journal article·2011-12

Synthesis and characterization of nickel ferrite magnetic nanoparticles

P. Sivakumar, R. Ramesh, A. Ramanand, S. Ponnusamy, C. Muthamizhchelvan

Materials Research Bulletin· Volume 46· Issue 12
Publisher page

Abstract

Abstract Nickel ferrite (NiFe 2 O 4 ) nanoparticles are prepared by a polyvinyl alcohol (PVA) assisted sol–gel auto-combustion method. The structure, composition, morphology and magnetic properties of the gel precursor are characterized by powder XRD, FT-IR, TGA, HR-SEM, TEM, HR-TEM and VSM. XRD confirms the formation of single-phase nickel ferrite with space group of Fd3m and inverse spinel structure. The vibration properties of nanoparticles are analysed by FT-IR spectrum. The thermal decomposition of the gel precursors is investigated by TGA. HR-SEM and TEM images show that the particles have spherical shape with particle size in the range of ∼30 nm and consistent with XRD result. The magnetic properties of these nanoparticles are studied for confirming the ferromagnetic behaviour at room temperature.
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Research context

OpenAlex topics: Magnetic Properties and Synthesis of Ferrites · Electromagnetic wave absorption materials · Multiferroics and related materials

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