Invar-type nanocrystalline compacts obtained by spark plasma sintering from mechanically alloyed powders
Source abstract
Abstract
Invar36 (Fe64Ni36) and Invar-Cu (Fe59Ni36Cu5) nanocrystalline compacts were successfully obtained by spark plasma sintering from mechanically alloyed powders. The coefficient of thermal expansion (CTE) was determined for both Invar36 and Invar-Cu compacts. For Invar36 powder, the lattice parameter value is constant up to 250 °C, while for the Invar-Cu powder, the value of lattice parameter changes for the temperatures that exceed 160 °C. Both Invar36 and Invar-Cu nanocrystalline compacts were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), and dilatometry. The value of CTE is very low for both Invar36 compact (α = 0.6 × 10−6/°C) and Invar-Cu (α = 5.2 × 10−6/°C) up to Curie temperature (T C), in agreement with in situ (high-temperature X-ray diffraction—HT-XRD) analyses of Invar-type powders.
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Research context
OpenAlex topics: Advanced materials and composites · Advanced ceramic materials synthesis · Metallic Glasses and Amorphous Alloys
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