journal article·2020-01

Microstructure, mechanical properties, and texture evolution of Mg–Zn–Y–Zr alloy fabricated by hot extrusion–shearing process

Shuai Dai, Feng Wang, Zhi Wang, Zheng Liu, Pingli Mao

Journal of Materials Science· Volume 55· Issue 1
Publisher page

Abstract

In this study, ultrafine-grained Mg–Zn–Y–Zr alloys were obtained via a novel extrusion–shearing (ES) deformation process, which combined initial forward extrusion with subsequent shearing. The experimental results showed that the composition of the main phase was converted from the α-Mg, I (Mg3Zn6Y), and W (Mg3Zn3Y2) phases to the α-Mg and W phases as the Zn/Y mass ratio of the as-cast alloys decreased from 4 to 0.67. Needle-shaped YZn5 and micron-sized Mg7Zn3 phases were also observed in the as-homogenized Mg–4Zn–1Y–0.6Zr and Mg–3Zn–2Y–0.6Zr alloys. The quantitative electron backscatter diffraction results demonstrated that the dynamic recrystallization (DRX) and the growth of fine DRX grains had a strong dependence on the equivalent strain and increased temperature caused by the die corner. The abundance of W precipitates resulted in the gradual evolution of the sub-grains into fresh DRX grains for the ES alloy III. Additionally, reduced strength anisotropies were related to the decreased pole density caused by the increasing addition of Y; a weakened basal texture with a rare-earth texture component was also achieved at 3 wt% of Y addition. Finally, the influences of the grain size and basal texture on the ductility and strength of the ES alloys were systematically investigated.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Magnesium Alloys: Properties and Applications · Aluminum Alloys Composites Properties · Metal and Thin Film Mechanics

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (42)

Show source-provided references
1. Kulekci MK (2008) Magnesium and its alloys applications in automotive industry. Int J Adv Manuf Technol 39:851–86510.1007/s00170-007-1279-2 ↗
2. Mordike BL, Ebert T (2001) Magnesium properties–applications–potential. Mater Sci Eng, A 302(1):37–4510.1016/S0921-5093(00)01351-4 ↗
3. Yuan W, Panigrahi SK, Su J-Q, Mishra RS (2011) Influence of grain size and texture on Hall–Petch relationship for a magnesium alloy. Scr Mater 65(11):994–99710.1016/j.scriptamat.2011.08.028 ↗
4. Song B, Xin RL, Chen G, Zhang XY, Liu Q (2012) Improving tensile and compressive properties of magnesium alloy plates by pre-cold rolling. Scr Mater 66(12):1061–106410.1016/j.scriptamat.2012.02.047 ↗
5. Krajňák T, Minárik P, Stráská J, Gubicza J, Máthis K, Miloš J (2019) Influence of the initial state on the microstructure and mechanical properties of AX41 alloy processed by ECAP. J Mater Sci 54(4):3469–3484. https://doi.org/10.1007/s10853-018-3033-610.1007/s10853-018-3033-6 ↗
6. Chino Y, Kimura K, Mabuchi M (2008) Twinning behavior and deformation mechanisms of extruded AZ31 Mg alloy. Mater Sci Eng, A 486(1–2):481–48810.1016/j.msea.2007.09.058 ↗
7. Wang MY, Xin RL, Wang BS, Liu Q (2011) Effect of initial texture on dynamic recrystallization of AZ31 Mg alloy during hot rolling. Mater Sci Eng, A 528(6):2941–295110.1016/j.msea.2010.11.069 ↗
8. Luo AA, Mishra RK, Sachdev AK (2011) High-ductility magnesium–zinc–cerium extrusion alloys. Scr Mater 64(5):410–41310.1016/j.scriptamat.2010.10.045 ↗
9. Janeček M, Yi S, Král R, VrátnáJ Kainer KU (2010) Texture and microstructure evolution in ultrafine-grained AZ31 processed by EX-ECAP. J Mater Sci 45(17):4665–4671. https://doi.org/10.1007/s10853-010-4675-110.1007/s10853-010-4675-1 ↗
10. Figueiredo RB, Langdon TG (2006) The development of superplastic ductilities and microstructural homogeneity in a magnesium ZK60 alloy processed by ECAP. Mater Sci Eng, A 430(1–2):151–15610.1016/j.msea.2006.05.056 ↗
11. Imandoust A, Barrett CD, Al-Samman T, Inal KA, El Kadiriet H (2017) A review on the effect of rare-earth elements on texture evolution during processing of magnesium alloys. J Mater Sci 52(1):1–29. https://doi.org/10.1007/s10853-016-0371-010.1007/s10853-016-0371-0 ↗
12. Xu C, Nakata T, Fan GH, Li XW, Tang GZ, Geng L, Kamado S (2019) Microstructure and mechanical properties of extruded Mg–Gd–Y–Zn alloy with Mn or Zr addition. J Mater Sci 54:10473–10488. https://doi.org/10.1007/s10853-019-03607-410.1007/s10853-019-03607-4 ↗
13. Sanjari M, Kabir ASH, Farzadfar A, Ustunomiya H, Petrov R, Kestens L, Yue S (2014) Promotion of texture weakening in magnesium by alloying and thermomechanical processing: (I) alloying. J Mater Sci 49(3):1408–1425. https://doi.org/10.1007/s10853-013-7826-310.1007/s10853-013-7826-3 ↗
14. Sanjari M, Farkoosh AR, Shalchi Amirkhiz B, He Y, Javaid A, Kabir AS, Su J, Jung IH, Yue S (2017) The role of the Zn/Nd ratio in the microstructural evolution of the Mg–Zn–Nd system during static recrystallization: grain boundary partitioning of solutes. Scr Mater 134:1–510.1016/j.scriptamat.2017.01.033 ↗
15. Zhang JS, Chao X, Cheng WL, Bian LP, Wang HG, Xu CX (2013) Research on long-period-stacking-ordered phase in Mg–Zn–Dy–Zr alloy. J Alloys Compd 558(5):195–20210.1016/j.jallcom.2012.12.165 ↗
16. Kim S-H, Lee JU, Kim YJ, Jung J-G, Park SH (2018) Controlling the microstructure and improving the tensile properties of extruded Mg–Sn–Zn alloy through Al addition. J Alloys Compd 751:1–1110.1016/j.jallcom.2018.04.063 ↗
17. Lee JY, Kim DH, Lim HK, Kim DH (2005) Effects of Zn/Y ratio on microstructure and mechanical properties of Mg–Zn–Y alloys. Mater Lett 59(29–30):3801–380510.1016/j.matlet.2005.06.052 ↗
18. Shen MJ, Wang XJ, Li CD, Zhang MF, Hu XS, Zheng MY, Wu K (2013) Effect of bimodal size SiC particulates on microstructure and mechanical properties of AZ31B magnesium matrix composites. Mater Des 52:1011–101710.1016/j.matdes.2013.05.067 ↗
19. Park SS, Kim YJ, Cheng WL, Kim YM (2011) Tensile properties of extruded Mg–8Sn–1Zn alloys subjected to different heat treatments. Philos Mag Lett 91(1):35–4210.1080/09500839.2010.523019 ↗
20. Yin SQ, Zhang ZQ, Liu X, Le QC, Lan Q, Bao L, Cui JZ (2017) Effects of Zn/Gd ratio on the microstructures and mechanical properties of Mg–Zn–Gd–Zr alloys. Mater Sci Eng, A 695:135–14310.1016/j.msea.2017.03.117 ↗
21. Xu DK, Liu L, Xu YB, Han EH (2007) Effect of microstructure and texture on the mechanical properties of the as-extruded Mg–Zn–Y–Zr alloys. Mater Sci Eng, A 443(1–2):248–25610.1016/j.msea.2006.08.037 ↗
22. Jiang MG, Xu C, Nakata T, Yan H, Chen RS, Kamado S (2016) Development of dilute Mg–Zn–Ca–Mn alloy with high performance via extrusion. J Alloy Compd 668:13–2110.1016/j.jallcom.2016.01.195 ↗
23. Oh-ishi K, Mendis CL, Homma T, Kamado S, Ohkubo T, Hono K (2009) Bimodally grained microstructure development during hot extrusion of Mg–2.4Zn–0.1Ag–0.1Ca–0.16Zr(at.%) alloys. Acta Mater 57(18):5593–560410.1016/j.actamat.2009.07.057 ↗
24. Bai Y, Cheng WL, Ma SC, Zhang J, Guo C, Zhang Y (2018) The influence of initial microstructure on the strengthening effect of extruded Mg–8Sn–4Zn–2Al alloys. Acta Metall Sin 31(5):487–49510.1007/s40195-017-0673-5 ↗
25. Zhang DF, Hu H-J, Pan FS, Yang MB, Zhang JP (2010) Numerical and physical simulation of new SPD method combining extrusion and equal channel angular pressing for AZ31 magnesium alloy. Trans Nonferr Metal Soc 20(3):478–48310.1016/S1003-6326(09)60165-5 ↗
26. Dumitru F-D, Higuera-Cobos OF, Cabrera JM (2014) ZK60 alloy processed by ECAP: microstructural, physical and mechanical characterization. Mater Sci Eng, A 594:32–3910.1016/j.msea.2013.11.050 ↗
27. Geng JW, Teng XY, Zhou GR, Zhao DG (2013) Microstructure transformations in the heat-treated Mg–Zn–Y alloy. J Alloy Compd 577:498–50610.1016/j.jallcom.2013.07.009 ↗
28. Li JC, He ZL, Fu PH, Wu YJ, Peng LM, Ding WJ (2016) Heat treatment and mechanical properties of a high-strength cast Mg–Gd–Zn alloy. Mater Sci Eng, A 651:745–75210.1016/j.msea.2015.11.021 ↗
29. Xu DK, Tang WN, Liu L, Xu YB, Han EH (2007) Effect of Y concentration on the microstructure and mechanical properties of as-cast Mg–Zn–Y–Zr alloys. J Alloy Compd 432(1–2):129–13410.1016/j.jallcom.2006.05.123 ↗
30. Singh A, Watanabe M, Kato A, Tsai AP (2004) Microstructure and strength of quasicrystal containing extruded Mg–Zn–Y alloys for elevated temperature application. Mater Sci Eng, A 385(1–2):382–39610.1016/S0921-5093(04)00903-7 ↗
31. Xu SW, Zheng MY, Kamado S, Wu K (2012) The microstructural evolution and superplastic behavior at low temperatures of Mg–5.00Zn–0.92Y–0.16Zr (wt%) alloys after hot extrusion and ECAP process. Mater Sci Eng, A 549:60–6810.1016/j.msea.2012.03.116 ↗
32. Bohlen J, Yi SB, Letzig D, Kainer KU (2010) Effect of rare earth elements on the microstructure and texture development in magnesium-manganese alloys during extrusion. Mater Sci Eng, A 527(26):7092–709810.1016/j.msea.2010.07.081 ↗
33. Huppmann M, Gall S, Müller S, Reimers W (2010) Changes of the texture and the mechanical properties of the extruded Mg alloy ME21 as a function of the process parameters. Mater Sci Eng, A 528(1):342–35410.1016/j.msea.2010.09.025 ↗
34. Chen HB, Liu TM, Zhang Y, Song B, Hou DW, Pan FS (2016) The yield asymmetry and precipitation behavior of pre-twinned ZK60 alloy. Mater Sci Eng, A 652:167–17410.1016/j.msea.2015.11.092 ↗
35. Wang XJ, Wu K, Zhang HF, Huang WX, Chang H, Gan WM, Zheng MY, Peng DL (2007) Effect of hot extrusion on the microstructure of a particulate reinforced magnesium matrix composite. Mater Sci Eng, A 465(1–2):78–84
36. Xu SW, Zheng MY, Kamado S, Wu K, Wang JG, Lv XY (2011) Dynamic microstructural changes during hot extrusion and mechanical properties of a Mg–5.0Zn–0.9Y–0.16Zr (wt%) alloy. Mater Sci Eng, A 528(12):4055–406710.1016/j.msea.2011.01.103 ↗
37. Jung J-G, Park SH, You BS (2015) Effect of aging prior to extrusion on the microstructure and mechanical properties of Mg–7Sn–1Al–1Zn alloy. J Alloys Compd 627:324–33210.1016/j.jallcom.2014.11.213 ↗
38. Xin YC, Wang MY, Zeng Z, Huang GJ, Liu Q (2011) Tailoring the texture of magnesium alloy by twinning deformation to improve the rolling capability. Scr Mater 64(10):986–98910.1016/j.scriptamat.2011.02.010 ↗
39. Figueiredo RB, Cetlin PR, Langdon TG (2007) The processing of difficult-to-work alloys by ECAP with an emphasis on magnesium alloys. Acta Mater 55(14):4769–477910.1016/j.actamat.2007.04.043 ↗
40. Wusatowska-Sarnek AM, Miura H, Sakai T (2002) Nucleation and microtexture development under dynamic recrystallization of copper. Mater Sci Eng, A 323(1–2):177–18610.1016/S0921-5093(01)01336-3 ↗
41. Jiang L, Jonas JJ, Mishra RK, Luo A, Sachdev AK, Godet S (2007) Twinning and texture development in two Mg alloys subjected to loading along three different strain paths. Acta Mater 55(11):3899–391010.1016/j.actamat.2007.03.006 ↗
42. Koike J, Kobayashi T, Mukai T, Watanabe H, Suzuki M, Maruyama K, Higashi K (2003) The activity of non-basal slip systems and dynamic recovery at room temperature in fine-grained AZ31B magnesium alloys. Acta Mater 51(7):2055–206510.1016/S1359-6454(03)00005-3 ↗