journal article·2014-11

Characterization of porous graphitic monoliths from pyrolyzed wood

A. Gutiérrez-Pardo, J. Ramírez-Rico, A. R. de Arellano-López, J. Martínez-Fernández

Journal of Materials Science· Volume 49· Issue 22
Publisher page

Abstract

Porous graphitic carbons were obtained from wood precursors using Ni as a graphitization catalyst during pyrolysis. The structure of the resulting material retains that of the original wood precursors with highly aligned, hierarchical porosity. Thermal characterization was performed by means of thermogravimetry and differential scanning calorimetry, and the onset temperature for graphitization was determined to be ~900 °C. Structural and microstructural characterization was performed by means of electron microscopy, electron and x-ray diffraction, and Raman spectroscopy. The effect of maximum pyrolysis temperature on the degree of graphitization was assessed. No significant temperature effect was detected by means of Raman scattering in the range of 1000–1400 °C, but at temperatures over the melting point of the catalyst, the formation of graphite grains with long-range order was detected.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Supercapacitor Materials and Fabrication · Fiber-reinforced polymer composites · Lignin and Wood Chemistry

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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