Precipitation of various oxides in ODS ferritic steels
Source abstract
Abstract
The reactive elements (Ti, Al and Zr) have been widely used for the improvement of the strength or the oxide resistance of ODS steels. In the present work, we studied the effect of the reactive elements on the precipitation of oxide particles, especially focusing upon the appropriate amount of the oxide composing elements, by addition of the large amounts of Y2O3 and reactive elements. The mechanically alloyed powders are annealed in a wide temperature range from 773 to 1423K and then analysed by various analysis methods (small-angle X-ray scattering and X-ray diffraction by synchrotron radiation X-ray, scanning transmission electron microscope combined with energy dispersion X-ray spectroscopy, high-resolution transmission microscopy and 3D-atom probe). Ti, Al and Zr enhanced the growth of oxide particles, opposite to the many studies of Ti- and Zr-added ODS steels, as a result of the addition of Y2O3 and these elements ten times larger than those for usual use. The nucleation and growth of oxide particles are discussed by simulating the critical radius of nucleation and the growth based on the LSW theory. Y4Zr3O12 is stable and easy to precipitate even at lower annealing temperature. All reactive elements enhance the growth of oxide particles because of their big molar volume as compared to that of Y2O3.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Fusion materials and technologies · High-Temperature Coating Behaviors · Nuclear Materials and Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (64)
Show source-provided references
1. Ukai S, Harada M, Okada H, Inoue M, Nomura S, Shikakura S, Asabe K, Nishida T, Fujiwara M (1993) Alloying design of oxide dispersion for long life FBRs core materials strengthened ferritic steel. J Nucl Mater 204:65–7310.1016/0022-3115(93)90200-I ↗
2. Ukai S, Mizuta S, Fujiwara M, Okuda T, Kobayashi T (2002) Development of 9Cr-ODS martensitic steel claddings for fuel pins by means of ferrite to austenite phase transformation. J Nucl Sci Tech 39(7):778–78810.1080/18811248.2002.9715260 ↗
3. Dubuisson P, Carlan YD, Garat V, Blat M (2012) ODS ferritic/martensitic alloys for sodium fast reactor fuel pin cladding. J Nucl Mater 428(1–3):6–1210.1016/j.jnucmat.2011.10.037 ↗
4. Ukai S, Fujiwara M (2002) Perspective of ODS alloys application in nuclear environments. J Nucl Mater 307–311(1):749–75710.1016/S0022-3115(02)01043-7 ↗
5. Lindau R, Möslang A, Rieth M, Klimiankou M, Materna-Morris E, Alamo A, Tavassoli A-A, Cayron C, Lancha A-M, Fernandez P, Baluc N, Schäublin R, Diegele E, Filacchioni G, Rensman J, Schaaf B, Lucon E, Dietz W (2005) Present development status of EUROFER and ODS-EUROFER for application in blanket concepts. Fus Eng Des 75–79:989–99610.1016/j.fusengdes.2005.06.186 ↗
6. Oksiuta Z, Olier P, Carlan YD, Baluc N (2009) Development and characterisation of a new ODS ferritic steel for fusion reactor application. J Nucl Mater 393:114–11910.1016/j.jnucmat.2009.05.013 ↗
7. Baluc N, Boutard J, Dudarev S, Rieth M, Correia JB, Fournier B, Henry J, Legendre F, Leguey T, Lewandowska M, Linday R, Marquis E, Muñoz A, Radiguet B, Oksiuta Z (2011) Review on the EFDA work programme on nano-structured ODS RAF steels. J Nucl Mater 417:149–15310.1016/j.jnucmat.2010.12.065 ↗
8. Ukai S, Oono N, Ohtsuka S, Kaito T, Sakamoto K, Torimaru T, Kiimura A, Hayashi S (2016) Development of FeCrAl-ODS Steels for ATF Cladding. In: Proceedings light water reactor (LWR) fuel performance meeting (TOP FUEL) 2016
9. Kim S, Ohtsuka S, Kaito T, Yamashita S, Inoue M, Asayama T, Shobu T (2011) Formation of nano-size oxide particles and δ-ferrite at elevated temperature in 9Cr-ODS steel. J Nucl Mater 417(1–3):209–21210.1016/j.jnucmat.2011.01.063 ↗
10. He P, Liu T, Möslang A, Lindau R, Ziegler R, Hoffmann J, Kurinskiy P, Commin L, Vladimirov P, Nikitenko S, Silveir M (2012) XAFS and TEM studies of the structural evolution of yttrium-enriched oxides in nanostructured ferritic alloys fabricated by a powder metallurgy process. Mater Chem Phys 136:990–99810.1016/j.matchemphys.2012.08.038 ↗
11. Oono N, Ukai S (2018) Precipitation of oxide particles in oxide dispersion strengthened (ODS) ferritic steels. Mater Trans 59(10):1651–165810.2320/matertrans.M2018110 ↗
12. Alinger M, Odette G, Hoelzer D (2004) The development and stability of Y–Ti–O nanoclusters in mechanically alloyed Fe–Cr based ferritic alloys. J Nucl Mater 239–333:382–38610.1016/j.jnucmat.2004.04.042 ↗
13. Hoelzer D, Bentley J, Sokolov M, Miller M, Odette G, Alinger M (2007) Influence of particle dispersions on the high-temperature strength of ferritic alloys. J Nucl Mater 367–370:166–17210.1016/j.jnucmat.2007.03.151 ↗
14. Ukai S, Ohtsuka S (2007) Nano-mesoscopic structure control in 9Cr-ODS ferritic steels. Energy Mater 2(1):26–3510.1179/174892407X210357 ↗
15. Kim I, Choi B, Kang C, Okuda T, Maziasz P, Miyahara K (2003) Effect of Ti and W on the mechanical properties and microstructure of 12% Cr base mechanical-alloyed nano-sized ODS ferritic alloys. ISIJ Int 43(10):1640–164610.2355/isijinternational.43.1640 ↗
16. Sakasegawa H, Legendre F, Boulanger L, Brocq M, Chaffron L, Cozzika T, Malaplate J, Henry J, Carlan YD (2011) Stability of non-stoichiometric clusters in the MA957 ODS ferrtic alloy. J Nucl Mater 417:229–23210.1016/j.jnucmat.2010.12.056 ↗
17. Ribis J, Carlan YD (2012) Interfacial strained structure and orientation relationships of the nanosized oxide particles deduced from elasticity-driven morphology in oxide dispersion strengthened materials. Acta Mater 60:238–25210.1016/j.actamat.2011.09.042 ↗
18. Hirata A, Fujita T, Wen Y, Schneibel J, Liu C, Chen M (2011) Atomic structure of nanoclusters in oxide-dispersion-strengthened steels. Nat Mater 10(12):922–92610.1038/nmat3150 ↗
19. Brocq M, Radiguet B, Poissonnet S, Cuvilly F, Pareige P, Legendre F (2011) Nanoscale characterization and formation mechanism of nanoclusters in an ODS steel elaborated by reactive-inspired ball-milling and annealing. J Nucl Mater 409:80–8510.1016/j.jnucmat.2010.09.011 ↗
20. Rogozhkin S, Orlov NN, Nikitin A, Aleev A, Zaluzhnyi A, Kozodaev M, Lindau R, Möslang A, Vladimirov P (2015) Nanoscale characterization of 13.5% Cr oxide dispersion strengthened steels with various titanium concentrations. Inorg Mater Appl Res 6(2):151–15510.1134/S2075113315020136 ↗
21. Liu S, Odette G, Segre C (2014) Evidence for core–shell nanoclusters in oxygen dispersion strengthened steels measured using X-ray absorption spectroscopy. J Nucl Mater 445:50–5610.1016/j.jnucmat.2013.10.042 ↗
22. Jiang Y, Smith J, Odette G (2009) Formation of Y–Ti–O nanoclusters in nanostructured ferritic alloys: a first-principles study. Phys Rev B 79:06410310.1103/PhysRevB.79.064103 ↗
23. Materials Database Group (2010) Inorganic material database (AtomWork). Natl Inst Mater Sci 06. [Online]. http://crystdb.nims.go.jp/index_en.html . Accessed 06 2017
24. Oba Y, Koppoju S, Ohnuma M, Murakami T, Hatano H, Sasakawa K, Kitahara A, Suzuki J (2011) Quantitative analysis of precipitate in vanadium-microalloyed medium carbon steels using small-angle X-ray and neutron scattering methods. ISIJ Int 51(11):1852–285810.2355/isijinternational.51.1852 ↗
25. Kogure T (2015) Geometry of electron diffraction and its calculation. Microsc (Jpn) 50(1):1–5
26. Bale CW, Bélisle E, Chartrand P, Decterov SA, Eriksson G, Hack K, Jung IH, Kang YB, Melançon J, Pelton AD, Robelin C, Petersen S (2009) FactSage thermochemical software and databases—recent developments. Calphad 33(2):295–31110.1016/j.calphad.2008.09.009 ↗
27. Adylov T, Voronov G, Mansurova E, Sigalov LM, Urazaeva E (1988) The Y2O3–Al2O3 system above 1473 K. Russ J Inorg Chem 33:1062–1063
28. Schaedler T, Fabrichanaya O, Levi C (2008) Phase equilibria in the TiO2–YO1.5–ZrO2 system. J Eur Ceram Soc 28:2509–252010.1016/j.jeurceramsoc.2008.03.011 ↗
29. Foëx M, Traverse J-P (1965) Étude à haute température des transformations allotropiques des sesquioexydes d’yttrium, d’erbium et de thulium. Comptes rendus hebdomadaires des séances de l’Académie des sciences 261(9):2490–2493
30. Buntushkin V, Romanovich I, Timofeeva N (1971) High-temperature microhardness and certain properties of refractory oxides. Inorg Mater 7(9):1456–1457
31. Red’ko V, Lopato L (1991) Magnetic Susceptibility Of M4ZR3O12 and M4HF3O12 (M-rare-earth element). Inorg Mater 27:1495–1497
32. Maister I, Lopato L, Zaitseva Z, Shevchenko A (1991) Interaction in the ZRO2-Y2O3-SC2O3 system at 1300–1900C. Inorg Mater 27(11):1997–2000
33. Kim D-J, Hyun S-H, Kim S-G, Yashima M (1994) Effective ionic radius of Y3 + determined from lattice parameters of fluorite-type HfO2 and ZrO2 solid solutions. J Am Ceram Soc 77(2):597–59910.1111/j.1151-2916.1994.tb07035.x ↗
34. Sharygin L, Galkin V, Vovk S, Dorofeev Y (1991) Solid solutions of the ZRO2-Y2O3 system produced by the sol–gel method. Inorg Mater 27(2):221–224
35. Skrikanth V, Sato A, Yoshimoto J, Kim J, Ikegami T (1994) Synthesis and crystal structure study of Y2O3 high-pressure polymorph. Cryst Res Technol 29(7):981–98410.1002/crat.2170290712 ↗
36. Andrievskaya ELLKVZZ (1996) Inorg Mater 32:645–653
37. Dolgikh V, Lavat E (1991) Russ J Inorg Chem 36:1389–1392
38. Bertaut F, Mareschal J, Hebd CR (1963) Seances Acad Sci 257:867–870
39. Zhou Y, Lu X, Xiang H, Feng Z (2015) Preparation, mechanical, and thermal properties of a promising thermal barrier material: Y4Al2O9. J Adv Ceram 4(2):94–10210.1007/s40145-015-0141-5 ↗
40. Larson D, Maziasz P, Kim I, Miyahara K (2001) Three-dimensional atom probe observation of nanoscale titanium-oxygen clustering in an oxide-dispersion-strengthened Fe–12Cr–3W–0.4Ti + Y2O3 ferritic alloy. Scr Mater 44:359–36410.1016/S1359-6462(00)00593-5 ↗
41. Miller M, Russell K, Hoelzer D (2006) Characterization of precipitates in MA/ODS ferritic alloys. J Nucl Mater 351:261–26810.1016/j.jnucmat.2006.02.004 ↗
42. London A, Santra S, Amirthapandian S, Panigrahi B, Sarguna R, Balaji S, Vijay R, Sundar C, Lozano-Perez S, Grovenor C (2015) Effect of Ti and Cr on dispersion, structure and composition of oxide nano-particles in model ODS alloys. Acta Mater 97:223–23310.1016/j.actamat.2015.06.032 ↗
43. Boulant X, Perez M, Fabrègue D, Cazottes S, de Carlan Y (2016) Characterization and modeling of oxides precipitation in ferritic steels during fast non-isothermal consolidation. Acta Mater 107:390–40310.1016/j.actamat.2016.01.034 ↗
44. Pavlina EJ, Speer JG, Van Tyne CJ (2012) Equilibrium solubility products of molybdenum carbide and tungsten carbide in iron. Scr Mater 66:243–24610.1016/j.scriptamat.2011.10.047 ↗
45. Dou P, Kimura A, Kasasda R, Okuda T, Inoe M, Ukai S, Ohnuki S, Fujisawa T, Abe F (2014) TEM and HRTEM study of oxide particles in an Al-alloyed high-Cr oxide dispersion strengthened steel with Zr addition. J Nucl Mater 444:441–45310.1016/j.jnucmat.2013.10.028 ↗
46. Oono N, Tang Q, Ukai S (2016) Oxide particle refinement in Ni-based ODS alloy. Mater Sci Eng A 649:250–25310.1016/j.msea.2015.09.094 ↗
47. Schuler T, Nastar M, Soisson F (2017) Vacancy-induced dissolution of precipitates in out-of-equilibrium systems: a test case of FeX (X = C, N, O) alloys. Phys Rev B 95(1):1–1310.1103/PhysRevB.95.014113 ↗
48. Latella B, Humphries S (2004) Young’s modulus of a 2.25Cr–1Mo steel at elevated temperature. Scr Mater 51:635–63910.1016/j.scriptamat.2004.06.028 ↗
49. Elsukov E, Voronina E, Barinov V (1992) J Magn Magn Mater 115:271–28010.1016/0304-8853(92)90069-Z ↗
50. Skandan G, Foster C, Frase H, Ali MN, Parker JC, Hahn H (1992) Phase characterization and stabilization due to grain size effects of nanostructured Y2O3. Nanostruct Mater 1(4):313–32210.1016/0965-9773(92)90038-Y ↗
51. Villars P, Cenzual K (eds) Y2Ti2O7 Crystal Structur: datasheet from “PAULING FILE multinaries edition - 2012”. Springer, Hidelberg and Material Phases Data System (MDPS), Switzerland & National Institute for Materials Science (NIMS), Japan, 2016. [Online]. https://materials.springer.com/isp/crystallographic/docs/sd_1903246 . Accessed 18 Dec 2018
52. Persson KA (2016) “Materials data on Y4Al2O9 (SG: 14)” Materials Project, United States. [Online]. https://doi.org/10.17188/1264857 . Accessed Dec 18 201810.17188/1264857 ↗
53. Oono N, Nakamura K, Ukai S, Kaito T, Torimaru T, Kimura A, Hayashi S (2016) Oxide particle coarsening at temperature over 1473 K in 9CrODS steel. Nucl Mater Energy 9:342–34510.1016/j.nme.2016.06.008 ↗
54. Villars P, Cenzual K (2012) YAlO3; YAP (YAlO3 rt) crystal structure: datasheet from “PAULING FILE Multinaries Edition – 2012”. In: SpringerMaterials. Springer, Berlin & Material Phases Data System (MPDS), Switzerland & National Institute for Materials Science (NIMS), Japan, 2012. [Online]. https://materials.springer.com/isp/crystallographic/docs/sd_1924024 . Accessed 18 Dec 2018
55. Persson KA (2014) “Materials data on Y4Zr3O12 (SG:2)” Materials Project. United States. [Online]. https://doi.org/10.17188/1282854 . Accessed 28 Dec 201810.17188/1282854 ↗
56. Oono NH, Ukai S, Hayashi S, Ohtsuka S, Kaito T, Kimura A, Torimaru T, Sakamoto K (2017) Growth of oxide particles in FeCrAl- oxide dispersion strengthened steels at high temperature. J Nucl Mater J 493:180–18810.1016/j.jnucmat.2017.06.018 ↗
57. Wagner C (1961) Theorie der Alterung von Niederschlägen durch Umlösen (Ostwald-Reifung). Zeitschrift für Elektrochemie 65(7):581–591
58. Rios PR (1993) Quasi-stoichiometric coarsening of f.c.c. carbides in microalloyed austenite containing niobium and vanadium. Mater Sci Eng A 171(1–2):175–17910.1016/0921-5093(93)90404-3 ↗
59. Zhang W, Liu G, Han K (1986) Fe–Y (iron–yttrium). In: Massalski TB (ed) Binary alloy phase diagrams, vol 2. Fe–Ru to Zn–Zr. American Society for Metals, Metals Park, pp 1793–1794
60. Darken LS, Gurry RW (1946) The system iron—oxygen. II. Equilibrium and thermodynamics of liquid oxide and other phases. J Am Chem Soc 68(5):798–81610.1021/ja01209a030 ↗
61. Alinger MJ (2004) On the formation and stability of nanometer scale precipitates in ferritic alloys during processing and high temperature service. University of California Santa Barbara, California
62. Hirvonen J, Räisänen J (1982) Diffusion of aluminum in ion-implanted alpha iron. J Appl Phys 53:3314–331610.1063/1.330990 ↗
63. Murali D, Panigrahi B, Valsakumar M, Sundar C (2011) Diffusion of Y and Ti/Zr in bcc iron: a first principles study. J Nucl Mater 419:208–21210.1016/j.jnucmat.2011.05.018 ↗
64. Klugkist P, Herzig C (1995) Tracer diffusion of titanium in α-iron. Phys Stat Solidi (a) 148:413–42110.1002/pssa.2211480209 ↗