978-0-408-10714-3.50007-1 ↗
3. W.A. Tiller, Liquid Metals and Solidification, ASM, Metals Park, OH, 1958, p. 276.
4. D.M. Stefanuscu, G.J. Abbaschian, R.J. Bayuzick, Solidification Processing of Eutectic Alloys, The Metallurgical Society, Inc., Ohio, 1988.
5. W. Kurz, D.J. Fisher, Fundamentals of Solidification, 3th ed., Trans Tech Publications, USA, 1989.
6. S.H. Davies (General Ed.), Theory of Solidification, Cambridge University Press, Cambridge, 2001.
7. Kurz · Int. Metals Rev. · 1979 · 224 · 177
8. Kurz · Acta Metall. · 1990 · 38 · 110.1016/0956-7151(90)90129-5 ↗
9. J.D. Hunt, S.-Z. Lu, in: D.T. Hurle (Ed.), Handbook of Crystal Growth, vol. 2b, North Holland, Amsterdam, 1994, p. 1111.
10. Hunt · J. Cryst. Growth · 1968 · 3/4 · 8210.1016/0022-0248(68)90103-6 ↗
11. Hunt · Metall. Trans. · 1970 · 1 · 31810.1007/BF02819287 ↗
12. Jordan · Metall. Trans. · 1971 · 2 · 340110.1007/BF02811622 ↗
13. Sato · J. Cryst. Growth · 1974 · 22 · 25910.1016/0022-0248(74)90170-5 ↗
14. Kurz · Acta Metall. · 1980 · 28 · 77710.1016/0001-6160(80)90155-8 ↗
15. Jones · Z. Metallkde. · 1981 · 4 · 792
16. Picone · Scripta Metall. · 1992 · 15 · 854
17. Pandey · Acta Metall. · 1987 · 35 · 254910.1016/0001-6160(87)90152-0 ↗
18. Eshelman · Acta Metall. · 1987 · 35 · 244310.1016/0001-6160(87)90141-6 ↗
19. B. Drevet, D. Camel, J.J. Favier, in: Proceedings of the VIIth European Symposium on Materials and Fluid Science in Microgravity, Oxford, 1989.
20. Liu · Acta Metall. · 1990 · 38 · 162510.1016/0956-7151(90)90004-Z ↗
21. Magnin · Acta Metall. · 1991 · 39 · 46910.1016/0956-7151(91)90115-H ↗
22. Fecht · Acta Metall. · 1991 · 39 · 100310.1016/0956-7151(91)90301-G ↗
23. Liu · Scripta Metall. · 1992 · 26 · 17910.1016/0956-716X(92)90169-F ↗
24. Leonhardt · Acta Metall. · 1999 · 47 · 2961
25. Kitazono · Acta Metall. · 1999 · 47 · 135
26. Çadırlı · J. Mater. Process. Technol. · 2000 · 97 · 7410.1016/S0924-0136(99)00344-1 ↗
27. Norlund · Metall. Trans. · 2000 · 31A · 126110.1007/s11661-000-0121-3 ↗
28. Zhuang · Sci. Tech. Adv. Mater. · 2001 · 2 · 3710.1016/S1468-6996(01)00023-7 ↗
29. Hunt · Sci. Tech. Adv. Mater. · 2001 · 2 · 14710.1016/S1468-6996(01)00040-7 ↗
30. Milenkovic · J. Cryst. Growth · 2002 · 237–239 · 9510.1016/S0022-0248(01)01875-9 ↗
31. Chen · Acta Metall. · 2002 · 50 · 2269
32. Zener · Trans. A.I.M.E. · 1946 · 167 · 550
33. Jackson · Trans. Metall. Soc. A.I.M.E. · 1966 · 236 · 1129
34. Trivedi · Acta Metall. · 1987 · 35 · 97110.1016/0001-6160(87)90176-3 ↗
35. Jordan · Metall. Trans. · 1972 · 3 · 138510.1007/BF02643021 ↗
36. Magnin · Acta Metall. · 1987 · 35 · 111910.1016/0001-6160(87)90059-9 ↗
37. Magnin · Acta Metall. · 1991 · 39 · 45310.1016/0956-7151(91)90114-G ↗
38. Kurz · Metall. Trans. · 1991 · 22A · 305110.1007/BF02650266 ↗
39. Moore · J. Inst. Metals · 1967 · 95 · 369
40. Seetharaman · Metall. Trans. · 1988 · 19A · 295510.1007/BF02647722 ↗
41. Trivedi · Metall. Trans. · 1991 · 22A · 252310.1007/BF02665018 ↗
42. Nash · J. Cryst. Growth · 1977 · 38 · 15510.1016/0022-0248(77)90295-0 ↗
43. Sharma · Acta Mater. · 2000 · 48 · 87510.1016/S1359-6454(99)00378-X ↗
44. Liu · Mater. Sci. Eng. A · 1992 · 157 · 7310.1016/0921-5093(92)90100-F ↗
45. Liu · Scripta Metall. · 1992 · 27 · 122310.1016/0956-716X(92)90604-D ↗
46. Çadırlı · Mater. Trans. JIM · 1999 · 40 · 98910.2320/matertrans1989.40.989 ↗
47. Ourdjini · Mater. Sci. Technol. · 1994 · 10 · 31210.1179/mst.1994.10.4.312 ↗
48. A. Moore, R. Elliott, The solidification of metals, in: Joint Conference, Iron Steel Ins. Publ., Brighton, 1969, pp. 100, 167.
49. Cline · Mater. Sci. Eng. · 1984 · 65 · 9310.1016/0025-5416(84)90203-9 ↗
50. Hogan · Metall. Trans. · 1987 · 18A · 70710.1007/BF02649487 ↗
51. Toloui · Acta Metall. · 1976 · 24 · 56510.1016/0001-6160(76)90102-4 ↗
52. Elliott · Acta Metall. · 1980 · 28 · 148910.1016/0001-6160(80)90049-8 ↗
53. Li · Mater. Trans. JIM · 1997 · 38 · 55310.2320/matertrans1989.38.553 ↗
54. Series · J. Cryst. Growth · 1977 · 40 · 22110.1016/0022-0248(77)90009-4 ↗
55. Fetch · Metall. Trans. · 1989 · 20A · 785
56. Gündüz · Acta Metall. · 1985 · 33 · 165110.1016/0001-6160(85)90161-0 ↗
57. T. Massalski (Ed.), Binary Alloy Phase Diagrams, ASM, Metals Park, OH, 1986.
58. Kraft · Trans. A.I.M.E. · 1961 · 221 · 95
59. Jordan · Metall. Trans. · 1971 · 2 · 340110.1007/BF02811622 ↗
60. Liu · Metall. Trans. · 1995 · 26A · 47110.1007/BF02664683 ↗
61. Cline · Trans. Metall. Soc. A.I.M.E. · 1968 · 242 · 1613
62. Hiller · J. Cryst. Growth · 1968 · 3/4 · 57410.1016/0022-0248(68)90226-1 ↗
63. Strassler · Phys. Condens. Matter. · 1974 · 17 · 15310.1007/BF01475921 ↗
64. Cline · J. Appl. Phys. · 1979 · 50 · 478010.1063/1.326538 ↗
65. Langer · Phys. Rev. Lett. · 1980 · 44 · 102310.1103/PhysRevLett.44.1023 ↗
66. Datye · Phys. Rev. · 1981 · 24B · 415510.1103/PhysRevB.24.4155 ↗
67. Kassner · Phys. Rev. · 1991 · 44A · 651310.1103/PhysRevA.44.6513 ↗
68. Kassner · Phys. Rev. · 1991 · 44A · 653310.1103/PhysRevA.44.6533 ↗
69. Himemiya · Mater. Trans. JIM · 1999 · 40 · 66510.2320/matertrans1989.40.665 ↗