journal article·2022-09

Microstructure analysis and quantitative strengthening evaluation of medium carbon bainitic multiphase steel

Xiaowen Sun, Dongyun Sun, Yuefeng Wang, Fucheng Zhang, Guoliang Sheng, Yanming He, Tiansheng Wang

Journal of Materials Science· Volume 57· Issue 36
Publisher page

Abstract

The microstructure and properties of bainitic multiphase steels with bainitic ferrite as the main phase are the focus of the current research. In the work, multiphase microstructures of pre-formed martensite (PM), bainitic ferrite (BF), and retained austenite (RA) was obtained via austempering processes in medium carbon bainitic steel. The relationship between the multiphase characteristics and mechanical properties was analyzed quantitatively. The results show that the thickness of bainitic ferrite laths and the size of blocky retained austenite of the PM-BF-RA samples are smaller than those of the BF-RA samples. The dislocation density of bainitic ferrite and carbon content in retained austenite of the PM-BF-RA samples are higher. The PM-BF-RA samples obtain higher strength. The yield strength that was calculated by measured microstructural parameters is similar to the tested value. The dominant strengthening phases of PM-BF-RA samples are pre-formed martensite and bainitic ferrite dual phases, while those of the BF-RA samples are the bainitic ferrite. The main of the strengthening mechanism of bainitic ferrite is grain boundary strengthening, while it is solid solution strengthening for martensite and retained austenite. Small and stable retained austenite with high carbon content effectively ensures the high plasticity of PM-BF-RA samples. Moreover, the high toughness of PM-BF-RA samples can be attributed to fine bainitic ferrite and small blocky retained austenite. This study demonstrates that medium carbon bainitic multiphase steel with PM-BF-RA microstructure exhibits excellent combination of strength, plasticity, and toughness.
Source: expertdata · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Microstructure and Mechanical Properties of Steels · Metal Alloys Wear and Properties · Magnetic Properties and Applications

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (52)

Show source-provided references
1. Caballero FG, Bhadeshia HKDH (2004) Very strong bainite. Curr Opin Solid St M 8(3):251–25710.1016/j.cossms.2004.09.005 ↗
2. Haiko O, Kaikkonen P, Somani M, Valtonen K, Kmi J (2020) Characteristics of carbide-free medium-carbon bainitic steels in high-stress abrasive wear conditions. Wear 456–457:20338610.1016/j.wear.2020.203386 ↗
3. Kumar A, Makineni SK, Dutta A, Goulas C, Steenbergen M, Petrov RH, Sietsma J (2019) Design of high-strength and damage-resistant carbide-free fine bainitic steels for railway crossing applications. Mater Sci Eng A 759:210–22310.1016/j.msea.2019.05.043 ↗
4. Zhao J, Wang TS, Lv B, Zhang FC (2015) Microstructures and mechanical properties of a modified high-C-Cr bearing steel with nano-scaled bainite. Mater Sci Eng A 628:327–33110.1016/j.msea.2014.12.121 ↗
5. Ravi AM, Navarro-López A, Sietsma J, Santofimia MJ (2020) Influence of martensite/austenite interfaces on bainite formation in low-alloy steels below Ms. Acta Mater 188:1–1210.1016/j.actamat.2020.02.003 ↗
6. Lu XH, Yang ZH, Qian DS, Lan J, Hua L (2021) Effect of martensite pre-quenching on bainite transformation kinetics, martensite/bainite duplex microstructures, mechanical properties and retained austenite stability of GCr15 bearing steel. J Mater Res Technol 15:2429–243810.1016/j.jmrt.2021.09.070 ↗
7. Zhao JL, Lv B, Zhang FC, Yang ZN, Qian LH, Chen C, Long XY (2019) Effects of austempering temperature on bainitic microstructure and mechanical properties of a high-C high-Si steel. Mater Sci Eng A 742:179–18910.1016/j.msea.2018.11.004 ↗
8. Baradari S, Boutorabi SMA (2015) Effects of isothermal transformation conditions on the microstructure and hardness values of a high-carbon Al-Si alloyed steel. Mater Des 86:603–60910.1016/j.matdes.2015.07.151 ↗
9. Jian F, Frankenbach T, Wettlaufer M (2017) Strengthening 42CrMo4 steel by isothermal transformation below martensite start temperature. Mater Sci Eng A 683:110–11510.1016/j.msea.2016.12.013 ↗
10. Yang ZN, Liu CB, Zhang CY, Fang QW, Li YG, El-Fallah GMAM, Ooi SW, Zhang FC (2021) Microplasticity behavior of multiphase high-strength nanobainitic steel based on a modified law of mixtures. Mater Sci Eng A 825:14184810.1016/j.msea.2021.141848 ↗
11. Zhao JL, Zhang FC, Lv B, Yang ZN, Chen C, Long XY, Zhao XJ, Chu CH (2019) Inconsistent effects of austempering time within transformation stasis on monotonic and cyclic deformation behaviors of an ultrahigh silicon carbide-free nanobainite steel. Mater Sci Eng A 751:80–8910.1016/j.msea.2019.01.100 ↗
12. Long XY, Zhao GC, Zhang FC, Xu S, Yang ZN, Du GJ, Branco R (2020) Evolution of tensile properties with transformation temperature in medium-carbon carbide-free bainitic steel. Mater Sci Eng A 775:13896410.1016/j.msea.2020.138964 ↗
13. Qian LH, Li Z, Wang TL, Li DD, Zhang FC, Meng JY (2022) Roles of pre-formed martensite in below-Ms bainite formation, microstructure, strain partitioning and impact absorption energies of low-carbon bainitic steel. J Mater Sci Technol 96:69–8410.1016/j.jmst.2021.05.002 ↗
14. Pashangeh S, Somani M, Banadkoukia SSG (2020) Microstructural evolution in a high-silicon medium carbon steel following quenching and isothermal holding above and below the Ms temperature. J Mater Sci Technol 9(3):3438–3446
15. Garcia-Mateo C, Caballero FG, Bhadeshia HKDH (2005) Mechanical properties of low-temperature bainite. Mater Sci Forum 500–501:495–50210.4028/www.scientific.net/MSF.500-501.495 ↗
16. Tan X, Xu Y, Yang X, Wu D (2014) Microstructure-properties relationship in a one-step quenched and partitioned steel. Mater Sci Eng A 589:101–11110.1016/j.msea.2013.09.063 ↗
17. Zhao LJ, Qian LH, Zhou Q, Li DD, Wang TL, Jia ZG, Zhang FC, Meng JY (2019) The combining effects of ausforming and below-Ms or above-Ms austempering on the transformation kinetics, microstructure and mechanical properties of low-carbon bainitic steel. Mater Des 183:108–12310.1016/j.matdes.2019.108123 ↗
18. Guo H, Feng XY, Zhao AM, Li Q, Ma J (2019) Influence of prior martensite on bainite transformation, microstructures, and mechanical properties in ultra-fine bainitic steel. Materials 12(3):52710.3390/ma12030527 ↗
19. Navarro-López A, Hidalgo J, Sietsma J, Santofimia MJ (2018) Influence of the prior athermal martensite on the mechanical response of advanced bainitic steel. Mater Sci Eng A 735:343–35310.1016/j.msea.2018.08.047 ↗
20. Hasan HS, Peet MJ, Avettand-Fènoël M-N, Bhadeshia HKDH (2014) Effect of tempering upon the tensile properties of a nanostructured bainitic steel. Mater Sci Eng A 615:340–34710.1016/j.msea.2014.07.097 ↗
21. Fostera D, Paladugu M, Hughes J, Kapousidou M, Barcellini C, Daisenberger D, Jimenez-Melero E (2020) Comparative micromechanics assessment of high-carbon martensite/bainite bearing steel microstructures using in-situ synchrotron X-ray diffraction. Materialia 14:10094810.1016/j.mtla.2020.100948 ↗
22. Abbaszadeh P, Kheirandish S, Saghafian H, Goodarzy MH (2017) Effect of austenitizing temperature on mechanical properties of the mixed bainite-martensite microstructure in CrMoV steel. Mater Res 21(1):046910.1590/1980-5373-mr-2017-0469 ↗
23. Garcia-Mateo C, Caballero FG, Sourmail T, Kuntz M, Cornide J, Smanio V, Elvira R (2012) Tensile behaviour of a nanocrystalline bainitic steel containing 3 wt% silicon. Mater Sci Eng A 549:185–19210.1016/j.msea.2012.04.031 ↗
24. Zhao JL, Zhao XM, Dong CY, Zhao XY, Kang SX (2018) Effect of bainitic transformation combined with hot forming on the microstructure and mechanical properties of bainite-martensite multiphase steel. Mater Sci Eng A 731:102–10610.1016/j.msea.2018.05.111 ↗
25. Avishana B, Khoshkebari SM, Yazdani S (2021) Effect of pre-existing martensite within the microstructure of nano bainitic steel on its mechanical properties. Mater Chem Phys 260:12416010.1016/j.matchemphys.2020.124160 ↗
26. Long XY, Sun DY, Wang K, Zhang FC, Yang ZN, Li YG, Zheng CL (2022) Effect of carbon distribution range in mixed bainite/martensite/retained austenite microstructure on mechanical properties. J Mater Res Technol 17:898–91210.1016/j.jmrt.2021.12.121 ↗
27. De AK, Murdock DC, Mataya MC, Speer JG, Matlock DK (2004) Quantitative measurement of deformation-induced martensite in 304 stainless steel by X-ray diffraction. Scripta Mater 50(12):1445–144910.1016/j.scriptamat.2004.03.011 ↗
28. Williamson GK, Smallman RE III (1956) Dislocation densities in some annealed and cold-worked metals from measurements on the X-ray debye-scherrer spectrum. Philos Mag 1(1):34–4610.1080/14786435608238074 ↗
29. Germain L, Gey N, Mercier R, Blaineau P, Humbert M (2012) An advanced approach to reconstructing parent orientation maps in the case of approximate orientation relations: Application to steels. Acta Mater 60:4551–456210.1016/j.actamat.2012.04.034 ↗
30. Garcia-Mateo C, Caballero FG, Bhadeshia HKDH (2003) Acceleration of Low-temperature Bainite. ISIJ Int 43(11):1821–182510.2355/isijinternational.43.1821 ↗
31. Koistinen D, Marburger R (1959) A general equation prescribing the extent of the austenite-martensite transformation in pure iron-carbon alloys and plain carbon steels. Acta Metall 7:59–6010.1016/0001-6160(59)90170-1 ↗
32. Dyson DJ, Holmes B (1970) Effect of alloying additions on the lattice parameter of austenite. J Iron Steel Inst 208:469–474
33. Rakha K, Beladi H, Timokhina H, Xiong XY, Kabra S, Liss K-D, Hodgson P (2014) On low temperature bainitic transformation characteristics using in-situ neutron diffraction and atom probe tomography. Mater Sci Eng A 589:303–30910.1016/j.msea.2013.09.055 ↗
34. Wang XB, Liu CB, Qin YM, Li YG, Yang ZN, Long XY, Wang MM, Zhang FC (2022) Effect of tempering temperature on microstructure and mechanical properties of nanostructured bainitic steel. Mater Sci Eng A 832:14235710.1016/j.msea.2021.142357 ↗
35. Xiong XC, Chen B, Huang MX, Wang JF, Wang L (2013) The effect of morphology on the stability of retained austenite in a quenched and partitioned steel. Scr Mater 68:321–32410.1016/j.scriptamat.2012.11.003 ↗
36. M. Peet, H.K.D.H. Bhadeshia, Available online: https://www.msm.cam.ac.uk/map/steel/tar/mucg83.exe
37. Yoozbashi MN, Yazdani S, Wang TS (2011) Design of a new nanostructured, high-Si bainitic steel with lower cost production. Mater Des 32(6):3248–325310.1016/j.matdes.2011.02.031 ↗
38. Kawata H, Hayashi K, Sugiura N, Yoshinaga N, Takahashi M (2010) Effect of martensite in initial structure on bainite transformation. Mater Sci Forum 638–642:3307–331210.4028/www.scientific.net/MSF.638-642.3307 ↗
39. Gong W, Tomota Y, Harjo S, Su YH, Aizawa K (2015) Effect of prior martensite on bainite transformation in nanobainite steel. Acta Mater 85:243–24910.1016/j.actamat.2014.11.029 ↗
40. Toji Y, Matsuda H, Raabe D (2016) Effect of Si on the acceleration of bainite transformation by pre-existing martensite. Acta Mater 116:250–26210.1016/j.actamat.2016.06.044 ↗
41. Yan JJ, Song H, Dong YP, Quach WM, Yan M (2020) High strength (~2000MPa) or highly ductile (~11%) additively manufactured H13 by tempering at different conditions. Mater Sci Eng A 773:13884510.1016/j.msea.2019.138845 ↗
42. Carretero Olalla V, Bliznuk V, Sanchez N, Thibaux P, Kestens LAI, Petrov RH (2014) Analysis of the strengthening mechanisms in pipeline steels as a function of the hot rolling parameters. Mater Sci Eng A 604:46–5610.1016/j.msea.2014.02.066 ↗
43. Kamikawa N, Sato K, Miyamoto G, Murayama M, Sekido N, Tsuzaki K, Furuhara T (2016) Stress-strain behavior of ferrite and bainite with nano-precipitation in low carbon steels. Acta Mater 83:383–39610.1016/j.actamat.2014.10.010 ↗
44. Winchell PG, Cohen M (1962) The strength of martensite. Trans ASM 55:347
45. Langford G, Cohen M (1970) Calculation of cell-size strengthening of wire-drawn iron. Metall Mater Trans B 1:1478–148010.1007/BF02900287 ↗
46. Young CH, Bhadeshia HKDH (1994) Strength of mixtures of bainite and martensite. Mater Sci Technol 10:20910.1179/mst.1994.10.3.209 ↗
47. Hutchinson B, Hagström J, Karlsson O, Lindell D, Tornberg M, Lindberg F, Thuvander M (2011) Microstructures and hardness of as-quenched martensites (0.1–0.5%C). Acta Mater 59:5845–585810.1016/j.actamat.2011.05.061 ↗
48. Cao J, Yong Q, Liu Q, Sun X (2007) Precipitation of MC phase and precipitation strengthening in hot rolled Nb–Mo and Nb–Ti steels. J of Mater Sci 42(24):10080–1008410.1007/s10853-007-2000-4 ↗
49. Zhou Q, Qian LH, Meng JY, Zhao LJ, Zhang FC (2015) Low-cycle fatigue behavior and microstructural evolution in a low-carbon carbide-free bainitic steel. Mater Des 85:487–49610.1016/j.matdes.2015.06.172 ↗
50. Navarro-López A, Hidalgo J, Sietsma J, Santofimia MJ (2020) Unravelling the mechanical behaviour of advanced multiphase steels isothermally obtained below Ms. Mater Des 188:10848410.1016/j.matdes.2020.108484 ↗
51. Bhadeshia HKDH (2015) Bainite in steels: theory and practice, Third Edition. pp 92–94, University of Cambridge
52. Gao G, Zhang H, Gui X, Luo P, Tan Z, Bai B (2014) Enhanced ductility and toughness in an ultrahigh-strength Mn-Si-Cr-C steel: the great potential of ultrafine filmy retained austenite. Acta Mater 76:425–43310.1016/j.actamat.2014.05.055 ↗