Crystal structure and in situ investigation of a mechanochemical synthesized 3D zinc N-(phosphonomethyl)glycinate
Source abstract
Abstract
The mechanochemical synthesis of the zinc N-(phosphonomethyl)glycinate Zn(O3PCH2NH2CH2CO2)·H2O (1) is presented. The structure was solved from powder X-ray diffraction (PXRD) data. In the three-dimensional pillared structure, the Zn atoms are coordinated tetrahedrally. In situ investigations of the reaction process with synchrotron PXRD and Raman spectroscopy reveal a two-step process including the formation of an intermediate.
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Research context
OpenAlex topics: Chemical Synthesis and Characterization · Crystallography and molecular interactions · Metal-Organic Frameworks: Synthesis and Applications
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