journal article·2014-10

New structure in refractory high-entropy alloys

L. Lilensten, J.P. Couzinié, L. Perrière, J. Bourgon, N. Emery, I. Guillot

Materials Letters· Volume 132
Publisher page

Abstract

Abstract The microstructure of a new refractory high-entropy alloy of composition close to Ti 35 Zr 27.5 Hf 27.5 Nb 5 Ta 5 prepared by arc melting and induction techniques was investigated using X-Ray diffraction (XRD) and transmission electron microscopy (TEM). This alloy presents optimal empirical parameters for the formation of a solid solution phase. The as-cast material displays a density of 8480 kg m −3 and a Vickers microhardness close to 2400 MPa. While the Rietveld refinement of XRD data indicates an orthorhombic (martensite) α׳׳-type structure for the bulk alloy, TEM observations prove that the alloy exhibits a twinned hexagonal structure as thin foil. An orthorhombic–hexagonal transformation by stress relaxation during TEM sample preparation is discussed.
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Research context

OpenAlex topics: High Entropy Alloys Studies · High-Temperature Coating Behaviors · Advanced materials and composites

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