journal article·2017-02

Influences of heat treatment on microstructural evolution and tensile behavior of squeeze-cast Mg–Gd–Y–Zr alloy

Cunlong Wang, Guohua Wu, Enrique J. Lavernia, Wenjiang Ding

Journal of Materials Science· Volume 52· Issue 4
Publisher page

Abstract

The effects of solution heat treatment and aging on the microstructural evolution and mechanical behavior of a squeeze-cast (SC) Mg–10Gd–3Y–0.5Zr (GW103K) alloy, processed using various applied pressures (e.g., 0.1, 40, 80 and 160 MPa) were systematically investigated. Our results show that, after solution heat treatment, secondary phases and pressure-induced dislocations are dissolved in the matrix of the squeeze-cast alloys. Moreover, subsequent aging heat treatment leads to an increased age-hardening response relative to that in squeeze-cast GW103K and this trend increases with increasing applied pressure. The room temperature tensile test results show that the yield strength (YS) for the squeeze-cast alloy in the as-cast, the as-T4 heat-treated and the as-T6 heat-treated states increases with increasing applied pressure, from 0.1 to 80 MPa, and remains relatively constant when the applied pressure is increased to 160 MPa, whereas the ultimate tensile strength (UTS) and elongation-to-failure (E f) increases continuously with increasing applied pressure. The measured increases in YS and UTS (or E f), are discussed in terms of the mechanisms that govern the evolution of microstructure in squeeze-cast GW103K, paying particular attention to gain size and porosity.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Magnesium Alloys: Properties and Applications · Aluminum Alloys Composites Properties · Aluminum Alloy Microstructure Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (28)

Show source-provided references
1. Dai J, Zhu S, Easton MA, Zhang M, Qiu D, Wu G, Liu W, Ding W (2013) Heat treatment, microstructure and mechanical properties of a Mg–Gd–Y alloy grain-refined by Al additions. Mater Sci Eng A 576:298–305. doi: 10.1016/j.msea.2013.04.01610.1016/j.msea.2013.04.016 ↗
2. Nie J-F (2012) Precipitation and hardening in magnesium alloys. Metall Mater Trans A 43(11):3891–3939. doi: 10.1016/j.jma.2014.01.01010.1016/j.jma.2014.01.010 ↗
3. Wang C, Dai J, Liu W, Zhang L, Wu G (2015) Effect of Al additions on grain refinement and mechanical properties of Mg–Sm alloys. J Alloy Compd 620:172–179. doi: 10.1016/j.jallcom.2014.09.02510.1016/j.jallcom.2014.09.025 ↗
4. Wang C, Chen A, Zhang L, Liu W, Wu G, Ding W (2015) Preparation of an Mg–Gd–Zn alloy semisolid slurry by low frequency electro-magnetic stirring. Mater Des 84:53–63. doi: 10.1016/j.matdes.2015.06.12610.1016/j.matdes.2015.06.126 ↗
5. Xu W, Zhang Y, TerBush JR, Peng L, Ding W, Nie J (2014) Effects of alloying elements on creep properties of Mg-Gd-Zr alloys. Metall Mater Trans A. doi: 10.1007/s11661-014-2335-910.1007/s11661-014-2335-9 ↗
6. Wang C, Lavernia EJ, Wuuu G, Liuuu W, Ding W (2016) Influence of pressure and temperature on microstructure and mechanical behavior of squeeze cast Mg–10Gd–3Y–05Zr alloy. Metall Mater Trans A 47(8):4104–4115. doi: 10.1007/s11661-016-3546-z10.1007/s11661-016-3546-z ↗
7. Guo Y, Li J, Li J, Yang Z, Zhao J, Xia F, Liang M (2008) Mg–Gd–Y system phase diagram calculation and experimental clarification. J Alloy Compd 450(1–2):446–451. doi: 10.1016/j.jallcom.2006.10.12510.1016/j.jallcom.2006.10.125 ↗
8. He SM, Zeng XQ, Peng LM, Gao X, Nie JF, Ding WJ (2006) Precipitation in a Mg–10Gd–3Y–0.4Zr (wt%) alloy during isothermal ageing at 250°C. J Alloy Compd 421(12):309–313. doi: 10.1016/j.jallcom.2005.11.04610.1016/j.jallcom.2005.11.046 ↗
9. Dai J, Zhu S, Easton MA, Xu W, Wu G, Ding W (2014) Precipitation process in a Mg–Gd–Y alloy grain-refined by Al addition. Mater Characterization 88:7–14. doi: 10.1016/j.matchar.2013.10.01010.1016/j.matchar.2013.10.010 ↗
10. Liu WC, Cao L, Zhang S, Nodooshan H, Wu GH, Ding WJ (2013) High temperature mechanical properties of sand-Cast Mg–Gd–Y magnesium alloy. In: Wohlbier FH (ed) Materials Science Forum. Trans Tech Publ, Pfaffikon, pp 543–548
11. Xiao HC, Jiang SN, Tang B, Hao WH, Gao YH, Chen ZY, Liu CM (2015) Hot deformation and dynamic recrystallization behaviors of Mg–Gd–Y–Zr alloy. Mater Sci Eng A 628:311–318. doi: 10.1016/j.msea.2015.01.04110.1016/j.msea.2015.01.041 ↗
12. Masoumi M, Hu H (2011) Influence of applied pressure on microstructure and tensile properties of squeeze cast magnesium Mg-Al-Ca alloy. Mater Sci Eng A 528(10–11):3589–3593. doi: 10.1016/j.msea.2011.01.03210.1016/j.msea.2011.01.032 ↗
13. Ghomashchi MR, Vikhrov A (2000) Squeeze casting: an overview. J Mate Process Technol 101(1–3):1–9. doi: 10.1016/S0924-0136(99)00291-510.1016/S0924-0136(99)00291-5 ↗
14. Heee SM, Zeng XQ, Peng LM, Gao X, Nie JF, Ding WJ (2007) Microstructure and strengthening mechanism of high strength Mg–10Gd–2Y–0.5Zr alloy. J Alloy Compd 427(1–2):316–323. doi: 10.1016/j.jallcom.2006.03.01510.1016/j.jallcom.2006.03.015 ↗
15. Ming S, Guohua W, Wei W, Wenjiang D (2009) Effect of Zr on the microstructure, mechanical properties and corrosion resistance of Mg-10Gd-3Y magnesium alloy. Mater Sci Eng A 523(1–2):145–151. doi: 10.1016/j.msea.2009.06.00210.1016/j.msea.2009.06.002 ↗
16. Gao L, Chen RS, Han EH (2009) Effects of rare-earth elements Gd and Y on the solid solution strengthening of Mg alloys. J Alloy Compd 481(1–2):379–384. doi: 10.1016/j.jallcom.2009.02.13110.1016/j.jallcom.2009.02.131 ↗
17. Gao L, Chen RS, Han EH (2009) Microstructure and strengthening mechanisms of a cast Mg–1.48Gd–1.13Y–0.16Zr (at%) alloy. J Mater Sci 44(16):4443–4454. doi: 10.1007/s10853-009-3672-810.1007/s10853-009-3672-8 ↗
18. Caceres C, Lukáč P (2008) Strain hardening behaviour and the Taylor factor of pure magnesium. Philos Mag 88(7):977–98910.1080/14786430801968611 ↗
19. Handbook AS (1999) Magnesium and magnesium alloys. ASM Int, Russell, pp 106–118
20. Wen H, Topping TD, Isheim D, Seidman DN, Lavernia EJ (2013) Strengthening mechanisms in a high-strength bulk nanostructured Cu–Zn–Al alloy processed via cryomilling and spark plasma sintering. Acta Mater 61(8):2769–2782. doi: 10.1016/j.actamat.2012.09.03610.1016/j.actamat.2012.09.036 ↗
21. Űnal O, Tiryakioğlu M (2015) On the ductility potential and assessment of structural quality in Mg alloy castings. Mater Sci Eng A 643:51–54. doi: 10.1016/j.msea.2015.07.00310.1016/j.msea.2015.07.003 ↗
22. Cáceres CH (1995) On the effect of macroporosity on the tensile properties of the Al–7%Si–0.4%Mg casting alloy. Scr Metall Mater 32(11):1851–1856. doi: 10.1016/0956-716X(95)00031-P10.1016/0956-716X(95)00031-P ↗
23. Zhang Q, Masoumi M, Hu H (2012) Influence of applied pressure on tensile behaviour and microstructure of squeeze cast Mg alloy AM50 with Ca addition. J Mater Eng Perform 21(1):38–46. doi: 10.1007/s11665-010-9810-210.1007/s11665-010-9810-2 ↗
24. Cáceres CH, Selling BI (1996) Casting defects and the tensile properties of an AlSiMg alloy. Mater Sci Eng A 220(1–2):109–116. doi: 10.1016/S0921-5093(96)10433-010.1016/S0921-5093(96)10433-0 ↗
25. Weiler JP, Wood JT (2012) Modeling the tensile failure of cast magnesium alloys. J Alloy Compd 537:133–140. doi: 10.1016/j.jallcom.2012.05.09010.1016/j.jallcom.2012.05.090 ↗
26. Meyers MA, Chawla KK (2009) Mechanical behavior of materials, vol 2. Cambridge University Press, Cambridge, pp 165–167
27. Lee CD, Shin KS (2014) Constitutive prediction of the defect susceptibility of tensile properties to microporosity variation in A356 aluminum alloy. Mater Sci Eng A 599:223–232. doi: 10.1016/j.msea.2014.01.09110.1016/j.msea.2014.01.091 ↗
28. Lee CD, Shin KS (2007) Effect of microporosity on the tensile properties of AZ91 magnesium alloy. Acta Mater 55(13):4293–4303. doi: 10.1016/j.actamat.2007.03.02610.1016/j.actamat.2007.03.026 ↗