journal article·2025-06Open access

Microstructure and impact toughness evolution in high-strength anchor chain steel: A Jominy test-based investigation

Penglong Zhu, Haitao Zhao, Zanyang Liu, Junheng Gao, Honghui Wu, Chaolei Zhang, Yuhe Huang, Jun Lu, Shuize Wang, Xinping Mao

Materials & Design· Volume 254

Abstract

• Impact toughness correlates to ductility for the entirely ductile fracture. • Impact toughness correlates to effective grain size refinement for mixed fracture. • The relationship between impact toughness and Jominy distances is elucidated. • A method for predicting impact toughness of anchor chain is proposed. Ensuring the impact toughness of anchor chains remains challenging due to inhomogeneities in microstructure and mechanical properties induced by variations in cooling rates during quenching. In this research, the evolution of microstructure and impact toughness at different distances from the quenched end ( d qe ) of the Jominy test for a high-strength anchor chain steel were analysed though instrumented Charpy impact tests, microstructure characterization, phase transformation kinetics, and crystallographic analysis. Our results reveal that with the increase of d qe , the transformed microstructure gradually transits from full martensite (1.5 mm, d qe hereafter the same) to martensite dominant (9 mm) and bainite dominant (13–40 mm), accompanied by a monotonic decrease in Vickers hardness. The impact absorbed energy at 0℃ increases from 172.83 J (1.5 mm) to 215.24 J (9 mm) despite the reduced density of high angle grain boundary, due to the higher ductility at d qe of 9 mm enhancing both the crack initiation and propagation energy. Then the impact absorbed energy continuously decreases from 215.24 J (9 mm) to 124.97 J (40 mm), attributed to the higher ductile–brittle transition temperature for coarser microstructure at larger d qe , which increases the proportion of brittle fracture surface. The coarser microstructure at larger d qe can be explained by the severe variant selection during phase transformation.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Microstructure and Mechanical Properties of Steels · Fatigue and fracture mechanics · Metal Forming Simulation Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (61)

Show source-provided references
1. Anchor geotechnics for floating offshore wind: current technologies and future innovations10.1016/j.oceaneng.2023.114327 ↗
2. Numerical investigation of the capacity of anchor chain links in clay10.1061/JGGEFK.GTENG-11676 ↗
3. Maintenance analysis of anchor chain against corrosion rate by painting method
4. Characteristics of grade R4 steel manufactured by ingot casting and used in the production of offshore mooring chains
5. Reliability of mooring lines and piles for a permanently manned vessel in a tropical cyclone environment10.1016/j.apor.2018.10.019 ↗
6. Effect of tempering temperature on the microstructure and mechanical properties in mooring chain steel10.1016/j.msea.2015.03.102 ↗
7. I.L. Stern, M.F. Wheatcroft, Toward Improving the Reliability of Anchor Chain and Accessories, Offshore Technology Conference, OTC, 1978, pp. OTC-3206-MS, https://doi.org/10.4043/3206-MS.10.4043/3206-MS ↗
8. Influence of the microstructure on fatigue and fracture toughness properties of large heat-treated mold steels10.1016/j.msea.2012.08.113 ↗
9. Effects of cooling rate during quenching and tempering conditions on microstructures and mechanical properties of carbon steel flange10.3390/ma13184186 ↗
10. Thickness effect on microstructure, strength, and toughness of a quenched and tempered 178 mm thickness steel plate10.3390/met10050572 ↗
11. Thickness dependence of toughness in ultra-heavy low-alloyed steel plate after quenching and tempering10.3390/met8080628 ↗
12. Crystallographic study on microstructure and impact toughness of coarse grained heat affected zone of ultra-high strength steel10.1016/j.matlet.2022.132552 ↗
13. X. Long, R. Yang, D. Sun, W. Liu, Y. Zhang, F. Zhang, Z. Yang, Y. Li, Roles of cooling rate of undercooled austenite on isothermal transformation kinetics, microstructure, and impact toughness of bainitic steel, Mater. Sci. Eng., A. 870 (2023) 144821, doi: 10.1016/j.msea.2023.144821.10.1016/j.msea.2023.144821 ↗
14. Austenite to bainite phase transformation in the heat-affected zone of a high strength low alloy steel10.1016/j.actamat.2004.01.025 ↗
15. New insights into the mechanism of cooling rate on the impact toughness of coarse grained heat affected zone from the aspect of variant selection10.1016/j.msea.2017.07.095 ↗
16. Analysis of impact toughness scatter in simulated coarse-grained HAZ of E550 grade offshore engineering steel from the aspect of crystallographic structure10.1016/j.matchar.2018.03.037 ↗
17. Study on the mechanism of heat input on the grain boundary distribution and impact toughness in CGHAZ of X100 pipeline steel from the aspect of variant10.1016/j.matchar.2021.111344 ↗
18. Influence of typical elements and heat treatment parameters on hardenability in steel: a review
19. Comparative analysis of hardenability and microstructure of ferrous alloys
20. Impact of quenching intensity conditions on using a finite element model to investigate the microstructure and hardenability of low-alloy steel, heat treating conference
21. Correlation between Jominy test and quenched round bars
22. S. Smokvina Hanza, T. Marohnić, D. Iljkić, R. Basan, Artificial neural networks-based prediction of hardness of low-alloy steels using specific jominy distance, Metals 11 (2021) 714, doi: 10.3390/met11050714.10.3390/met11050714 ↗
23. Mathematical modeling and computer simulation of steel quenching10.1520/MPC20180040 ↗
24. N. Kobasko, Hardness and structure prediction at the core of any steel part using Jominy standard test, Proceedings of the Fifth WSEAS Conference on Heat and Mass Transfer (HMT’08), Acapulco, Mexico, 2008.
25. Prediction of mechanical properties and microstructure distribution of quenched and tempered steel shaft10.1016/j.jmatprotec.2005.04.068 ↗
26. D.S. Mackenzie, Applications of hardenability, Gear Solutions. (marec, 2017), str.
27. Understanding the Jominy end quench test
28. How to estimate hardening depth in bars
29. Numerical–Experimental correlation of microstructures, cooling rates and mechanical properties of AISI 1045 steel during the Jominy end-quench test10.1016/j.matdes.2015.03.031 ↗
30. New insight into the hardenability of high strength low alloy steel from the perspective of crystallography10.1016/j.matlet.2021.129624 ↗
31. Correlation of cooling rate, microstructure and hardness of S34MnV steel10.1007/s11663-019-01621-0 ↗
32. Conversional model of transformation strain to phase fraction in low alloy steels10.1016/j.actamat.2006.09.008 ↗
33. Mapping microstructure inhomogeneity using electron backscatter diffraction in 316L stainless steel subjected to hot plane strain compression tests10.1179/026708310X12688283410280 ↗
34. Microstructural evolution in an aluminum solid solution alloy processed by ECAP10.1016/j.msea.2011.04.017 ↗
35. Accumulative channel-die compression bonding (ACCB): A new severe plastic deformation process to produce bulk nanostructured metals10.1016/j.jmatprotec.2013.02.016 ↗
36. Variant selection in grain boundary nucleation of upper bainite10.1007/s11661-008-9510-9 ↗
37. Variant selection in grain boundary nucleation of bainite in Fe-2Mn-C alloys10.1016/j.actamat.2017.01.035 ↗
38. Quantitative analysis of variant selection in ausformed lath martensite10.1016/j.actamat.2011.11.018 ↗
39. Role of carbon content on microstructure evolution and impact toughness in coarse-grained heat-affected zone of high-strength steel10.3390/met13010106 ↗
40. Recent progress in visualization and digitization of coherent transformation structures and application in high-strength steel10.1007/s12613-023-2781-8 ↗
41. The morphology and crystallography of lath martensite in Fe-C alloys10.1016/S1359-6454(02)00577-3 ↗
42. Variant pairing quantification method for a bainitic HSLA steel10.1007/s11661-023-07149-y ↗
43. Relationship between yield ratio and the material constants of the swift equation10.1007/BF03027468 ↗
44. S.X. Huang, Q.Y. Zhao, C. Lin, C. Wu, Y.Q. Zhao, W.J. Jia, C.L. Mao, Effects of oxygen content on Charpy impact properties and crack resistance of α titanium alloys, Mater. Sci. Eng., A. 818 (2021) 141394, doi: 10.1016/j.msea.2021.141394.10.1016/j.msea.2021.141394 ↗
45. Effect of grain refinement to 1 μm on strength and toughness of dual-phase steels10.1016/j.msea.2010.08.062 ↗
46. Effect of normalization temperatures on ductile–brittle transition temperature of a modified 9Cr–1Mo steel10.1016/j.msea.2014.09.021 ↗
47. On the ductile-brittle transition in lath martensitic steel10.2355/isijinternational.51.1569 ↗
48. Effect of microstructural refinement on the toughness of low carbon martensitic steel10.1016/j.scriptamat.2007.10.053 ↗
49. Mechanical properties of ultra fine grained steels10.1016/S0924-0136(01)00797-X ↗
50. The physical metallurgy of microalloyed steels
51. F.B. Pickering, T. Gladman, An investigation into some factors which control the strength of carbon steels, British Iron and Steel Research Association, carbon steel committee, Harrogate conference, 1963.
52. Physical interpretation of grain refinement-induced variation in fracture mode in ferritic steel10.2355/isijinternational.53.382 ↗
53. Influence of grain size on the ductile fracture toughness of ferritic steel10.2355/isijinternational.54.1958 ↗
54. T. Hanamura, H. Qiu, Analysis of Fracture Toughness Mechanism in Ultra-fine-grained Steels, Springer , Japan, Tokyo, 2014, doi: 10.1007/978-4-431-54499-9.10.1007/978-4-431-54499-9 ↗
55. Microstructural characteristics and toughness of the simulated coarse grained heat affected zone of high strength low carbon bainitic steel10.1016/j.msea.2011.09.017 ↗
56. F. Wang, Q. Sun, H.C. Ren, N.N. Cao, X.D. Song, S. Deng, D.S. Qian, M. Wu, A novel quenching-electroshocking-tempering process for toughness improvement by microstructure refining and austenite stability tailoring in aviation bearing steel, Mater. Sci. Eng., A. 854 (2022) 143817, doi: 10.1016/j.msea.2022.143817.10.1016/j.msea.2022.143817 ↗
57. Effect of tempering temperature on resistance to deformation behavior for low carbon bainitic YP960 steels10.1016/j.msea.2014.09.054 ↗
58. Effects of transformation temperature on variant pairing of bainitic ferrite in low carbon steel10.1016/j.actamat.2011.12.018 ↗
59. Effect of austenite grain size on the bainitic ferrite morphology and grain refinement of a pipeline steel after continuous cooling10.1016/j.matchar.2016.11.025 ↗
60. Novel reconstruction approaches of austenitic annealing twin boundaries and grain boundaries of ultrafine grained prior austenite10.1016/j.matdes.2023.111692 ↗
61. In-situ observation of variant pair formation in bainite of low carbon steel by digital holographic microscopy10.1016/j.actamat.2024.120212 ↗