journal article·2019-08Open access

Microneedle array sensors based on carbon nanoparticle composites: interfacial chemistry and electroanalytical properties

Catherine Hegarty, Stephen McKillop, Ruairi J. McGlynn, Robert B. Smith, Ashish Mathur, James Davis

Journal of Materials Science· Volume 54· Issue 15

Abstract

Conductive microneedle patches consisting of carbon nanoparticles embedded in a polystyrene matrix have been prepared using micro-moulding techniques. The interfacial properties of the structures before and after electrochemical etching have been characterised using X-ray photoelectron spectroscopy and contact angle. Anodisation of the needles leads to a significant increase in oxygen functionality and is shown to dramatically improve the electroanalytical capabilities of the microneedle array. The detection of uric acid in horse blood was used as a model system through which to assess the performance of the system. The composite approach is shown to lead to viable carbon-based sensors and can offer a rapid prototype option for the development of tailored microneedle systems.
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Research context

OpenAlex topics: Electrochemical sensors and biosensors · Electrochemical Analysis and Applications · Carbon Nanotubes in Composites

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