journal article·2000-12

Ambient-dried silica aerogel doped with TiO2 powder for thermal insulation

Young-Geun Kwon, Se-Young Choi, Eul-Son Kang, Seung-Su Baek

Journal of Materials Science· Volume 35· Issue 24
Publisher page

Abstract

Two step-derived SiO2 sol doped with TiO2 powder dissolved in ethanol was prepared. After aging and washing of wet gel, surface modification with TMCS (trimethylchlorosilane) was followed to prevent additional condensation reaction during drying. Ambient-dried SiO2-TiO2 gel was heat-treated at various temperatures. The effects of the heat-treated temperature on the chemical bonding state of SiO2-TiO2 gel were investigated by means of FTIR and XRD analyses. After heat-treatment at 350 °C, crack-free SiO2-TiO2 gel was synthesized with density of 0.14 g/cm3, porosity of 94%, and specific surface area of 613 m2/g. Ambient-dried SiO2-TiO2 gel heat-treated at 350 °C exhibited thermal conductivities of 0.0136 W/m·K and 0.0284 W/m·K at room temperature and 400 °C, respectively.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Synthesis and properties of polymers · Engineering Applied Research · Aerogels and thermal insulation

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (14)

Show source-provided references
1. J. FRICKE and T. TILLOTSON, Thin Solid Films 297 (1997) 212.10.1016/S0040-6090(96)09441-2 ↗
2. J. KUHN, T. GLEISSNER, M. C. ARDUINI-SCHUSTER, S. KORDER and J. FRICKE, J. Non-Cryst. Solids 186 (1995) 291.10.1016/0022-3093(95)00067-4 ↗
3. D. J. KIM and S. H. HYUN, J. Kor. Ceram. Soc. 33(5) (1996) 485.
4. D. M. SMITH, R. DESHPANDE and C. J. BRINKER, Mat. Res. Soc. Symp. Proc. 271 (1992) 567.10.1557/PROC-271-567 ↗
5. S. K. KANG and S. Y. CHOI, J. Kor. Ceram. Soc. 33(12) (1996) 1394.
6. H. S. YANG and S. Y. CHOI, ibid. 34(2) (1997) 188.
7. H. S. YANG, S. Y. CHOI, S. H. HYUN, H. H. PARK and J. K. HONG, J. Non-Cryst. Solids 221 (1997) 151.10.1016/S0022-3093(97)00335-9 ↗
8. S. K. KANG and S. Y. CHOI, J. Mat. Sci., submitted.
9. H. S. YANG, S. Y. CHOI, S. H. HYUN and C. G. PARK, Thin Solid Films 348 (1999) 69.10.1016/S0040-6090(99)00016-4 ↗
10. Y. G. KWON, S. Y. CHOI and S. K. KANG, J. Kor. Ceram. Soc. 36(11) (1999) 1189.
11. S. LOWELL and J. E. SHIELDS, “Powder Surface Area and Porosity” (Chapman & Hall, 1991) p. 52.10.1007/978-94-015-7955-1_8 ↗
12. H. B. EBERT, V. BOCK, O. NILSSON and J. FRICKE, High Temp.-High Press. 25 (1993) 113.
13. R. K. ILER, “The Chemistry of Silica” (John Wiley & Sons, Inc., 1979) p. 622.
14. Z. DENG, J. WANG, A. WU, J. SHEN and B. ZHOU, J. Non-Cryst. Solids 225 (1998) 101.10.1016/S0022-3093(98)00106-9 ↗