journal article·2012-01

Probing material properties with sharp indenters: a retrospective

Brian R. Lawn, Robert F. Cook

Journal of Materials Science· Volume 47· Issue 1
Publisher page

Abstract

A retrospective on the use of sharp, fixed-profile indenters as materials probes is presented. Indentation is proposed as a simple but powerful methodology for evaluating basic mechanical properties—elastic modulus, hardness, toughness—in all classes of materials. Indentation also provides unique insight into fundamental deformation and fracture processes. Of particular interest is the existence of intrinsic size effects as characteristic contact dimensions pass from macro- to micro- to nano-scale dimensions. The utility of indentations as ‘controlled flaws’ in the context of strength of materials is outlined. The roles of two other important material factors—rate effects and microstructure—are considered. Examples of technological and biological applications are presented as illustrations of the widespread power of the technique. Strengths and limitations of the methodology as a routine testing protocol are discussed.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Metal and Thin Film Mechanics · Force Microscopy Techniques and Applications · Adhesion, Friction, and Surface Interactions

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (100+)

Show source-provided references
1. Hertz H (1896) Hertz’s miscellaneous papers. Macmillan, London Chs. 5, 6
2. Tabor D (1951) Hardness of metals. Clarendon, Oxford
3. Samuels LE, Mulhearn TO (1957) J Mech Phys Solids 5:12510.1016/0022-5096(57)90056-X ↗
4. Johnson KL (1985) Contact mechanics. Cambridge University Press, London10.1017/CBO9781139171731 ↗
5. Lawn BR, Wilshaw TR (1975) J Mater Sci 10:1049. doi: 10.1007/BF0082322410.1007/BF00823224 ↗
6. Ostojic P, McPherson R (1987) Int J Fract 33:29710.1007/BF00044418 ↗
7. Cook RF, Pharr GM (1990) J Am Ceram Soc 73:78710.1111/j.1151-2916.1990.tb05119.x ↗
8. Johnson K (1982) Proc Inst Mech Eng Tribol 196:36310.1243/PIME_PROC_1982_196_039_02 ↗
9. Lawn BR (1998) J Am Ceram Soc 81:197710.1111/j.1151-2916.1998.tb02580.x ↗
10. Hill R (1950) The mathematical theory of plasticity. Oxford University Press, London
11. Lawn BR (2004) J Mater Res 19:2210.1557/jmr.2004.19.1.22 ↗
12. Sneddon IN (1948) Math Proc Camb Philos Soc 44:49210.1017/S0305004100024518 ↗
13. Marsh DM (1964) Proc R Soc Lond A282:3310.1098/rspa.1964.0210 ↗
14. Johnson KL (1970) J Mech Phys Solids 18:11510.1016/0022-5096(70)90029-3 ↗
15. Stilwell NA, Tabor D (1961) Proc Phys Soc Lond 78:16910.1088/0370-1328/78/2/302 ↗
16. Lawn BR, Howes VR (1981) J Mater Sci 16:2745. doi: 10.1007/BF0240283710.1007/BF02402837 ↗
17. Marshall DB, Noma T, Evans AG (1982) J Am Ceram Soc 65:C17510.1111/j.1151-2916.1982.tb10357.x ↗
18. Loubet JJ, Georges JM, Meille G (1983) In: Blau PJ, Lawn BR (eds) Micro indentation hardness testing. A.S.T.M. Special Technical Publication 899, Philadelphia, PA, p 72
19. Pharr GM, Cook RF (1990) J Mater Res 5:84710.1557/JMR.1990.0847 ↗
20. Cook RF, Oyen ML (2007) Int J Mater Res 98:37010.3139/146.101480 ↗
21. Thurn J, Morris DJ, Cook RF (2002) J Mater Res 17:267910.1557/JMR.2002.0388 ↗
22. Arora A, Marshall DB, Lawn BR, Swain MV (1979) J Non Cryst Solids 31:41510.1016/0022-3093(79)90154-6 ↗
23. Hagan JT (1979) J Mater Sci 14:462. doi: 10.1007/BF0058984010.1007/BF00589840 ↗
24. Minomura S, Drickamer HG (1962) J Phys Chem Solids 23:45110.1016/0022-3697(62)90085-9 ↗
25. Latella BA, O’Connor BH, Padture NP, Lawn BR (1997) J Am Ceram Soc 80:102710.1111/j.1151-2916.1997.tb02940.x ↗
26. Toivola Y, Stein A, Cook RF (2004) J Mater Res 19:26010.1557/jmr.2004.19.1.260 ↗
27. Zhang J, Wong T-F, Davis DM (1990) J Geophys Res 95:34110.1029/JB095iB01p00341 ↗
28. Oyen ML, Cook RF (2003) J Mater Res 18:13910.1557/JMR.2003.0020 ↗
29. Yoffe E (1982) Philos Mag A 46:61710.1080/01418618208236917 ↗
30. Atkins AG, Silverio A, Tabor D (1966) J Inst Met 94:369
31. Brookes CA, O’Neil JB, Redfern BAW (1971) Proc R Soc Lond 322:7310.1098/rspa.1971.0055 ↗
32. Hockey BJ, Lawn BR (1975) J Mater Sci 10:1275. doi: 10.1007/BF0054081610.1007/BF00540816 ↗
33. Lawn BR, Swain MV (1975) J Mater Sci 10:113. doi: 10.1007/BF0054103810.1007/BF00541038 ↗
34. Evans AG, Wilshaw TR (1976) Acta Metall 24:93910.1016/0001-6160(76)90042-0 ↗
35. Lawn BR, Fuller ER (1975) J Mater Sci 10:2016. doi: 10.1007/BF0055747910.1007/BF00557479 ↗
36. Hagan JT, Swain MV (1978) J Phys D 11:209110.1088/0022-3727/11/15/007 ↗
37. Lawn BR, Marshall DB (1984) J Natl Bur Stand 89:43510.6028/jres.089.024 ↗
38. Shetty DK, Wright IG, Mincer PN, Clauer AH (1985) J Mater Sci 20:1873. doi: 10.1007/BF0055529610.1007/BF00555296 ↗
39. Marshall DB, Lawn BR (1979) J Mater Sci 14:2001. doi: 10.1007/BF0055104310.1007/BF00551043 ↗
40. Lawn BR, Evans AG, Marshall DB (1980) J Am Ceram Soc 63:57410.1111/j.1151-2916.1980.tb10768.x ↗
41. Marshall DB, Lawn BR, Evans AG (1982) J Am Ceram Soc 65:56110.1111/j.1151-2916.1982.tb10782.x ↗
42. Wiederhorn SM, Hockey BJ (1983) J Mater Sci 18:766. doi: 10.1007/BF0074557510.1007/BF00745575 ↗
43. Anstis GR, Chantikul P, Marshall DB, Lawn BR (1981) J Am Ceram Soc 64:53310.1111/j.1151-2916.1981.tb10320.x ↗
44. Palmqvist S (1957) Jernkontorets Ann 141:300
45. Nihara K (1983) J Mater Sci Lett 2:22110.1007/BF00725625 ↗
46. Laugier MT (1985) J Am Ceram Soc 68:C-5110.1111/j.1151-2916.1985.tb15281.x ↗
47. Ponton CB, Rawlings RD (1989) Mater Sci Technol 5:86510.1179/mst.1989.5.9.865 ↗
48. Ponton CB, Rawlings RD (1989) Mater Sci Technol 5:96110.1179/mst.1989.5.10.961 ↗
49. Evans AG, Charles EA (1976) J Am Ceram Soc 59:37110.1111/j.1151-2916.1976.tb10991.x ↗
50. Lawn BR, Jensen T, Arora A (1976) J Mater Sci 11:573. doi: 10.1007/BF0054094010.1007/BF00540940 ↗
51. Lawn BR, Marshall DB (1979) J Am Ceram Soc 62:34710.1111/j.1151-2916.1979.tb19075.x ↗
52. Swain MV, Hagan JT (1976) J Phys D Appl Phys 9:220110.1088/0022-3727/9/15/011 ↗
53. Hagan JT (1979) J Mater Sci 14:2975. doi: 10.1007/BF0061148210.1007/BF00611482 ↗
54. Hagan JT (1980) J Mater Sci 15:1417. doi: 10.1007/BF0075212110.1007/BF00752121 ↗
55. Lawn BR, Dabbs TP, Fairbanks CJ (1983) J Mater Sci 18:2785. doi: 10.1007/BF0054759610.1007/BF00547596 ↗
56. Lawn BR, Evans AG (1977) J Mater Sci 12:2195. doi: 10.1007/BF0055224010.1007/BF00552240 ↗
57. Fischer-Cripps AC (2002) Nanoindentation. Springer-Verlag, New York10.1007/978-0-387-22462-6 ↗
58. Oliver WC, Pharr GM (1992) J Mater Res 7:156410.1557/JMR.1992.1564 ↗
59. Field JS, Swain MV (1993) J Mater Res 8:29710.1557/JMR.1993.0297 ↗
60. Pharr GM, Harding DS, Oliver WC (1993) In: Nastasi M, Parkin DM, Gleiter H (eds) Mechanical properties and deformation behavior of materials having ultra-fine microstructures. Kluwer Academic Publishers, Dordrecht, p 44910.1007/978-94-011-1765-4_29 ↗
61. Pharr GM (1998) Mater Sci Eng A253:15110.1016/S0921-5093(98)00724-2 ↗
62. Morris DJ, Cook RF (2004) J Am Ceram Soc 87:149410.1111/j.1551-2916.2004.01494.x ↗
63. Morris DJ, Cook RF (2004) Int J Fract 136:23710.1007/s10704-005-6034-9 ↗
64. Morris DJ, Vodnik AM, Cook RF (2004) Int J Fract 136:26510.1007/s10704-005-6033-x ↗
65. Doerner MF, Nix WD (1986) J Mater Res 1:60110.1557/JMR.1986.0601 ↗
66. McColm IJ (1990) Ceramic hardness. Plenum, New York10.1007/978-1-4757-4732-4 ↗
67. Nix WD, Gao H (1998) J Mech Phys Solids 46:41110.1016/S0022-5096(97)00086-0 ↗
68. Ma Q, Clarke DR (1995) J Mater Res 10:85310.1557/JMR.1995.0853 ↗
69. Fleck NA, Muller GM, Ashby MF, Hutchinson JW (1994) Acta Metall Mater 42:47510.1016/0956-7151(94)90502-9 ↗
70. Gane N, Bowden FP (1970) J Appl Phys 39:143210.1063/1.1656376 ↗
71. Hill MJ, Rowcliffe DJ (1974) J Mater Sci 9:1569. doi: 10.1007/BF0054075310.1007/BF00540753 ↗
72. Clarke DR, Kroll MC, Kirchner PD, Cook RF, Hockey BJ (1988) Phys Rev Lett 60:215610.1103/PhysRevLett.60.2156 ↗
73. Page TF, Oliver WC, McHargue CJ (1992) J Mater Res 7:45010.1557/JMR.1992.0450 ↗
74. Stach EA, Freeman T, Minor AM, Owen DK, Cumings J, Wall MA, Chraska T, Hull R, Morris JW, Zettl A (2001) Microsc Microanal 7:50710.1007/S10005-001-0012-4 ↗
75. Bradby JG, Williams JS, Wong-Leung J, Swain MV, Munroe P (2001) J Mater Res 16:150010.1557/JMR.2001.0209 ↗
76. Bradby JG, Williams JS, Wong-Leung J, Kucheyev SO, Swain MV, Munroe P (2002) Philos Mag A 82:193110.1080/01418610208235705 ↗
77. Zarudi I, Zhang LC, Swain MV (2003) J Mater Res 18:75810.1557/JMR.2003.0104 ↗
78. Piermarini G, Block S (1975) Rev Sci Instrum 46:97310.1063/1.1134381 ↗
79. Domnich V, Gogotsi Y, Dub S (2000) Appl Phys Lett 76:221410.1063/1.126300 ↗
80. Domnich V, Gogotsi Y (2002) Rev Adv Mater Sci 3:110.1016/S1468-6996(01)00150-4 ↗
81. Jang J, Lance MJ, Wen S, Tsui TY, Pharr GM (2005) Acta Mater 53:175910.1016/j.actamat.2004.12.025 ↗
82. Gerbig YB, Stranick SJ, Cook RF (2011) Phys Rev B 83:20520910.1103/PhysRevB.83.205209 ↗
83. Oliver DJ, Bradby JE, Willliams JS, Swain MV, Munroe P (2007) J Appl Phys 101:04352410.1063/1.2490563 ↗
84. Cottrell AH (1964) The mechanical properties of matter. Wiley, New York
85. Griffith AA (1920) Philos Trans R Soc Lond A221:163
86. Kelly A (1966) Strong solids. Clarendon Press, Oxford
87. Lawn BR (1983) In: Bradt RC, Evans AG, Hasselman DPH, Lange FF (eds) Fracture mechanics of ceramics, vol 5. Plenum, New York, p 110.1007/978-1-4613-3488-0_1 ↗
88. Marshall DB, Lawn BR, Chantikul P (1979) J Mater Sci 14:2225. doi: 10.1007/BF0068842910.1007/BF00688429 ↗
89. Lawn BR (1993) Fracture of brittle solids. Cambridge University Press, Cambridge10.1017/CBO9780511623127 ↗
90. Lawn BR, Wiederhorn SM, Johnson H (1975) J Am Ceram Soc 58:42810.1111/j.1151-2916.1975.tb19015.x ↗
91. Lawn BR, Fuller ER, Wiederhorn SM (1976) J Am Ceram Soc 59:19310.1111/j.1151-2916.1976.tb10930.x ↗
92. Lawn BR, Marshall DB (1978) In: Bradt RC, Hasselman DPH, Lange FF (eds) Fracture mechanics of ceramics, vol 3. Plenum, New York, p 205
93. Wiederhorn SM, Lawn BR (1979) J Am Ceram Soc 62:6610.1111/j.1151-2916.1979.tb18808.x ↗
94. Wiederhorn SM, Marshall DB, Lawn BR (1979) J Am Ceram Soc 62:7110.1111/j.1151-2916.1979.tb18809.x ↗
95. Cook RF, Lawn BR (1983) J Am Ceram Soc 66:C20010.1111/j.1151-2916.1983.tb10571.x ↗
96. Jung Y-G, Pajares A, Banerjee R, Lawn BR (2004) Acta Mater 52:345910.1016/j.actamat.2004.03.043 ↗
97. Dabbs TP, Marshall DB, Lawn BR (1980) J Am Ceram Soc 63:22410.1111/j.1151-2916.1980.tb10696.x ↗
98. Dabbs TP, Lawn BR (1985) J Am Ceram Soc 68:56310.1111/j.1151-2916.1985.tb16156.x ↗
99. Pajares A, Chumakov M, Lawn BR (2004) J Mater Res 19:65710.1557/jmr.2004.19.2.657 ↗
100. Fairbanks CJ, Polvani RS, Wiederhorn SM, Hockey BJ, Lawn BR (1982) J Mater Sci Lett 1:39110.1007/BF00724848 ↗