journal article·2001-02

A new simple hydrothermal preparation of nanocrystalline magnetite Fe3O4

R Fan, X.H Chen, Z Gui, L Liu, Z.Y Chen

Materials Research Bulletin· Volume 36· Issue 3-4
Publisher page

Abstract

Nanocrystalline magnetite particles have been prepared by hydrothermal reaction of ferrous sulfate (FeSO4), sodium hydroxide and sodium thiosulfate (Na2S2O3) at 140°C. X-ray powder diffraction pattern indicates that the product is single-phase magnetite in an inverse cubic spinel structure. Its composition is determined by traditional chemical analysis combined with X-ray photoelectron spectroscopy. Transmission electron microscopy images show that the magnetite particles are homogenous in the shape of quasi-sphere polyhedron with average diameter of 50 nm.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Magnetic Properties and Synthesis of Ferrites · Iron oxide chemistry and applications · Characterization and Applications of Magnetic Nanoparticles

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (12)

Show source-provided references
1. G. Bate, Ferromagnetic Material, Vol. 2, Recording Materials, Chapter 7, in: E.D. Wohlfarth (Ed), North-Holland Publishing Co., Amsterdam, 1980, pp. 381–507.10.1016/S1574-9304(05)80108-7 ↗
2. P.E. Matijeric, Colloid Science of Composite System, Science of Ceramic Chemical Processing, in: L.L. Hench and D.B. Ulrich (Eds.), John Wiley & Sons, New York, 1986, pp. 463–481.
3. K.K. Lepers, Vestn. Akad. Naud. Kaz. SSR. 4 (1990) 26.
4. L.S. Darken, R.W. Gurry, J. Am. Chem. Soc. 68 (1946) 798.10.1021/ja01209a030 ↗
5. V. Osterhout, Magnetic Oxides, in: D.S. Craik (Ed.), John Wiley & Sons, New York, 1975, pp. 700.
6. G. Visalakski, G. Venkateswaran, S.K. Kulshreshtha, P.H. Moorphy, Mater. Res. Bull. 28 (1993) 829.10.1016/0025-5408(93)90024-8 ↗
7. Y.T. Qian, Y. Xie, C. He, J. Li, Z.Y. Chen, Mater. Res. Bull. 29 (1994) 953.10.1016/0025-5408(94)90055-8 ↗
8. M.S. Whittingham, J.D. Guo, R. Chen, T. Chirayil, G. Janauer, P. Zavalij, Solid State Ionics 75 (1995) 257.10.1016/0167-2738(94)00220-M ↗
9. M.I. Khan, Q. Chen, J. Zubieta, Inorg. Chem. 32 (1993) 2924.10.1021/ic00065a021 ↗
10. H.B. Du, J.S. Chen, W.Q. Pang, Stud. Surf. Catal. 105 (1997) 397.10.1016/S0167-2991(97)80581-2 ↗
11. N.S. Akhmetov, General and Inorganic Chemistry, in: H. Campbell Creighton (Ed.), MIR Publishers, Moscow, 1983, pp. 585.
12. M.E. Fleet, J. Solid State Chem. 62 (1986) 75.10.1016/0022-4596(86)90218-5 ↗