Fabrication of highly crystalline titanium-containing SiC fibers with different boron contents exhibiting excellent electromagnetic wave absorption
Source abstract
Abstract
The Sylramic fibers containing both titanium and boron elements have attracted extensive research interests in recent years. In this work, the titanium-containing Si–C–B–Ti–O fibers with boron contents ranging from 5.19 to 9.30 wt% were successfully prepared and transformed to highly crystalline SiC (B, Ti) fibers after sintering. However, the boron contents of SiC (B, Ti) fibers were decreased to only around 1.0 wt%, which could be attributed to the preferential reaction between boron and oxygen during sintering to generate B2O3 gas. The boron element mainly existed in the forms of TiBx, BxCy, and BCxOy phases. It is fascinating that the tensile strengths of the SiC (B, Ti) fibers had certain degree of improvement. Simultaneously, the SiC (B, Ti) fibers exhibited both excellent high-temperature resistance (~ 2000 °C) and outstanding electromagnetic wave absorption performance. The minimum reflection loss value of − 55.82 dB was achieved with fitting thickness of 1.80 mm, and the effective absorption bandwidth could reach 3.24 GHz. Our work provides a convenient strategy for developing a new type of raw material with structural and functional integration, which has broad application prospects in the field of advanced aircraft.
Source: expertdata · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Electromagnetic wave absorption materials · Advanced ceramic materials synthesis · Aluminum Alloys Composites Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (48)
Show source-provided references
1. Okamura K, Shimoo T, Suzuya K, Suzuki K (2007) SiC-based ceramic fibers prepared via organic-to-inorganic conversion process-a review. J Ceram Soc Jpn 114:445–45410.2109/jcersj.114.445 ↗
2. Kang W, Chen J, Zhang Y, Zhang Q, Chen T, Gou Y (2023) SiC fibers with different diameters exhibiting excellent high-temperature resistance and oxidation resistance. J Mater Res Technol 23:1559–156910.1016/j.jmrt.2023.01.129 ↗
3. Takeda M, Urano A, Sakamoto J, Imai Y (2000) Microstructure and oxidation behavior of silicon carbide fibers derived from polycarbosilane. J Am Ceram Soc 83:1171–117610.1111/j.1151-2916.2000.tb01350.x ↗
4. Bunsell AR, Piant A (2006) A review of the development of three generations of small diameter silicon carbide fibres. J Mater Sci 41:823–839. https://doi.org/10.1007/s10853-006-6566-z10.1007/s10853-006-6566-z ↗
5. Schawaller D, Clauß B, Buchmeiser MR (2012) Ceramic filament fibers-a review. Macromol Mater Eng 297:502–52210.1002/mame.201100364 ↗
6. Bhatt R, Eldridge J (2023) Heat treatment effects on microstructure and properties of CVI SiC/SiC composites with Sylramic™-iBN SiC fibers. J Eur Ceram Soc 43:2376–238710.1016/j.jeurceramsoc.2022.12.034 ↗
7. Bhatt RT, Halbig MC (2022) Creep properties of melt infiltrated SiC/SiC composites with Sylramic™-iBN and Hi-Nicalon™-S fibers. Int J Appl Ceram Technol 19:1074–109110.1111/ijac.13996 ↗
8. Gou Y, Jian K, Wang H, Wang J (2018) Fabrication of nearly stoichiometric polycrystalline SiC fibers with excellent high-temperature stability up to 1900 °C. J Am Ceram Soc 101:2050–205910.1111/jace.15366 ↗
9. Braun J, Sauder C (2022) Mechanical behavior of SiC/SiC composites reinforced with new Tyranno SA4 fibers: effect of interphase thickness and comparison with Tyranno SA3 and Hi-Nicalon S reinforced composites. J Nucl Mater 558:15336710.1016/j.jnucmat.2021.153367 ↗
10. Lv X, Yu S, Ge M, Tian Y, Zhang W (2016) Synthesis and microstructure of continuous composite ceramic fibres of ZrC/ZrB2-SiC derived from polymeric precursors. Ceram Int 42:9299–930310.1016/j.ceramint.2016.02.112 ↗
11. Ji D, Ouyang Q, Wang Y, Wang H, Liang H, He L, Huang Q (2023) Flexible and thermally stable SiC fiber mats derived from electrospun boron-doped polyaluminocarbosilane precursors. Ceram Int 49:9279–928610.1016/j.ceramint.2022.11.094 ↗
12. Zhang H, Ge M, Shui H, Yu S, Ma Q, Zhang H, Ma S, Kong W, Ma Z, Zhang W (2021) Investigations on the thermal behaviours of SiC-ZrC continuous ceramic fibres. J Eur Ceram Soc 41:4689–469610.1016/j.jeurceramsoc.2021.03.009 ↗
13. Bhatt RT, Sola F, Evans LJ, Rogers RB, Johnson DF (2021) Microstructural, strength, and creep characterization of Sylramic™, Sylramic™-iBN and super Sylramic™-iBN SiC fibers. J Eur Ceram Soc 41:4697–470910.1016/j.jeurceramsoc.2021.03.024 ↗
14. Yu Z, Zhan J, Zhou C, Yang L, Li R, Xia H (2011) Synthesis and characterization of SiC(Ti) ceramics derived from a hybrid precursor of titanium-containing polycarbosilane. J Inorg Organomet Polym Mater 21:412–42010.1007/s10904-011-9483-9 ↗
15. Wen Q, Yu Z, Riedel R, Ionescu E (2021) Single-source-precursor synthesis and high-temperature evolution of a boron-containing SiC/HfC ceramic nano/micro composite. J Eur Ceram Soc 41:3002–301210.1016/j.jeurceramsoc.2020.05.031 ↗
16. Sha JJ, Hinoki T, Kohyama A (2007) Microstructural characterization and fracture properties of SiC-based fibers annealed at elevated temperatures. J Mater Sci 42:5046–5056. https://doi.org/10.1007/s10853-006-0579-510.1007/s10853-006-0579-5 ↗
17. Cheng Y, Sun X, Yang S, Wang D, Liang L, Wang S, Ning Y, Yin W, Li Y (2023) Multifunctional elastic rGO hybrid aerogels for microwave absorption, infrared stealth and heat insulation. Chem Eng J 452:13937610.1016/j.cej.2022.139376 ↗
18. Ren B, Deng Y, Jia Y, Han L, Wang X, Li H (2023) Achieving broadband electromagnetic absorption at a wide temperature range up to 1273 K by metamaterial design on polymer-derived SiC-BN@CNT ceramic composites. Chem Eng J 478:14725110.1016/j.cej.2023.147251 ↗
19. Chen N, Wei S, Shi B, Yan R, Li X, Zhan T (2021) Investigating the electromagnetic wave-absorbing capacity and mechanical properties of flexible radar-absorbing knitted compound materials. J Ind Text 51:343–36110.1177/1528083719877006 ↗
20. Liang L, Yang R, Han G, Feng Y, Zhao B, Zhang R, Wang Y, Liu C (2020) Enhanced electromagnetic wave-absorbing performance of magnetic nanoparticles-anchored 2D Ti3C2Tx MXene. ACS Appl Mater Interfaces 12:2644–265410.1021/acsami.9b18504 ↗
21. Zou Y, Huang X, Fan B, Tang Z, Zhou J, Peng P, Liu X, Zhu J, Liu Y, Yue J (2023) Constructing hierarchical Ti3SiC2 layer and carbon nanotubes on SiC fibers for enhanced electromagnetic wave absorption. Ceram Int 49:8048–805710.1016/j.ceramint.2022.10.323 ↗
22. Zhang Y, Zhao Y, Chen Q, Hou Y, Zhang Q, Cheng L, Zheng L (2021) Flexible SiC-CNTs hybrid fiber mats for tunable and broadband microwave absorption. Ceram Int 47:8123–813210.1016/j.ceramint.2020.11.167 ↗
23. Huang B, Chen X, Wang Y, Liu Y, Zhou J, Liu Y, Yue J (2023) FeNi-modified carbon nanotube arrays on silicon carbide fibers for electromagnetic wave absorption. Ceram Int 49:36715–3672310.1016/j.ceramint.2023.08.357 ↗
24. Zhang Q, Chen T, Kang W, Xing X, Wu S, Gou Y (2023) Synthesis of polytitanocarbosilane and preparation of Si-C-Ti-B Fibers. Processes 11:118910.3390/pr11041189 ↗
25. Chen H, Yang J, Shuai Q, Li J, Ouyang Q, Zhang S (2020) In-situ doping B4C nanoparticles in PAN precursors for preparing high modulus PAN-based carbon fibers with boron catalytic graphitization. Compos Sci Technol 200:10845510.1016/j.compscitech.2020.108455 ↗
26. Wang H, Guo Q, Yang J, Liu Z, Zhao Y, Li L, Feng Z, Liu L (2013) Microstructural evolution and oxidation resistance of polyacrylonitrile-based carbon fibers doped with boron by the decomposition of B4C. Carbon 56:296–30810.1016/j.carbon.2013.01.017 ↗
27. Lee S, Cho SY, Chung YS, Choi YC, Lee S (2022) High electrical and thermal conductivities of a PAN-based carbon fiber via boron-assisted catalytic graphitization. Carbon 199:70–7910.1016/j.carbon.2022.07.068 ↗
28. Bai H, Wen G, Huang X, Han Z, Zhong B, Hu Z, Zhang X (2011) Synthesis and structural characterization of SiBOC ceramic fibers derived from single-source polyborosiloxane. J Eur Ceram Soc 31:931–94010.1016/j.jeurceramsoc.2010.11.020 ↗
29. Chen J, Zhang Y, Yan D, Gou Y (2022) Flexible ultrafine nearly stoichiometric polycrystalline SiC fibers with excellent oxidation resistance and superior thermal stability up to 1900 °C. J Eur Ceram Soc 42:1938–194610.1016/j.jeurceramsoc.2021.12.049 ↗
30. Jiang Y, Lu J, Huang F, Du L (2015) Thermo-oxidative stability of polymer-derived Si-B-C Ceramics. Int J Appl Ceram Technol 12:991–99910.1111/ijac.12399 ↗
31. Zhang Y, Chen J, Yan D, Wang S, Li G, Gou Y (2021) Conversion of silicon carbide fibers to continuous graphene fibers by vacuum annealing. Carbon 182:435–44410.1016/j.carbon.2021.06.043 ↗
32. Liu Y, Liu Y, Choi WC, Chae S, Lee J, Kim B-S, Park M, Kim HY (2017) Highly flexible, erosion resistant and nitrogen doped hollow SiC fibrous mats for high temperature thermal insulators. J Mater Chem A 5:2664–267210.1039/C6TA09475A ↗
33. Liu C, Han J, Han W, Zhang X, Hong C, Du S (2015) Sol-gel-derived SiBOC ceramics with highly graphitized free carbon. Ceram Int 41:15292–1529610.1016/j.ceramint.2015.08.078 ↗
34. Kong J, Wang M, Zou J, An L (2015) Soluble and meltable hyperbranched polyborosilazanes toward high-temperature stable SiBCN ceramics. ACS Appl Mater Interfaces 7:6733–674410.1021/am509129a ↗
35. Ischenko V, Pippel E, Woltersdorf J, Yappi BRN, Hauser R, Fasel C, Riedel R, Poli F, Müller K (2008) Influence of the precursor cross-linking route on the thermal stability of Si–B–C–O ceramics. Chem Mater 20:7148–715610.1021/cm701916g ↗
36. Chen P, Li W, Li X, Zhu Y, Zhu B (2022) Effect of boron content on the microstructure and electromagnetic properties of SiBCN ceramics. Ceram Int 48:3037–305010.1016/j.ceramint.2021.10.079 ↗
37. Wang H, Li Y, Wang Y, Hu S, Hou H (2017) Highly microporous graphite-like BCxO3-x/C nanospheres for anode materials of lithium-ion batteries. J Mater Chem A 5:2835–284310.1039/C6TA10778H ↗
38. Schiavon MA, Armelin NA, Yoshida IVP (2008) Novel poly(borosiloxane) precursors to amorphous SiBCO ceramics. Mater Chem Phys 112:1047–105410.1016/j.matchemphys.2008.07.041 ↗
39. Tamayo A, Peña-Alonso R, Rubio F, Rubio J, Oteo J (2012) Synthesis and characterization of boron silicon oxycarbide glass fibers. J Non-Cryst Solids 358:155–16210.1016/j.jnoncrysol.2011.09.002 ↗
40. Wang P, Cheng L, Zhang Y, Zhang L (2017) Flexible SiC/Si3N4 ccmposite nanofibers with in situ embedded graphite for highly efficient electromagnetic wave absorption. ACS Appl Mater Interfaces 9:28844–2885810.1021/acsami.7b05382 ↗
41. Qian J, Shui A, Du B, Cai M, He C, Zeng S, Zhong X, Lou J (2022) Synthesis and tunable electromagnetic shielding and absorption performance of the three-dimensional SiC nanowires/carbon fiber composites. J Eur Ceram Soc 42:4154–416110.1016/j.jeurceramsoc.2022.03.058 ↗
42. Liang C, Liu C, Wang H, Wu L, Jiang Z, Xu Y, Shen B, Wang Z (2014) SiC-Fe3O4 dielectric-magnetic hybrid nanowires: controllable fabrication, characterization and electromagnetic wave absorption. J Mater Chem A 2:16397–1640210.1039/C4TA02907K ↗
43. Zhang W, Dai F-Z, Xiang H, Zhao B, Wang X, Ni N, Karre R, Wu S, Zhou Y (2021) Enabling highly efficient and broadband electromagnetic wave absorption by tuning impedance match in high-entropy transition metal diborides. J Adv Ceram 10:1299–131610.1007/s40145-021-0505-y ↗
44. Zhou W, Zhang Y, Li Y, Gou Y, Zhou X (2022) In-situ synthesis of ternary layered Y3Si2C2 ceramic on silicon carbide fiber for enhanced electromagnetic wave absorption. Ceram Int 48:1908–191510.1016/j.ceramint.2021.09.275 ↗
45. Liu J, Feng Y, Liu C, Tong Y, Sun H, Peng H, Wu S, Lu J, Gong H, Guo X (2022) Novel SiBCN composite fibers with broadband and strong electromagnetic wave absorption performance. J Alloys Compd 912:16519010.1016/j.jallcom.2022.165190 ↗
46. Ye X, Zhang J, Chen Z, Xiang J, Jiang Y, Xie F, Ma X (2021) Microwave absorption properties of Ni/C@SiC composites prepared by precursor impregnation and pyrolysis processes. Def Technol 21:94–10210.1016/j.dt.2021.11.005 ↗
47. Long X, Zhang S, Shao C, Wang B, Wang Y (2020) Effects of heat-treatment on the microstructure, electromagnetic wave absorbing properties, and mechanical properties of SiCN fibers. Front Mater 7:56389110.3389/fmats.2020.563891 ↗
48. An Z, Ye C, Zhang R, Zhou P (2019) Flexible and recoverable SiC nanofiber aerogels for electromagnetic wave absorption. Ceram Int 45:22793–2280110.1016/j.ceramint.2019.07.321 ↗